# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 101228g in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 459.97 _exptl_crystal_F_000 1428.00 _reflns_d_resolution_high 0.8403 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.9868 _cell_length_b 14.7498 _cell_length_c 18.7887 _cell_angle_alpha 89.613 _cell_angle_beta 85.858 _cell_angle_gamma 88.490 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1110.48 880.49 44.94 o 3 0 0 358.88 367.72 34.73 o 4 0 0 53.39 75.59 32.69 o 5 0 0 7505.08 6980.62 243.11 o 6 0 0 6788.50 7975.52 281.92 o 7 0 0 8532.50 9358.57 330.95 o 8 0 0 111.58 208.38 63.33 o 9 0 0 1317.04 1062.31 104.19 o 10 0 0 62.28 110.32 75.59 o 11 0 0 252.49 230.54 69.67 o 12 0 0 665.62 1064.36 194.08 o -13 1 0 563.44 884.58 194.08 o -12 1 0 32.78 46.99 93.97 o -11 1 0 480.63 788.56 151.18 o -10 1 0 1020.85 960.17 149.13 o -9 1 0 401.28 546.17 73.63 o -8 1 0 11.17 -20.43 42.90 o -7 1 0 18.59 49.03 46.99 o -6 1 0 70.03 202.25 53.12 o -5 1 0 206.93 124.62 36.77 o -4 1 0 6158.19 7662.95 239.02 o -3 1 0 8596.90 7832.52 230.85 o -2 1 0 2303.72 2253.33 87.85 o 2 1 0 432.02 557.71 38.82 o 3 1 0 1519.86 1427.99 73.54 o 4 1 0 121.95 75.59 34.73 o 5 1 0 60.10 46.99 38.82 o 6 1 0 2451.92 2214.51 126.66 o 7 1 0 413.14 371.81 81.72 o 8 1 0 361.87 514.81 96.02 o 9 1 0 312.62 208.38 79.67 o 10 1 0 113.12 98.06 79.67 o 11 1 0 1236.94 1599.60 187.95 o 12 1 0 665.87 749.75 151.18 o -13 2 0 0.57 63.33 102.15 o -12 2 0 725.14 853.94 167.52 o -11 2 0 1435.08 1869.26 220.63 o -10 2 0 322.97 435.14 118.49 o -9 2 0 4019.11 3706.88 105.64 o -8 2 0 840.00 839.45 45.89 o -7 2 0 3450.93 3136.84 88.37 o -6 2 0 1848.33 2252.41 83.76 o -5 2 0 6219.62 5230.32 104.18 o -4 2 0 394.31 1034.95 33.62 o -3 2 0 15967.08 16762.60 330.20 o -2 2 0 143320.53 145829.02 3765.08 o -1 2 0 975.96 555.67 36.77 o 0 2 0 16023.67 19150.23 518.90 o 1 2 0 283.88 232.15 27.58 o 2 2 0 4589.06 4214.28 101.65 o 3 2 0 2186.12 2820.73 79.39 o 4 2 0 2227.50 3199.20 140.96 o 5 2 0 186.47 136.87 46.99 o 6 2 0 2155.32 1799.80 116.45 o 7 2 0 5272.06 5448.44 239.02 o 8 2 0 1527.79 1381.01 116.45 o 9 2 0 2215.70 2241.07 157.30 o 10 2 0 1362.36 1483.15 136.87 o 11 2 0 1705.62 1407.56 140.96 o 12 2 0 1095.07 1447.32 139.94 o 13 2 0 552.55 565.89 143.00 o -13 3 0 48.17 114.40 130.75 o -12 3 0 21.80 32.69 91.93 o -11 3 0 10.59 30.64 87.85 o -10 3 0 821.79 788.56 140.96 o -9 3 0 1718.54 1472.94 130.75 o -8 3 0 362.62 442.11 45.00 o -7 3 0 49.31 69.38 26.02 o -6 3 0 567.68 681.35 58.98 o -5 3 0 341.01 530.35 37.77 o -4 3 0 27133.67 29731.70 572.57 o -3 3 0 4476.28 5375.66 175.69 o -2 3 0 23689.43 23325.94 651.69 o -1 3 0 1395.38 1756.90 83.76 o 0 3 0 3900.64 3648.00 88.62 o 1 3 0 4927.30 6540.70 205.31 o 2 3 0 2991.61 2535.06 74.30 o 3 3 0 7070.95 7180.15 131.43 o 4 3 0 734.95 657.82 66.39 o 5 3 0 406.82 395.05 46.16 o 6 3 0 2668.00 1995.52 120.53 o 7 3 0 588.16 579.79 113.38 o 8 3 0 806.89 906.28 100.10 o 9 3 0 1.94 -24.97 41.59 o 10 3 0 517.11 505.24 80.86 o 11 3 0 26.56 -32.02 53.21 o 12 3 0 460.89 355.47 124.62 o 13 3 0 670.64 569.97 147.09 o -13 4 0 26.97 -130.75 98.06 o -12 4 0 24.77 -61.29 93.97 o -11 4 0 1646.08 1481.11 153.22 o -10 4 0 929.01 1103.17 159.35 o -9 4 0 1707.85 2300.32 171.60 o -8 4 0 2231.21 2067.42 153.22 o -7 4 0 2038.71 1989.84 135.85 o -6 4 0 1138.30 1250.09 114.40 o -5 4 0 146.51 438.86 109.30 o -4 4 0 58.56 -13.19 15.69 o -3 4 0 21132.66 23607.50 458.85 o -2 4 0 1578.52 2151.06 73.54 o -1 4 0 18533.38 18904.07 398.37 o 0 4 0 2601.97 4140.30 104.98 o 1 4 0 11722.26 11654.61 323.80 o 2 4 0 7857.82 8177.62 185.52 o 3 4 0 4036.58 4112.16 85.79 o 4 4 0 10636.99 10648.75 190.90 o 5 4 0 1841.85 1402.31 61.18 o 6 4 0 4334.92 4509.73 134.45 o 7 4 0 5161.90 5824.78 168.08 o 8 4 0 2556.15 2581.17 205.31 o 9 4 0 1302.38 1156.38 83.22 o 10 4 0 1312.80 1117.47 165.48 o 11 4 0 1040.06 1045.97 167.52 o 12 4 0 50.47 -26.56 89.89 o 13 4 0 0.90 -49.03 89.89 o -13 5 0 392.80 377.94 157.30 o -12 5 0 410.94 465.78 140.96 o -11 5 0 209.61 265.58 114.40 o -10 5 0 201.59 249.23 100.10 o -9 5 0 2046.12 1765.07 151.18 o -8 5 0 378.17 200.21 83.76 o -7 5 0 309.20 173.65 71.50 o -6 5 0 2442.94 2704.82 89.19 o -5 5 0 0.42 4.60 21.02 o -4 5 0 6327.54 6576.75 293.16 o -3 5 0 1432.25 1147.13 65.37 o -2 5 0 37.20 133.77 42.90 o -1 5 0 273.23 217.22 30.23 o 0 5 0 6016.04 6840.49 162.12 o 1 5 0 79.56 59.72 21.10 o 2 5 0 8568.34 9692.67 286.01 o 3 5 0 4021.04 4574.54 100.53 o 4 5 0 371.05 362.77 62.39 o 5 5 0 1177.44 984.04 42.19 o 6 5 0 88.45 127.52 36.24 o 7 5 0 232.34 222.54 56.18 o 8 5 0 19.61 -47.90 35.19 o 9 5 0 0.66 -12.26 65.37 o 10 5 0 0.62 -40.86 69.46 o 11 5 0 831.12 578.14 143.00 o 12 5 0 223.16 294.18 118.49 o 13 5 0 323.68 377.94 140.96 o -13 6 0 352.93 55.16 114.40 o -12 6 0 268.59 488.26 149.13 o -11 6 0 15.11 38.82 93.97 o -10 6 0 339.80 167.52 96.02 o -9 6 0 2183.15 2165.48 171.60 o -8 6 0 1327.48 1252.30 161.39 o -7 6 0 464.05 420.84 98.06 o -6 6 0 1172.27 1084.78 104.19 o -5 6 0 376.34 588.97 40.38 o -4 6 0 230.02 343.33 44.94 o -3 6 0 7864.04 9426.02 211.54 o -2 6 0 12134.21 12840.66 274.58 o -1 6 0 8049.36 8756.06 466.80 o 0 6 0 6105.59 5791.63 171.60 o 1 6 0 2361.62 2771.77 91.65 o 2 6 0 4727.57 3846.74 116.98 o 3 6 0 1230.68 1672.94 72.68 o 4 6 0 14986.27 16298.33 280.68 o 5 6 0 4623.83 5342.32 119.11 o 6 6 0 1118.84 1170.12 62.49 o 7 6 0 265.13 83.76 55.16 o 8 6 0 103.59 63.33 71.50 o 9 6 0 726.45 688.46 136.87 o 10 6 0 1893.54 2010.22 173.65 o 11 6 0 1804.14 1630.24 165.48 o 12 6 0 1192.57 1376.92 212.46 o 13 6 0 211.52 273.75 136.87 o -12 7 0 672.94 813.08 179.78 o -11 7 0 968.22 1058.23 185.90 o -10 7 0 43.24 91.93 85.80 o -9 7 0 38.62 -79.67 61.29 o -8 7 0 7.35 -30.64 63.33 o -7 7 0 3.78 44.94 67.42 o -6 7 0 3.63 -49.03 46.99 o -5 7 0 257.76 486.21 96.02 o -4 7 0 3.06 9.45 21.02 o -3 7 0 183.62 410.51 92.95 o -2 7 0 4900.52 4470.61 125.17 o -1 7 0 72.21 10.90 25.52 o 0 7 0 553.22 547.50 52.00 o 1 7 0 4518.20 4499.49 132.80 o 2 7 0 99.11 124.45 35.37 o 3 7 0 51.69 50.92 27.48 o 4 7 0 20.36 24.93 31.68 o 5 7 0 821.81 668.68 96.46 o 6 7 0 79.56 53.87 45.97 o 7 7 0 440.21 471.91 108.27 o 8 7 0 99.24 -24.51 65.37 o 9 7 0 1087.99 1227.79 171.60 o 10 7 0 293.05 192.03 110.32 o 11 7 0 199.08 114.40 104.19 o 12 7 0 181.45 204.29 120.53 o 13 7 0 17.94 -26.56 110.32 o -12 8 0 20.35 -140.96 93.97 o -11 8 0 22.51 16.34 89.89 o -10 8 0 144.93 -10.21 89.89 o -9 8 0 710.05 668.03 140.96 o -8 8 0 1878.66 1454.55 145.05 o -7 8 0 2276.01 2206.34 169.56 o -6 8 0 112.66 108.27 77.63 o -5 8 0 1930.54 2310.53 159.35 o -4 8 0 1485.67 1289.08 112.36 o -3 8 0 374.15 415.65 52.09 o -2 8 0 3955.35 3879.10 118.25 o -1 8 0 1726.66 1713.78 74.08 o 0 8 0 12462.66 13474.02 305.59 o 1 8 0 3124.29 3754.75 206.33 o 2 8 0 4828.65 4490.68 149.13 o 3 8 0 92.26 198.94 43.62 o 4 8 0 515.81 360.21 55.26 o 5 8 0 2163.16 2567.12 110.53 o 6 8 0 59.97 56.46 40.71 o 7 8 0 2175.76 2131.21 105.85 o 8 8 0 1218.31 1334.02 138.92 o 9 8 0 171.16 77.63 81.72 o 10 8 0 615.66 490.30 128.70 o 11 8 0 1006.57 1575.08 220.63 o 12 8 0 294.38 245.15 138.92 o -12 9 0 36.37 -73.54 104.19 o -11 9 0 632.17 723.19 177.73 o -10 9 0 327.21 214.51 118.49 o -9 9 0 4.52 4.09 69.46 o -8 9 0 43.46 96.02 77.63 o -7 9 0 13.84 -4.09 67.42 o -6 9 0 18.32 2.04 63.33 o -5 9 0 879.84 962.21 132.79 o -4 9 0 4185.25 3844.76 212.46 o -3 9 0 3243.34 3561.96 114.46 o -2 9 0 2540.95 2033.55 290.09 o -1 9 0 19.76 -16.34 43.92 o 0 9 0 796.67 966.44 79.93 o 1 9 0 15.52 24.25 62.31 o 2 9 0 933.74 973.62 64.96 o 3 9 0 228.24 226.16 68.44 o 4 9 0 54.20 40.69 35.37 o 5 9 0 181.91 107.46 43.05 o 6 9 0 192.55 234.64 59.23 o 7 9 0 424.20 673.37 121.55 o 8 9 0 89.56 73.54 85.80 o 9 9 0 13.45 14.30 83.76 o 10 9 0 112.59 32.69 77.63 o 11 9 0 4.76 -12.26 100.10 o 12 9 0 78.21 -61.29 106.23 o -11 10 0 619.87 584.27 175.69 o -10 10 0 758.48 862.11 185.90 o -9 10 0 196.24 18.39 93.97 o -8 10 0 19.11 0.00 79.67 o -7 10 0 1337.00 1781.42 200.21 o -6 10 0 311.63 396.32 104.19 o -5 10 0 185.01 232.89 96.02 o -4 10 0 94.62 77.63 71.50 o -3 10 0 250.53 163.43 73.54 o -2 10 0 699.13 688.26 56.76 o -1 10 0 1148.62 1088.30 78.65 o 0 10 0 1199.43 1313.82 161.39 o 1 10 0 2054.81 1949.47 93.60 o 2 10 0 2130.94 2267.81 103.22 o 3 10 0 1487.05 1704.70 91.72 o 4 10 0 1459.42 1229.37 80.55 o 5 10 0 1280.30 1528.17 180.80 o 6 10 0 176.13 116.67 69.46 o 7 10 0 357.27 334.68 72.99 o 8 10 0 404.86 367.72 116.45 o 9 10 0 552.78 486.21 124.62 o 10 10 0 323.16 443.31 140.96 o 11 10 0 257.37 12.26 110.32 o -10 11 0 810.54 829.42 183.86 o -9 11 0 656.42 678.25 159.35 o -8 11 0 19.32 8.17 77.63 o -7 11 0 23.91 -26.56 73.54 o -6 11 0 178.19 196.12 93.97 o -5 11 0 331.14 196.12 96.02 o -4 11 0 1067.23 1248.22 173.65 o -3 11 0 1435.84 1323.81 130.75 o -2 11 0 837.84 954.04 149.13 o -1 11 0 1133.49 960.07 100.10 o 0 11 0 0.18 -16.87 35.77 o 1 11 0 0.02 -9.87 38.68 o 2 11 0 0.90 -17.98 57.20 o 3 11 0 453.59 439.45 73.50 o 4 11 0 118.15 72.50 53.39 o 5 11 0 321.79 367.57 107.25 o 6 11 0 343.99 351.23 72.94 o 7 11 0 2.14 -39.94 44.16 o 8 11 0 362.54 185.90 106.23 o 9 11 0 99.45 153.22 106.23 o 10 11 0 8.23 4.09 93.97 o 11 11 0 63.27 -6.13 100.10 o -10 12 0 264.01 218.59 132.79 o -9 12 0 474.78 645.56 167.52 o -8 12 0 10.00 -6.13 83.76 o -7 12 0 1.87 -93.97 73.54 o -6 12 0 36.35 -57.20 77.63 o -5 12 0 23.66 14.30 71.50 o -4 12 0 722.64 888.67 157.30 o -3 12 0 1880.04 1889.69 163.43 o -2 12 0 980.33 1391.22 181.82 o -1 12 0 2190.64 1977.54 161.39 o 0 12 0 2399.77 2450.41 114.24 o 1 12 0 693.24 765.56 88.41 o 2 12 0 2595.85 2872.56 129.14 o 3 12 0 1242.01 1192.23 86.67 o 4 12 0 914.64 876.98 98.10 o 5 12 0 132.64 153.22 66.39 o 6 12 0 0.96 -17.61 48.10 o 7 12 0 29.79 34.73 83.76 o 8 12 0 93.27 -4.09 77.63 o 9 12 0 623.65 649.65 161.39 o 10 12 0 441.23 486.21 136.87 o -9 13 0 142.59 61.29 120.53 o -8 13 0 0.67 -122.57 81.72 o -7 13 0 2.76 2.04 87.85 o -6 13 0 0.30 -101.12 67.42 o -5 13 0 158.47 196.12 100.10 o -4 13 0 348.43 316.65 106.23 o -3 13 0 236.28 124.62 100.10 o -2 13 0 451.36 437.18 126.66 o -1 13 0 827.17 700.72 143.00 o 0 13 0 498.40 525.03 130.75 o 1 13 0 266.35 295.56 74.57 o 2 13 0 70.70 17.69 53.99 o 3 13 0 73.04 61.29 56.34 o 4 13 0 17.20 -12.01 57.20 o 5 13 0 139.81 143.70 57.05 o 6 13 0 103.93 51.07 87.85 o 7 13 0 0.04 -104.19 69.46 o 8 13 0 58.90 75.59 104.19 o 9 13 0 6.03 -73.54 85.80 o -8 14 0 114.89 -8.17 112.36 o -7 14 0 153.96 298.26 134.83 o -6 14 0 44.41 10.21 102.15 o -5 14 0 144.90 228.81 122.57 o -4 14 0 142.02 46.99 100.10 o -3 14 0 922.63 1115.43 177.73 o -2 14 0 456.04 682.33 136.87 o -1 14 0 7.81 36.77 89.89 o 0 14 0 78.07 85.80 91.93 o 1 14 0 20.70 -36.87 46.80 o 2 14 0 546.51 736.34 100.55 o 3 14 0 65.41 -18.13 51.94 o 4 14 0 267.03 363.29 125.64 o 5 14 0 203.57 155.13 67.16 o 6 14 0 7.26 -6.13 81.72 o 7 14 0 16.53 -26.56 87.85 o 8 14 0 167.79 198.16 124.62 o -7 15 0 31.15 14.30 116.45 o -6 15 0 352.57 341.17 145.05 o -5 15 0 337.82 200.21 124.62 o -4 15 0 366.12 279.88 120.53 o -3 15 0 116.57 65.37 102.15 o -2 15 0 229.60 249.23 126.66 o -1 15 0 75.11 53.12 91.93 o 0 15 0 245.47 312.57 120.53 o 1 15 0 143.75 28.60 91.93 o 2 15 0 64.66 -33.71 62.12 o 3 15 0 34.86 8.34 59.62 o 4 15 0 576.74 830.06 109.53 o 5 15 0 6.71 2.04 96.02 o 6 15 0 20.75 -16.34 96.02 o 7 15 0 119.61 143.00 118.49 o -5 16 0 13.19 -71.50 100.10 o -4 16 0 23.01 -30.64 98.06 o -3 16 0 3.02 -89.89 75.59 o -2 16 0 20.61 -132.79 89.89 o -1 16 0 4.71 12.26 98.06 o 0 16 0 248.75 298.26 126.66 o 1 16 0 129.54 89.89 96.02 o 2 16 0 624.95 563.84 153.22 o 3 16 0 366.68 330.64 127.68 o 4 16 0 173.25 162.15 73.63 o 5 16 0 126.50 218.59 124.62 o 6 16 0 174.64 132.79 116.45 o -3 17 0 0.73 -159.35 106.23 o -2 17 0 3.59 30.64 106.23 o -1 17 0 11.80 -59.24 87.85 o 0 17 0 143.85 326.87 130.75 o 1 17 0 140.85 236.98 132.79 o 2 17 0 25.87 -38.82 98.06 o 3 17 0 0.48 0.00 102.15 o -3 -17 1 271.52 177.73 126.66 o -2 -17 1 246.49 212.46 126.66 o -1 -17 1 556.60 455.57 149.13 o 0 -17 1 361.18 337.08 138.92 o 1 -17 1 137.52 63.33 116.45 o 2 -17 1 108.74 69.46 114.40 o 3 -17 1 55.10 -6.13 114.40 o -6 -16 1 116.24 87.85 112.36 o -5 -16 1 3.11 -65.37 91.93 o -4 -16 1 51.84 -42.02 60.27 o -3 -16 1 62.98 26.56 102.15 o -2 -16 1 29.57 -34.73 79.67 o -1 -16 1 104.05 83.76 104.19 o 0 -16 1 0.80 -87.85 85.80 o 1 -16 1 1.70 -96.02 83.76 o 2 -16 1 49.79 -38.82 100.10 o 3 -16 1 71.11 10.21 91.93 o 4 -16 1 195.78 34.73 112.36 o 5 -16 1 493.22 394.28 151.18 o -7 -15 1 184.55 81.72 122.57 o -6 -15 1 173.27 230.85 126.66 o -5 -15 1 598.25 1016.03 123.20 o -4 -15 1 392.57 415.52 131.77 o -3 -15 1 653.93 725.75 127.68 o -2 -15 1 79.38 -28.60 81.72 o -1 -15 1 83.71 49.03 89.89 o 0 -15 1 153.12 42.90 100.10 o 1 -15 1 385.51 310.52 124.62 o 2 -15 1 663.45 600.62 157.30 o 3 -15 1 346.54 418.80 134.83 o 4 -15 1 152.72 98.06 112.36 o 5 -15 1 57.44 104.19 116.45 o 6 -15 1 97.06 120.53 120.53 o 7 -15 1 27.65 -85.80 96.02 o -8 -14 1 10.97 18.39 110.32 o -7 -14 1 51.10 -4.09 96.02 o -6 -14 1 8.60 -82.90 55.26 o -5 -14 1 23.72 7.75 55.60 o -4 -14 1 0.13 -59.76 51.14 o -3 -14 1 47.17 69.66 57.30 o -2 -14 1 23.13 -3.17 51.37 o -1 -14 1 17.29 38.82 87.85 o 0 -14 1 175.09 87.85 89.89 o 1 -14 1 434.46 469.87 134.83 o 2 -14 1 545.00 363.64 130.75 o 3 -14 1 599.57 582.23 147.09 o 4 -14 1 722.15 643.52 138.92 o 5 -14 1 450.66 443.31 124.62 o 6 -14 1 134.04 114.40 112.36 o 7 -14 1 26.88 -114.40 89.89 o 8 -14 1 7.57 -28.60 100.10 o -9 -13 1 1064.20 1272.73 210.42 o -8 -13 1 244.92 275.79 126.66 o -7 -13 1 2.25 -59.24 79.67 o -6 -13 1 101.73 97.25 65.62 o -5 -13 1 245.10 162.41 65.00 o -4 -13 1 209.14 172.52 63.33 o -3 -13 1 407.94 518.13 81.61 o -2 -13 1 175.83 97.75 56.28 o -1 -13 1 246.31 299.48 112.36 o 0 -13 1 450.04 355.47 112.36 o 1 -13 1 762.89 639.43 145.05 o 2 -13 1 460.33 435.14 126.66 o 3 -13 1 1869.98 1732.39 157.30 o 4 -13 1 987.47 1268.65 187.95 o 5 -13 1 52.83 26.56 85.80 o 6 -13 1 69.29 61.29 96.02 o 7 -13 1 87.97 69.46 104.19 o 8 -13 1 43.26 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