Received 20 July 2011
The five-membered ring in the title compound, C6H13O3P, exists in an envelope conformation with one of the ring C atoms at the flap position. The coordination geometry around the P atom is a distorted tetrahedron. The crystal structure is stabilized by several weak C-HO and P-HO hydrogen bonds, forming a three-dimensional network.
For a discussion of 1,3,2-dioxaphospholane chemistry, see: Maffei & Buono (2003); Zwierzak (1967) and for the Heck reaction, see: Beletskaya & Cheprakov (2000); Skarzynska et al. (2011). For hydrogen-bond interactions, see: Desiraju & Steiner (1999). For bond lengths in organic compounds, see: Allen et al. (1987). For details of the temperature control applied during data collection, see: Cosier & Glazer (1986) and for specifications of the analytical numeric absorption correction, see: Clark & Reid (1995).
Data collection: CrysAlis CCD (Oxford Diffraction, 2010); cell refinement: CrysAlis RED (Oxford Diffraction, 2010); data reduction: CrysAlis RED; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: ORTEP-3 (Farrugia, 1997); software used to prepare material for publication: SHELXL97.
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: BT5583 ).
This work was partially supported by the Polish Ministry of Science and Higher Education through grant No. N204 028538. The financial support is gratefully acknowledged.
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