Acta Cryst. (2011). E67, o1727-o1728 [ doi:10.1107/S1600536811022768 ]
Online 18 June 2011
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Alert level C PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 28 PLAT915_ALERT_3_C Low Friedel Pair Coverage ...................... 89 Perc.
Alert level G REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 74.20 From the CIF: _reflns_number_total 3252 Count of symmetry unique reflns 1886 Completeness (_total/calc) 172.43% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 1366 Fraction of Friedel pairs measured 0.724 Are heavy atom types Z>Si present no PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 H2 O PLAT791_ALERT_4_G Note: The Model has Chirality at C19 (Verify) S PLAT916_ALERT_2_G Hooft y and Flack x Parameter values differ by . 0.25
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check
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