Acta Cryst. (2011). E67, o2755-o2756 [ doi:10.1107/S160053681103858X ]
Online 30 September 2011
No syntax errors found
Alert level C PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0073 Ang PLAT430_ALERT_2_C Short Inter D...A Contact O1 .. O2 .. 2.88 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 9
Alert level G REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 25.00 From the CIF: _reflns_number_total 2588 Count of symmetry unique reflns 1456 Completeness (_total/calc) 177.75% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 1132 Fraction of Friedel pairs measured 0.777 Are heavy atom types Z>Si present yes PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large. 0.10 PLAT791_ALERT_4_G Note: The Model has Chirality at C3 (Verify) R PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 60 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
checkCIF publication errors
Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
|Author Response: The contribution of the authors to this submission is as follows: Caracelli - co-responsible for final crystallography and write-up Coelho - responsible for the data collection and preliminary cryst. anal. Olivato - co-supervisor of students Cerqueira - responsible for the synthesis and crystallization Santos - responsible for the synthesis and crystallization Tiekink - co-responsible for final crystallography and write-up|
1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing
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