# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 348.17 _exptl_crystal_F_000 1192.00 _reflns_d_resolution_high 0.8393 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 15.4192 _cell_length_b 9.2424 _cell_length_c 21.2947 _cell_angle_alpha 90.000 _cell_angle_beta 109.924 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 33834.82 32268.14 620.53 o 4 0 0 274.08 366.88 7.09 o 6 0 0 3002.48 2616.60 37.92 o 8 0 0 10848.53 10169.53 139.07 o 10 0 0 9028.97 9220.54 196.24 o 12 0 0 1139.31 1110.50 21.69 o 14 0 0 1283.87 1277.90 37.20 o 16 0 0 1027.14 1122.19 36.46 o 1 1 0 38605.36 37895.97 732.51 o 3 1 0 296.42 369.00 8.23 o 5 1 0 7297.73 7344.91 81.98 o 7 1 0 11802.54 11666.49 129.51 o 9 1 0 9738.25 9854.69 95.77 o 11 1 0 421.96 457.29 8.57 o 13 1 0 13.08 16.42 5.72 o 15 1 0 987.42 1000.12 23.14 o 17 1 0 583.90 629.19 19.54 o 0 2 0 1288.82 1421.13 28.89 o 2 2 0 16321.35 17013.38 219.33 o 4 2 0 9707.75 9575.13 92.38 o 6 2 0 6471.65 6418.74 63.41 o 8 2 0 4182.42 4287.30 50.44 o 10 2 0 1112.89 1082.90 16.74 o 12 2 0 1064.25 1042.21 17.52 o 14 2 0 30.01 26.62 6.14 o 16 2 0 575.49 594.27 18.45 o 1 3 0 598.70 729.63 8.54 o 3 3 0 885.60 1029.45 11.36 o 5 3 0 3747.02 3423.21 35.06 o 7 3 0 242.35 134.98 5.85 o 9 3 0 1745.35 1668.17 22.81 o 11 3 0 3404.19 3336.49 41.87 o 13 3 0 1913.26 1915.11 27.69 o 15 3 0 1261.32 1290.29 27.84 o 0 4 0 4316.93 4060.34 46.63 o 2 4 0 6086.16 5803.29 57.00 o 4 4 0 7966.08 8164.19 71.01 o 6 4 0 9089.87 9648.35 119.37 o 8 4 0 1979.71 1960.29 25.95 o 10 4 0 3187.16 3164.61 49.54 o 12 4 0 2799.79 2763.55 45.59 o 14 4 0 2428.57 2416.22 62.50 o 16 4 0 877.37 964.65 24.43 o 1 5 0 1898.46 1793.11 19.51 o 3 5 0 3700.21 3477.65 35.73 o 5 5 0 4410.09 4568.00 46.49 o 7 5 0 4795.98 4962.01 59.57 o 9 5 0 2097.91 2025.64 28.60 o 11 5 0 2753.14 2631.04 43.84 o 13 5 0 1408.71 1445.63 29.49 o 15 5 0 996.51 1086.14 26.05 o 0 6 0 1982.50 1839.53 29.72 o 2 6 0 1091.42 986.99 12.50 o 4 6 0 6376.03 6296.20 62.97 o 6 6 0 4132.96 4101.14 42.88 o 8 6 0 1497.48 1522.37 23.01 o 10 6 0 825.95 830.69 16.50 o 12 6 0 301.68 338.66 14.19 o 14 6 0 676.56 761.24 21.56 o 1 7 0 2748.94 2787.23 30.65 o 3 7 0 784.90 810.25 13.83 o 5 7 0 292.77 276.23 8.25 o 7 7 0 11.77 16.47 4.91 o 9 7 0 230.97 248.69 9.94 o 11 7 0 236.28 275.76 12.73 o 13 7 0 591.46 641.12 54.19 o 0 8 0 648.71 641.95 15.48 o 2 8 0 1840.60 1842.13 22.35 o 4 8 0 562.62 564.10 11.99 o 6 8 0 647.22 636.20 17.10 o 8 8 0 1703.38 1821.65 44.77 o 10 8 0 732.13 796.98 21.95 o 1 9 0 489.33 488.31 10.15 o 3 9 0 1710.34 1688.89 21.74 o 5 9 0 1206.75 1276.12 26.39 o 7 9 0 871.91 886.17 21.96 o 9 9 0 362.72 376.01 16.17 o 0 10 0 1120.20 1054.93 22.84 o 2 10 0 866.48 819.58 16.46 o 4 10 0 1226.48 1220.23 21.47 o 6 10 0 624.85 683.77 19.81 o -17 1 1 0.85 12.79 8.74 o -15 1 1 67.12 50.74 8.72 o -13 1 1 4.03 -6.71 4.76 o -11 1 1 294.71 292.87 6.89 o -9 1 1 43.43 51.41 8.18 o -7 1 1 955.81 1231.72 21.30 o -5 1 1 31.75 44.17 2.78 o -3 1 1 1350.84 1440.09 21.32 o -1 1 1 1361.71 1367.17 28.52 o 1 1 1 1483.49 1647.26 23.58 o 3 1 1 220.25 194.64 4.09 o 5 1 1 1279.49 1224.79 15.89 o 7 1 1 171.67 159.22 5.58 o 9 1 1 73.07 62.00 6.16 o 11 1 1 41.60 30.15 3.65 o 13 1 1 5351.43 5139.77 62.42 o 15 1 1 136.77 156.75 9.41 o -16 2 1 17.59 33.35 8.82 o -14 2 1 466.51 398.44 11.27 o -12 2 1 1007.95 985.83 16.75 o -10 2 1 64.88 85.35 4.24 o -8 2 1 28.03 23.97 3.12 o -6 2 1 994.87 993.55 14.92 o -4 2 1 702.44 692.16 12.10 o -2 2 1 7529.92 7757.74 75.16 o 0 2 1 16363.78 16166.75 273.58 o 2 2 1 4517.21 4929.22 44.89 o 4 2 1 2397.89 2567.67 26.32 o 6 2 1 8598.69 9535.16 137.48 o 8 2 1 16.45 30.40 4.41 o 10 2 1 348.05 283.18 8.43 o 12 2 1 379.67 338.65 14.01 o 14 2 1 419.70 352.71 11.32 o 16 2 1 11.75 17.70 6.82 o -15 3 1 0.04 10.04 7.45 o -13 3 1 8.32 11.25 5.09 o -11 3 1 2.38 7.84 4.18 o -9 3 1 8.17 2.39 3.07 o -7 3 1 4329.32 4473.57 46.22 o -5 3 1 557.27 637.54 9.81 o -3 3 1 209.10 181.49 5.01 o -1 3 1 4714.95 4940.26 48.28 o 1 3 1 352.26 319.39 6.61 o 3 3 1 2499.89 2876.05 25.95 o 5 3 1 4096.15 4623.30 46.32 o 7 3 1 71.52 114.79 4.72 o 9 3 1 323.11 296.77 8.12 o 11 3 1 489.93 492.68 11.44 o 13 3 1 52.80 75.25 8.45 o 15 3 1 10.84 21.08 8.31 o -16 4 1 0.03 17.66 8.68 o -14 4 1 3.12 17.24 10.66 o -12 4 1 43.26 48.06 7.47 o -10 4 1 308.60 315.88 8.12 o -8 4 1 661.80 702.43 20.45 o -6 4 1 5037.14 5078.94 65.91 o -4 4 1 196.51 171.06 3.82 o -2 4 1 132.64 77.23 4.16 o 0 4 1 993.54 1128.63 13.61 o 2 4 1 678.08 827.60 10.18 o 4 4 1 567.20 677.96 9.27 o 6 4 1 1058.30 1155.00 14.44 o 8 4 1 5.55 4.90 3.17 o 10 4 1 72.05 73.61 7.02 o 12 4 1 16.64 33.53 13.58 o 14 4 1 19.07 33.11 13.83 o -15 5 1 238.16 284.92 15.07 o -13 5 1 295.31 285.44 13.50 o -11 5 1 66.55 60.36 6.71 o -9 5 1 2.39 0.12 4.44 o -7 5 1 385.78 353.62 9.37 o -5 5 1 3135.57 3380.21 35.17 o -3 5 1 1962.14 1975.37 21.48 o -1 5 1 587.18 560.00 6.18 o 1 5 1 821.95 824.85 10.44 o 3 5 1 749.98 757.45 19.36 o 5 5 1 3.20 5.97 2.49 o 7 5 1 1065.21 1201.10 18.73 o 9 5 1 346.21 371.41 10.68 o 11 5 1 167.27 155.77 10.68 o 13 5 1 61.67 61.11 9.29 o 15 5 1 7.16 17.67 9.05 o -14 6 1 50.43 71.59 10.09 o -12 6 1 25.44 23.34 7.70 o -10 6 1 124.22 129.16 7.85 o -8 6 1 49.51 67.17 6.79 o -6 6 1 307.41 328.29 15.56 o -4 6 1 482.97 497.50 11.65 o -2 6 1 72.85 88.56 3.87 o 0 6 1 31.24 27.94 2.83 o 2 6 1 522.18 625.23 9.23 o 4 6 1 9.38 6.88 4.74 o 6 6 1 614.09 553.59 9.53 o 8 6 1 15.50 14.24 4.73 o 10 6 1 4.59 4.18 5.30 o 12 6 1 2.07 -10.86 7.24 o 14 6 1 83.77 101.85 11.30 o -13 7 1 8.97 15.57 8.68 o -11 7 1 6.73 -3.21 6.18 o -9 7 1 2.37 5.58 6.75 o -7 7 1 8.08 5.03 4.44 o -5 7 1 451.15 457.72 13.28 o -3 7 1 1448.62 1455.73 22.21 o -1 7 1 330.35 343.25 8.71 o 1 7 1 566.54 538.60 9.37 o 3 7 1 360.34 322.95 8.57 o 5 7 1 17.57 19.18 3.54 o 7 7 1 144.05 119.75 7.29 o 9 7 1 2.87 -4.90 5.20 o 11 7 1 87.11 67.36 7.91 o 13 7 1 3.10 5.21 8.80 o -12 8 1 11.57 7.50 7.80 o -10 8 1 280.46 297.24 14.67 o -8 8 1 451.60 473.24 16.00 o -6 8 1 0.06 -9.33 7.32 o -4 8 1 184.51 168.56 10.27 o -2 8 1 97.22 98.95 5.57 o 0 8 1 2.01 0.64 3.92 o 2 8 1 452.65 434.43 9.12 o 4 8 1 986.11 977.01 17.40 o 6 8 1 432.01 420.14 14.25 o 8 8 1 303.64 293.12 19.84 o 10 8 1 232.01 216.25 13.96 o -9 9 1 256.23 284.06 28.83 o -7 9 1 79.71 89.85 9.90 o -5 9 1 30.10 23.46 7.89 o -3 9 1 2.51 -5.33 5.27 o -1 9 1 1.07 -6.44 4.30 o 1 9 1 34.13 26.60 4.77 o 3 9 1 145.99 159.60 7.46 o 5 9 1 415.23 441.56 15.56 o 7 9 1 0.09 6.12 8.02 o 9 9 1 137.82 154.94 12.54 o -6 10 1 6.88 1.07 8.59 o -4 10 1 344.57 307.80 11.24 o -2 10 1 27.93 6.67 8.38 o 0 10 1 0.19 -6.87 6.63 o 2 10 1 177.71 165.22 8.07 o 4 10 1 7.00 25.56 7.30 o 6 10 1 4.00 14.76 13.39 o -16 0 2 1917.14 1878.22 49.73 o -14 0 2 923.42 845.89 28.40 o -12 0 2 7294.09 7199.96 160.47 o -10 0 2 5576.85 5740.42 81.05 o -8 0 2 4716.68 5197.57 72.72 o -6 0 2 2799.41 2803.68 40.02 o -4 0 2 24655.54 23986.91 458.58 o -2 0 2 121218.91 121840.95 2403.02 o 0 0 2 39834.08 31630.37 612.85 o 4 0 2 6054.48 6239.69 121.40 o 6 0 2 4649.69 4708.94 94.25 o 8 0 2 3955.86 3846.07 55.98 o 10 0 2 2507.76 2423.89 38.34 o 12 0 2 434.57 460.37 22.70 o 14 0 2 213.54 215.03 23.50 o 16 0 2 991.08 1056.97 36.21 o -17 1 2 634.44 680.47 19.72 o -15 1 2 561.33 608.45 23.25 o -13 1 2 177.96 182.94 8.45 o -11 1 2 1654.82 1670.18 19.66 o -9 1 2 7638.63 7905.14 77.17 o -7 1 2 6164.65 6251.83 60.96 o -5 1 2 9026.50 9156.76 88.48 o -3 1 2 2625.53 2672.03 48.45 o -1 1 2 11024.46 11758.83 171.34 o 1 1 2 11109.26 11356.63 154.62 o 3 1 2 5928.51 5929.27 79.73 o 5 1 2 12465.65 13100.04 144.67 o 7 1 2 10758.41 11072.79 123.64 o 9 1 2 5236.99 5099.51 60.04 o 11 1 2 3371.96 3187.44 34.77 o 13 1 2 1594.00 1631.48 21.20 o 15 1 2 1358.36 1338.34 22.86 o -16 2 2 606.27 646.06 18.58 o -14 2 2 842.70 872.14 16.26 o -12 2 2 300.47 299.65 9.25 o -10 2 2 7082.19 6928.47 92.73 o -8 2 2 6084.67 5654.41 64.91 o -6 2 2 460.48 394.31 6.98 o -4 2 2 2414.21 2117.05 25.27 o -2 2 2 436.08 383.04 12.62 o 0 2 2 55173.43 53359.08 705.84 o 2 2 2 268.86 355.08 4.25 o 4 2 2 1729.16 1722.35 18.52 o 6 2 2 22187.12 23228.14 254.69 o 8 2 2 2260.51 2106.25 33.11 o 10 2 2 633.43 688.92 12.98 o 12 2 2 139.45 138.42 8.73 o 14 2 2 791.77 822.15 16.81 o 16 2 2 729.18 825.99 18.98 o -17 3 2 391.53 384.06 23.19 o -15 3 2 749.92 775.58 16.14 o -13 3 2 1631.60 1699.73 25.04 o -11 3 2 167.52 194.50 9.75 o -9 3 2 2215.32 1947.50 24.92 o -7 3 2 184.35 371.14 7.28 o -5 3 2 160.32 295.73 12.23 o -3 3 2 2401.01 2315.49 27.26 o -1 3 2 5848.25 5777.95 45.81 o 1 3 2 18503.04 18144.73 173.16 o 3 3 2 356.92 416.17 5.23 o 5 3 2 11333.87 12199.72 120.10 o 7 3 2 9155.73 9078.72 102.35 o 9 3 2 2385.32 2425.53 31.49 o 11 3 2 1562.23 1567.58 23.23 o 13 3 2 681.57 596.44 13.76 o 15 3 2 1253.63 1299.39 28.06 o -16 4 2 889.67 971.38 23.99 o -14 4 2 2198.36 2238.28 39.48 o -12 4 2 3419.94 3372.51 53.13 o -10 4 2 2625.03 2699.99 35.92 o -8 4 2 3577.47 3595.20 37.77 o -6 4 2 8196.69 8038.49 83.27 o -4 4 2 7285.52 7480.32 65.04 o -2 4 2 5865.85 5802.08 46.26 o 0 4 2 13607.64 13904.23 133.33 o 2 4 2 6517.98 6760.76 66.27 o 4 4 2 6814.73 6806.40 90.49 o 6 4 2 1465.04 1302.14 15.69 o 8 4 2 2825.25 2799.05 45.23 o 10 4 2 1982.29 1917.71 33.71 o 12 4 2 1116.15 1112.73 24.09 o 14 4 2 650.37 614.68 20.21 o -15 5 2 818.99 855.52 42.10 o -13 5 2 1523.33 1524.89 29.97 o -11 5 2 3456.11 3500.40 45.71 o -9 5 2 2461.19 2390.59 32.17 o -7 5 2 3926.30 3856.73 47.09 o -5 5 2 12555.36 12651.43 122.41 o -3 5 2 4371.70 4606.07 50.11 o -1 5 2 5491.16 5720.74 64.90 o 1 5 2 799.40 703.70 9.44 o 3 5 2 3298.78 3299.93 34.29 o 5 5 2 4463.05 4168.66 43.09 o 7 5 2 2063.26 2015.07 27.82 o 9 5 2 2940.31 2863.75 38.60 o 11 5 2 1109.20 1132.79 28.89 o 13 5 2 1137.45 1131.37 25.63 o -14 6 2 240.21 287.34 17.24 o -12 6 2 1306.58 1335.50 23.12 o -10 6 2 2163.10 2261.72 31.92 o -8 6 2 5437.10 5568.32 66.89 o -6 6 2 7873.72 7697.98 89.12 o -4 6 2 6700.68 6465.08 64.40 o -2 6 2 2648.63 2621.44 28.46 o 0 6 2 159.66 120.24 4.79 o 2 6 2 2255.77 2222.62 24.35 o 4 6 2 1191.18 1192.45 15.21 o 6 6 2 536.27 521.91 9.43 o 8 6 2 12.28 14.64 4.91 o 10 6 2 261.72 281.99 12.49 o 12 6 2 1024.37 1086.83 25.07 o -13 7 2 731.96 786.18 18.19 o -11 7 2 1018.80 1055.38 19.95 o -9 7 2 155.47 173.21 8.67 o -7 7 2 331.27 374.12 34.25 o -5 7 2 295.27 269.11 10.74 o -3 7 2 3633.93 3531.28 43.43 o -1 7 2 1098.28 1057.28 14.27 o 1 7 2 985.33 900.95 12.72 o 3 7 2 1415.21 1449.52 20.92 o 5 7 2 140.17 149.02 7.18 o 7 7 2 368.21 352.08 10.28 o 9 7 2 86.33 94.67 8.55 o 11 7 2 555.77 628.00 18.91 o -12 8 2 488.10 535.39 19.48 o -10 8 2 1049.68 1051.88 36.09 o -8 8 2 673.37 665.92 21.83 o -6 8 2 1307.02 1338.82 26.70 o -4 8 2 2775.25 2626.67 43.23 o -2 8 2 1658.24 1660.47 20.54 o 0 8 2 713.04 669.37 11.25 o 2 8 2 370.35 371.61 9.13 o 4 8 2 161.64 183.66 10.93 o 6 8 2 794.70 861.13 20.34 o 8 8 2 1103.91 1125.86 26.23 o 10 8 2 1009.59 1031.08 20.55 o -9 9 2 331.38 354.67 22.07 o -7 9 2 670.74 684.17 23.38 o -5 9 2 777.36 743.20 19.15 o -3 9 2 262.63 256.48 9.39 o -1 9 2 534.32 544.11 11.28 o 1 9 2 2355.63 2308.68 27.49 o 3 9 2 2840.24 2869.22 33.15 o 5 9 2 2006.35 1931.29 50.10 o 7 9 2 713.19 773.86 20.74 o 9 9 2 665.46 723.43 34.05 o -6 10 2 836.62 857.93 22.13 o -4 10 2 249.37 261.20 12.91 o -2 10 2 622.98 645.23 14.88 o 0 10 2 813.84 737.05 13.15 o 2 10 2 1933.53 1881.17 24.29 o 4 10 2 2040.43 2013.07 30.31 o 6 10 2 258.44 265.67 24.24 o -17 1 3 24.21 24.30 8.90 o -15 1 3 16.95 23.46 7.49 o -13 1 3 2054.12 2108.15 28.89 o -11 1 3 282.76 266.52 7.83 o -9 1 3 188.11 223.82 8.13 o -7 1 3 8524.25 9557.48 91.87 o -5 1 3 242.18 220.89 3.92 o -3 1 3 24698.23 24970.19 241.50 o -1 1 3 12215.47 12481.02 169.49 o 1 1 3 5260.23 5425.34 52.44 o 3 1 3 384.42 394.35 6.48 o 5 1 3 829.66 874.53 17.94 o 7 1 3 3.79 8.09 3.37 o 9 1 3 9.17 13.55 6.00 o 11 1 3 5125.78 4953.38 51.55 o 13 1 3 242.81 278.71 8.92 o 15 1 3 220.83 218.21 10.72 o -16 2 3 1.68 -6.38 7.32 o -14 2 3 405.90 401.12 11.16 o -12 2 3 2146.88 2109.96 28.55 o -10 2 3 44.67 47.39 6.79 o -8 2 3 1091.55 1167.78 12.49 o -6 2 3 213.35 232.80 5.59 o -4 2 3 281.40 238.67 4.54 o -2 2 3 3095.37 3107.64 30.88 o 0 2 3 109910.98 112203.27 4717.50 o 2 2 3 232.83 267.55 3.68 o 4 2 3 9308.92 9999.81 165.30 o 6 2 3 4656.30 5273.86 68.41 o 8 2 3 47.84 77.70 6.03 o 10 2 3 35.71 47.71 5.11 o 12 2 3 1859.69 1758.54 26.08 o 14 2 3 78.92 82.26 7.71 o 16 2 3 6.73 -2.14 6.67 o -17 3 3 8.58 7.44 12.28 o -15 3 3 53.97 50.46 6.59 o -13 3 3 246.84 266.93 9.40 o -11 3 3 197.11 190.41 11.94 o -9 3 3 1186.17 1193.66 15.30 o -7 3 3 74.91 74.57 3.69 o -5 3 3 470.05 448.15 6.53 o -3 3 3 523.57 557.55 7.11 o -1 3 3 4125.57 4183.65 31.19 o 1 3 3 20399.57 21139.11 245.45 o 3 3 3 433.56 442.36 5.65 o 5 3 3 21.74 44.81 3.11 o 7 3 3 1.31 13.35 4.11 o 9 3 3 868.99 881.82 14.92 o 11 3 3 21.92 18.82 4.94 o 13 3 3 286.28 269.85 12.92 o 15 3 3 28.10 30.34 9.98 o -16 4 3 24.12 35.85 9.05 o -14 4 3 71.11 94.08 9.34 o -12 4 3 4.61 11.93 6.46 o -10 4 3 76.19 80.26 5.91 o -8 4 3 2.42 25.53 7.25 o -6 4 3 63.26 58.03 2.65 o -4 4 3 898.15 1071.49 11.05 o -2 4 3 3631.48 3817.83 31.01 o 0 4 3 2197.39 2454.94 25.37 o 2 4 3 2371.01 2582.37 27.03 o 4 4 3 147.45 229.86 4.23 o 6 4 3 113.69 130.49 4.81 o 8 4 3 1425.08 1482.49 27.00 o 10 4 3 5.53 -3.19 5.42 o 12 4 3 40.47 46.85 7.87 o 14 4 3 120.56 86.05 9.98 o -15 5 3 163.27 128.71 11.96 o -13 5 3 7.31 14.41 7.27 o -11 5 3 0.30 6.11 5.43 o -9 5 3 41.15 45.32 5.26 o -7 5 3 297.05 294.15 11.96 o -5 5 3 406.21 399.88 9.28 o -3 5 3 1656.20 1656.49 14.68 o -1 5 3 2531.31 2751.83 30.78 o 1 5 3 1535.91 1672.46 18.61 o 3 5 3 3.24 -0.06 2.07 o 5 5 3 120.39 131.64 10.04 o 7 5 3 446.90 484.66 11.21 o 9 5 3 125.43 146.15 9.64 o 11 5 3 0.06 0.95 6.38 o 13 5 3 149.23 136.79 16.62 o -14 6 3 104.03 148.92 11.27 o -12 6 3 72.48 77.10 10.02 o -10 6 3 313.77 360.52 10.89 o -8 6 3 214.83 275.78 11.19 o -6 6 3 706.35 737.30 30.97 o -4 6 3 90.88 39.43 5.96 o -2 6 3 441.59 463.20 8.02 o 0 6 3 5.88 12.15 2.28 o 2 6 3 24.27 21.84 2.79 o 4 6 3 37.66 42.91 3.72 o 6 6 3 757.40 742.82 12.58 o 8 6 3 725.14 679.66 14.29 o 10 6 3 61.39 46.53 8.01 o 12 6 3 46.12 46.16 8.99 o -13 7 3 35.89 30.73 7.57 o -11 7 3 216.57 209.64 10.26 o -9 7 3 43.92 43.13 9.38 o -7 7 3 14.19 16.44 4.42 o -5 7 3 49.31 54.16 7.19 o -3 7 3 1524.99 1438.51 17.93 o -1 7 3 9.61 7.22 3.17 o 1 7 3 96.97 114.03 5.45 o 3 7 3 27.06 37.25 11.26 o 5 7 3 434.88 460.03 19.58 o 7 7 3 148.22 158.41 9.17 o 9 7 3 230.80 222.38 10.50 o 11 7 3 0.41 -7.31 7.64 o -12 8 3 5.01 6.59 9.16 o -10 8 3 0.83 3.96 8.42 o -8 8 3 410.23 414.85 14.91 o -6 8 3 538.91 488.13 15.48 o -4 8 3 140.83 129.90 7.43 o -2 8 3 3.51 -1.95 3.61 o 0 8 3 3.70 9.51 3.70 o 2 8 3 0.87 -2.54 3.61 o 4 8 3 72.03 80.42 6.15 o 6 8 3 200.81 174.74 12.34 o 8 8 3 46.85 46.54 9.01 o 10 8 3 81.96 90.99 8.83 o -9 9 3 52.56 59.52 10.07 o -7 9 3 79.26 81.72 9.25 o -5 9 3 1.87 4.96 10.61 o -3 9 3 24.44 12.68 5.36 o -1 9 3 1.29 -7.25 4.83 o 1 9 3 17.96 28.76 4.96 o 3 9 3 914.25 991.52 15.67 o 5 9 3 2.33 1.90 11.90 o 7 9 3 1.32 -3.12 7.93 o 9 9 3 1.18 7.46 9.41 o -6 10 3 92.23 85.39 10.54 o -4 10 3 66.62 58.42 9.18 o -2 10 3 1.60 -10.39 6.93 o 0 10 3 40.25 22.34 6.46 o 2 10 3 131.30 175.96 17.28 o 4 10 3 81.96 83.35 10.39 o 6 10 3 0.30 -1.24 11.78 o -18 0 4 868.65 888.30 33.11 o -16 0 4 2377.00 2325.39 58.16 o -14 0 4 8934.43 8732.99 175.97 o -12 0 4 6170.51 6211.66 126.74 o -10 0 4 6882.86 6422.08 89.72 o -8 0 4 2643.31 2615.09 41.05 o -6 0 4 2678.68 2965.34 41.93 o -4 0 4 30369.00 28596.63 697.85 o -2 0 4 1804.20 1766.86 35.96 o 0 0 4 1469.06 1640.87 33.61 o 4 0 4 12070.89 12075.98 231.65 o 6 0 4 51261.10 51674.96 980.78 o 8 0 4 1247.55 1355.16 33.98 o 10 0 4 10.64 6.85 4.52 o 12 0 4 3491.48 3260.18 51.54 o 14 0 4 1673.30 1658.63 31.49 o 16 0 4 843.80 981.81 35.59 o -17 1 4 408.70 419.03 16.04 o -15 1 4 501.45 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