# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' [MnBr2(tptz)]' _shelx_refln_list_code 4 _shelx_F_calc_maximum 309.59 _exptl_crystal_F_000 514.00 _reflns_d_resolution_high 0.7494 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.7095 _cell_length_b 10.4975 _cell_length_c 11.2126 _cell_angle_alpha 110.094 _cell_angle_beta 98.471 _cell_angle_gamma 91.820 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1876.46 1985.48 33.85 o 3 0 0 1779.01 1786.55 45.84 o 4 0 0 12.86 17.52 8.39 o 5 0 0 373.02 293.82 25.36 o 6 0 0 821.54 760.20 42.88 o 7 0 0 410.68 441.47 37.63 o 8 0 0 318.92 258.23 33.29 o 9 0 0 16.33 77.84 23.06 o 10 0 0 616.83 730.69 57.64 o 11 0 0 379.48 321.74 45.84 o -11 1 0 647.20 839.69 62.80 o -10 1 0 36.73 54.60 21.86 o -9 1 0 316.77 333.66 39.84 o -8 1 0 87.60 78.21 23.98 o -7 1 0 26.33 26.47 16.42 o -6 1 0 828.37 711.32 42.61 o -5 1 0 206.24 227.15 24.25 o -4 1 0 2071.20 2405.09 65.02 o -3 1 0 4482.32 4605.18 86.60 o -2 1 0 112.74 119.64 15.95 o -1 1 0 9081.15 9733.77 280.31 o 0 1 0 7425.70 7098.92 72.05 o 1 1 0 143.72 150.87 5.07 o 2 1 0 5691.19 5833.47 50.67 o 3 1 0 2035.96 2079.28 29.80 o 4 1 0 209.54 181.96 18.63 o 5 1 0 1459.73 1485.54 52.11 o 6 1 0 115.93 124.04 21.58 o 7 1 0 229.24 172.18 26.38 o 8 1 0 29.58 27.99 12.16 o 9 1 0 422.33 438.11 31.30 o 10 1 0 772.02 808.69 43.02 o 11 1 0 27.71 50.09 14.40 o -11 2 0 133.68 162.04 37.53 o -10 2 0 250.79 381.90 44.73 o -9 2 0 7.19 14.39 17.61 o -8 2 0 30.57 11.07 16.51 o -7 2 0 396.96 368.52 37.17 o -6 2 0 122.46 113.71 23.61 o -5 2 0 2.54 -0.65 8.95 o -4 2 0 1163.68 1190.68 38.00 o -3 2 0 383.30 359.74 14.29 o -2 2 0 13788.06 14070.51 135.38 o -1 2 0 17159.93 17158.81 227.70 o 0 2 0 16240.00 15231.79 148.77 o 1 2 0 15675.32 15700.84 118.18 o 2 2 0 395.15 374.48 13.53 o 3 2 0 90.31 82.65 6.70 o 4 2 0 2347.02 2385.14 33.60 o 5 2 0 647.59 563.01 15.91 o 6 2 0 5.94 5.18 7.40 o 7 2 0 487.62 451.00 52.15 o 8 2 0 840.31 836.74 38.63 o 9 2 0 787.22 940.38 43.46 o 10 2 0 0.42 31.91 20.38 o 11 2 0 454.66 422.38 49.62 o -11 3 0 97.21 15.31 18.08 o -10 3 0 0.23 -7.65 18.17 o -9 3 0 132.98 95.54 27.48 o -8 3 0 59.63 38.92 21.49 o -7 3 0 1116.58 1031.80 59.95 o -6 3 0 558.62 598.53 43.25 o -5 3 0 293.39 278.61 16.69 o -4 3 0 655.82 639.08 30.89 o -3 3 0 9861.72 10291.62 187.12 o -2 3 0 9676.86 9878.70 157.52 o 0 3 0 12146.18 11186.06 174.67 o 1 3 0 757.72 696.50 21.33 o 2 3 0 4327.41 4396.53 48.77 o 3 3 0 5678.96 6086.48 63.64 o 4 3 0 3136.30 3147.53 43.48 o 5 3 0 173.81 172.64 12.93 o 6 3 0 609.34 632.06 28.54 o 7 3 0 121.54 127.44 17.98 o 8 3 0 445.93 484.30 30.04 o 9 3 0 187.24 237.66 37.81 o 10 3 0 311.61 308.21 42.70 o -11 4 0 15.13 -11.80 16.14 o -10 4 0 69.00 -3.14 17.43 o -9 4 0 40.78 20.66 21.58 o -8 4 0 336.81 402.74 44.91 o -7 4 0 546.91 495.24 44.82 o -6 4 0 1.46 -1.66 12.36 o -5 4 0 184.13 157.14 15.91 o -4 4 0 1919.90 1861.41 43.99 o -3 4 0 5201.40 5071.84 99.51 o -2 4 0 307.53 272.24 25.08 o -1 4 0 4594.22 4141.94 97.76 o 0 4 0 475.83 445.44 30.89 o 1 4 0 946.38 770.75 28.23 o 2 4 0 430.21 388.47 15.46 o 3 4 0 3832.11 3700.50 49.31 o 4 4 0 12.75 17.67 5.54 o 5 4 0 1688.70 1791.46 35.43 o 6 4 0 101.92 113.69 15.59 o 7 4 0 301.02 350.75 24.46 o 8 4 0 167.30 193.30 33.85 o 9 4 0 190.23 203.63 34.58 o 10 4 0 325.55 387.15 46.67 o -10 5 0 10.96 -0.92 13.00 o -9 5 0 369.14 432.16 48.05 o -8 5 0 34.74 88.63 28.77 o -7 5 0 18.69 10.14 17.34 o -6 5 0 79.15 94.25 14.35 o -5 5 0 576.43 615.03 38.32 o -4 5 0 2542.81 2470.86 80.19 o -3 5 0 19.32 12.99 6.99 o -2 5 0 4253.24 4071.85 105.32 o -1 5 0 161.83 123.86 23.33 o 0 5 0 8038.93 8763.99 171.07 o 1 5 0 229.82 258.73 27.81 o 2 5 0 5160.94 5106.71 64.21 o 3 5 0 348.53 307.13 15.29 o 4 5 0 2667.91 2800.48 46.73 o 5 5 0 969.65 921.01 27.02 o 6 5 0 1.41 7.39 8.79 o 7 5 0 0.58 3.23 15.86 o 8 5 0 0.70 -15.31 15.31 o 9 5 0 290.07 317.99 43.62 o 10 5 0 3.88 18.17 17.52 o -8 6 0 23.11 12.82 21.86 o -7 6 0 876.85 866.99 62.90 o -6 6 0 162.78 136.12 18.57 o -5 6 0 19.60 5.46 8.77 o -4 6 0 112.02 91.42 15.41 o -3 6 0 476.94 485.33 32.14 o -2 6 0 1686.23 1745.14 71.93 o -1 6 0 615.54 599.36 43.81 o 0 6 0 202.87 239.04 31.36 o 1 6 0 2509.58 2282.61 86.37 o 2 6 0 507.95 459.75 28.98 o 3 6 0 3572.34 3598.67 75.78 o 4 6 0 971.09 988.82 43.28 o 5 6 0 19.72 13.69 10.05 o 6 6 0 2.14 -2.67 13.65 o 7 6 0 3.20 16.32 19.09 o 8 6 0 287.01 232.68 38.64 o 9 6 0 102.31 114.73 32.55 o -9 7 0 17.17 -0.92 21.86 o -8 7 0 225.45 309.41 45.93 o -7 7 0 287.89 300.37 43.44 o -6 7 0 215.51 198.31 22.50 o -5 7 0 0.13 3.18 9.67 o -4 7 0 282.61 277.64 24.49 o -3 7 0 390.52 400.92 27.02 o -2 7 0 3.40 -11.80 12.17 o -1 7 0 238.67 263.11 35.97 o 0 7 0 1782.47 1879.42 83.19 o 1 7 0 1500.13 1513.76 75.35 o 2 7 0 127.13 136.98 21.76 o 3 7 0 1428.67 1427.93 52.62 o 4 7 0 334.15 285.20 26.67 o 5 7 0 76.53 74.61 26.01 o 6 7 0 0.28 -14.11 14.11 o 7 7 0 6.89 13.93 18.08 o 8 7 0 98.70 111.31 33.38 o 9 7 0 3.35 -10.24 15.22 o -9 8 0 169.00 174.39 42.15 o -8 8 0 277.63 332.28 47.96 o -7 8 0 24.78 7.01 21.40 o -6 8 0 1.81 -9.73 9.73 o -5 8 0 206.31 214.67 25.05 o -4 8 0 16.81 -2.98 10.81 o -3 8 0 30.32 32.11 13.22 o -2 8 0 209.33 242.82 38.55 o -1 8 0 150.02 190.44 38.00 o 0 8 0 598.44 665.21 56.90 o 1 8 0 584.69 660.23 57.92 o 2 8 0 2176.01 2389.98 75.02 o 3 8 0 1083.98 1099.64 51.61 o 4 8 0 112.60 130.96 23.77 o 5 8 0 16.48 33.86 15.22 o 6 8 0 12.98 32.09 22.50 o 7 8 0 81.87 68.61 24.99 o 8 8 0 10.88 12.91 21.30 o -9 9 0 79.09 137.69 37.90 o -8 9 0 15.10 -18.91 18.91 o -7 9 0 3.32 -15.86 19.27 o -6 9 0 13.07 0.29 15.08 o -5 9 0 81.54 80.57 21.81 o -4 9 0 163.20 153.38 23.70 o -3 9 0 2.48 2.47 11.60 o -2 9 0 11.12 4.98 22.50 o -1 9 0 117.88 112.51 32.55 o 0 9 0 58.71 54.04 26.47 o 1 9 0 2129.87 2349.02 109.47 o 2 9 0 431.77 475.14 54.69 o 3 9 0 196.40 205.69 63.77 o 4 9 0 228.25 183.21 27.97 o 5 9 0 20.67 35.49 17.00 o 6 9 0 70.78 86.41 28.50 o 7 9 0 29.65 92.41 27.94 o -8 10 0 122.23 138.80 40.02 o -7 10 0 6.56 -17.43 17.43 o -6 10 0 0.76 -1.08 12.66 o -5 10 0 35.72 60.11 17.67 o -4 10 0 0.53 6.70 13.85 o -3 10 0 40.21 47.52 15.88 o -2 10 0 189.36 219.58 45.10 o -1 10 0 1.25 24.25 23.52 o 0 10 0 404.68 560.17 60.41 o 1 10 0 534.47 546.33 59.02 o 2 10 0 155.77 198.93 44.36 o 3 10 0 80.31 68.24 59.30 o 4 10 0 35.90 36.48 33.66 o 5 10 0 19.39 3.50 25.45 o 6 10 0 48.10 87.43 32.19 o -7 11 0 6.43 22.59 22.23 o -6 11 0 36.65 71.84 19.03 o -5 11 0 81.59 101.30 21.52 o -4 11 0 2.90 8.91 13.33 o -3 11 0 12.50 14.61 13.26 o -2 11 0 6.30 -3.87 19.92 o -1 11 0 164.75 186.29 43.44 o 0 11 0 228.36 236.92 49.62 o 1 11 0 79.69 17.89 29.60 o 2 11 0 119.05 125.88 38.92 o 3 11 0 2.88 -19.18 19.18 o 4 11 0 7.42 12.29 17.93 o 5 11 0 117.19 187.73 29.44 o -5 12 0 15.61 61.88 25.55 o -4 12 0 26.79 25.44 16.03 o -3 12 0 1.73 15.49 14.02 o -2 12 0 58.08 15.86 13.10 o -1 12 0 128.64 -5.16 12.17 o 0 12 0 0.22 19.09 27.57 o 1 12 0 137.02 153.55 44.82 o 2 12 0 87.78 82.45 34.58 o 3 12 0 1.39 -18.17 20.75 o -2 13 0 109.79 0.37 17.06 o -1 13 0 1.49 6.27 19.64 o 0 13 0 66.54 77.65 34.86 o -2 -13 1 2.46 10.97 24.35 o -1 -13 1 30.07 14.85 34.40 o 0 -13 1 60.56 109.65 41.78 o 1 -13 1 11.16 10.42 20.29 o 2 -13 1 6.59 13.19 17.98 o 3 -13 1 19.79 4.80 18.26 o -4 -12 1 40.40 32.46 24.72 o -3 -12 1 0.65 12.91 23.52 o -2 -12 1 1.00 -22.50 22.50 o -1 -12 1 80.15 153.00 42.79 o 0 -12 1 32.51 16.14 28.96 o 1 -12 1 10.73 1.66 19.18 o 2 -12 1 0.18 -6.55 21.12 o 3 -12 1 66.98 116.73 94.53 o 4 -12 1 179.76 233.67 27.32 o 5 -12 1 0.18 3.59 22.36 o -5 -11 1 108.05 208.55 50.58 o -4 -11 1 0.41 12.07 38.09 o -3 -11 1 0.71 -18.26 18.26 o -2 -11 1 167.58 207.23 45.84 o -1 -11 1 111.92 77.28 35.14 o 0 -11 1 0.96 12.45 26.19 o 1 -11 1 92.38 76.18 33.75 o 2 -11 1 46.19 102.00 34.86 o 3 -11 1 260.06 308.83 30.62 o 4 -11 1 87.39 122.79 22.84 o 5 -11 1 31.14 38.41 16.88 o 6 -11 1 97.48 116.29 33.48 o 7 -11 1 21.41 -17.80 21.86 o -7 -10 1 1.47 -15.49 19.18 o -6 -10 1 176.68 235.35 41.78 o -5 -10 1 2.73 -9.57 13.06 o -4 -10 1 97.19 121.52 25.12 o -3 -10 1 283.31 411.78 53.12 o -2 -10 1 168.93 235.63 48.23 o -1 -10 1 0.45 7.93 24.44 o 0 -10 1 224.29 188.23 43.25 o 1 -10 1 236.25 197.17 43.71 o 2 -10 1 190.09 234.52 46.30 o 3 -10 1 67.87 76.82 29.88 o 4 -10 1 37.37 28.62 15.53 o 5 -10 1 382.05 373.15 34.17 o 6 -10 1 20.46 56.31 18.62 o 7 -10 1 2.49 42.79 25.91 o 8 -10 1 45.52 48.79 28.50 o -7 -9 1 321.67 352.11 45.84 o -6 -9 1 80.13 123.12 34.12 o -5 -9 1 9.87 17.90 19.69 o -4 -9 1 379.84 329.89 33.43 o -3 -9 1 1195.60 1252.28 98.49 o -2 -9 1 5.38 -2.12 24.44 o -1 -9 1 535.28 608.77 58.75 o 0 -9 1 598.16 531.85 55.33 o 1 -9 1 271.46 313.19 43.53 o 2 -9 1 801.77 808.80 62.90 o 3 -9 1 213.70 271.23 43.53 o 4 -9 1 1401.97 1582.08 93.56 o 5 -9 1 6.35 -3.87 11.48 o 6 -9 1 85.70 84.80 19.15 o 7 -9 1 24.87 10.05 23.33 o 8 -9 1 25.75 13.28 22.69 o 9 -9 1 30.02 30.53 25.18 o -8 -8 1 93.73 161.39 35.87 o -7 -8 1 43.19 70.27 27.02 o -6 -8 1 185.22 176.52 36.24 o -5 -8 1 141.80 127.66 22.16 o -4 -8 1 3609.67 3730.14 104.54 o -3 -8 1 408.11 381.14 73.18 o -2 -8 1 643.93 674.43 54.27 o -1 -8 1 677.42 747.66 60.68 o 0 -8 1 237.95 231.30 37.72 o 1 -8 1 122.44 161.21 34.40 o 2 -8 1 0.34 5.26 17.80 o 3 -8 1 39.77 33.20 20.57 o 4 -8 1 2662.98 2806.42 73.33 o 5 -8 1 34.37 46.85 14.59 o 6 -8 1 5.77 -2.11 13.29 o 7 -8 1 365.33 390.75 50.17 o 8 -8 1 15.93 -8.85 23.61 o 9 -8 1 415.05 525.86 58.93 o -9 -7 1 28.21 9.50 16.78 o -8 -7 1 332.84 387.34 46.20 o -7 -7 1 10.30 12.36 15.03 o -6 -7 1 88.21 87.80 28.04 o -5 -7 1 730.66 704.83 57.59 o -4 -7 1 468.62 456.99 22.93 o -3 -7 1 1180.23 1159.11 34.37 o -2 -7 1 3015.82 3036.45 113.20 o -1 -7 1 79.50 62.53 23.42 o 0 -7 1 75.30 79.59 24.35 o 1 -7 1 19.88 5.99 14.57 o 2 -7 1 946.41 1040.93 62.62 o 3 -7 1 308.49 310.98 36.70 o 4 -7 1 98.93 102.89 17.29 o 5 -7 1 241.45 243.76 24.24 o 6 -7 1 539.60 546.47 32.61 o 7 -7 1 69.48 14.39 23.06 o 8 -7 1 669.24 593.46 58.56 o 10 -7 1 1.82 9.31 19.09 o -9 -6 1 125.90 134.37 33.75 o -8 -6 1 0.86 7.47 17.89 o -7 -6 1 35.58 32.65 19.74 o -6 -6 1 901.35 830.69 47.38 o -5 -6 1 2066.21 2029.26 43.78 o -4 -6 1 841.19 850.68 27.56 o -3 -6 1 5779.97 5932.77 76.83 o -2 -6 1 707.73 647.35 23.39 o -1 -6 1 52.42 41.63 12.53 o 0 -6 1 63.06 48.05 18.26 o 1 -6 1 437.08 433.27 39.66 o 2 -6 1 743.72 673.23 46.20 o 3 -6 1 51.57 33.38 15.68 o 4 -6 1 419.48 406.88 26.12 o 5 -6 1 392.53 415.00 30.16 o 6 -6 1 364.00 362.92 25.45 o 7 -6 1 1478.89 1533.68 81.43 o 8 -6 1 1169.30 1188.39 75.72 o 9 -6 1 42.88 10.79 20.10 o 10 -6 1 77.35 11.71 12.91 o -10 -5 1 39.30 -1.66 17.61 o -9 -5 1 0.11 -14.48 15.49 o -8 -5 1 72.73 71.84 24.81 o -7 -5 1 384.12 377.64 62.25 o -6 -5 1 2718.45 2710.51 63.02 o -5 -5 1 114.48 104.73 11.97 o -4 -5 1 6704.60 6878.74 80.87 o -3 -5 1 1229.18 1219.22 43.55 o -2 -5 1 891.22 891.61 24.93 o -1 -5 1 12.13 16.55 11.22 o 0 -5 1 271.60 287.00 33.02 o 1 -5 1 2023.66 2125.29 76.18 o 2 -5 1 229.65 234.89 27.76 o 3 -5 1 73.32 63.36 16.60 o 4 -5 1 250.74 185.19 17.92 o 5 -5 1 351.40 348.12 28.27 o 6 -5 1 681.32 784.27 53.77 o 7 -5 1 3872.24 3857.43 124.41 o 8 -5 1 47.33 66.59 25.36 o 9 -5 1 694.02 798.01 64.19 o 10 -5 1 79.08 2.95 13.65 o -10 -4 1 72.64 119.89 30.71 o -9 -4 1 9.87 19.64 18.35 o -8 -4 1 33.61 36.12 12.54 o -7 -4 1 1639.12 1650.48 110.30 o -6 -4 1 18.32 31.87 10.52 o -5 -4 1 3806.98 3739.71 53.90 o -4 -4 1 959.48 779.57 22.41 o -3 -4 1 673.11 679.20 19.85 o -2 -4 1 558.71 479.75 16.29 o -1 -4 1 709.65 702.93 24.26 o 0 -4 1 162.70 122.10 17.98 o 1 -4 1 4135.90 4342.34 97.30 o 2 -4 1 166.90 145.44 19.55 o 3 -4 1 357.52 408.00 30.62 o 4 -4 1 1613.55 1545.29 62.16 o 5 -4 1 1367.25 1410.27 39.34 o 6 -4 1 4052.95 4223.19 119.34 o 7 -4 1 84.97 83.46 25.73 o 8 -4 1 1232.47 1223.16 72.30 o 9 -4 1 306.42 324.72 41.41 o 10 -4 1 105.11 40.12 22.50 o 11 -4 1 2.92 15.86 23.15 o -11 -3 1 0.84 -3.32 16.51 o -10 -3 1 7.84 10.30 11.54 o -9 -3 1 0.00 -10.32 10.32 o -8 -3 1 218.88 210.64 22.43 o -7 -3 1 29.88 42.70 12.27 o -6 -3 1 3931.01 4059.66 74.57 o -5 -3 1 6258.09 6436.05 70.51 o -4 -3 1 6081.23 6504.70 92.28 o -3 -3 1 4908.40 4753.43 54.00 o -2 -3 1 497.62 503.37 14.54 o -1 -3 1 531.05 513.60 17.30 o 0 -3 1 965.93 950.18 35.32 o 1 -3 1 619.82 622.97 28.31 o 2 -3 1 5.64 5.72 5.63 o 3 -3 1 37.72 31.49 6.45 o 4 -3 1 85.49 94.27 10.51 o 5 -3 1 6652.41 6746.00 89.77 o 6 -3 1 847.43 869.39 51.09 o 7 -3 1 2297.78 2254.86 87.43 o 8 -3 1 1070.11 996.20 62.90 o 9 -3 1 85.35 105.04 28.22 o 10 -3 1 120.50 163.88 36.15 o 11 -3 1 12.68 -18.44 18.44 o -11 -2 1 105.18 100.63 18.40 o -10 -2 1 83.24 89.82 30.39 o -9 -2 1 161.85 194.08 37.07 o -8 -2 1 3.79 -1.41 9.62 o -7 -2 1 1961.49 1969.46 53.80 o -6 -2 1 6125.89 6218.51 95.07 o -5 -2 1 289.18 246.87 17.59 o -4 -2 1 3014.88 2929.93 43.58 o -3 -2 1 12.07 8.17 3.18 o -2 -2 1 1190.43 1227.27 20.03 o -1 -2 1 1249.96 1243.55 18.78 o 0 -2 1 735.73 706.43 24.35 o 1 -2 1 817.31 829.55 26.38 o 2 -2 1 56.23 52.66 7.93 o 3 -2 1 7.15 2.63 4.12 o 4 -2 1 4463.81 4233.53 57.73 o 5 -2 1 1767.79 1778.81 62.99 o 6 -2 1 1498.35 1453.35 62.25 o 7 -2 1 3392.27 3456.81 104.67 o 8 -2 1 219.78 227.98 33.94 o 9 -2 1 170.44 161.48 33.02 o 10 -2 1 160.95 228.71 36.70 o 11 -2 1 175.70 259.70 41.59 o -11 -1 1 40.68 113.64 39.79 o -10 -1 1 31.11 38.75 14.64 o -9 -1 1 28.99 24.61 12.67 o -8 -1 1 214.28 223.55 33.02 o -7 -1 1 1092.11 1038.25 55.06 o -6 -1 1 24.78 17.98 13.10 o -5 -1 1 6573.83 6479.80 126.16 o -4 -1 1 4.35 2.95 6.64 o -3 -1 1 5967.36 6076.60 102.55 o -2 -1 1 60.34 56.39 5.47 o -1 -1 1 824.55 842.83 11.43 o 0 -1 1 92.56 92.26 10.24 o 1 -1 1 352.73 335.51 12.73 o 2 -1 1 687.01 684.39 25.68 o 3 -1 1 2581.29 2693.29 61.61 o 4 -1 1 2975.27 3093.08 74.24 o 5 -1 1 2399.07 2486.34 72.67 o 6 -1 1 2035.01 2022.55 70.00 o 7 -1 1 958.49 806.22 49.16 o 8 -1 1 283.52 240.61 33.57 o 9 -1 1 290.19 252.05 35.69 o 10 -1 1 512.21 533.42 50.26 o 11 -1 1 13.99 -12.63 12.63 o -11 0 1 24.72 13.88 11.19 o -10 0 1 32.58 38.00 19.27 o -9 0 1 858.56 866.99 59.02 o -8 0 1 767.77 817.28 54.32 o -7 0 1 4.49 -3.04 11.71 o -6 0 1 4362.10 4316.79 107.16 o -5 0 1 1347.36 1280.71 50.72 o -4 0 1 822.39 716.58 33.75 o -3 0 1 277.09 278.15 18.81 o -2 0 1 15956.95 16955.74 214.79 o -1 0 1 449.77 476.79 16.55 o 0 0 1 589.81 571.97 12.45 o 1 0 1 2134.47 2234.55 26.23 o 2 0 1 2416.12 2534.23 31.92 o 3 0 1 1847.63 1961.29 35.37 o 4 0 1 807.39 698.59 31.63 o 5 0 1 6098.40 6174.08 119.24 o 6 0 1 654.80 629.70 37.72 o 7 0 1 7454.57 7280.58 153.46 o 8 0 1 1.23 -0.83 11.80 o 9 0 1 1486.21 1525.84 74.79 o 10 0 1 6.21 11.67 12.13 o 11 0 1 332.59 401.36 48.69 o -11 1 1 19.73 42.42 22.78 o -10 1 1 249.71 324.53 41.59 o -9 1 1 628.35 582.30 50.91 o -8 1 1 117.95 120.17 27.85 o -7 1 1 1307.97 1260.42 62.16 o -6 1 1 1154.87 1106.50 52.75 o -5 1 1 2456.12 2410.17 72.21 o -4 1 1 2146.50 2030.48 59.30 o -3 1 1 14595.85 15235.90 141.37 o -2 1 1 3654.17 3808.83 45.39 o -1 1 1 2166.89 2143.55 40.02 o 0 1 1 3280.92 3391.34 38.75 o 1 1 1 205.32 194.67 5.41 o 2 1 1 892.07 908.78 15.29 o 3 1 1 543.81 518.91 20.99 o 4 1 1 2561.63 2576.30 33.99 o 5 1 1 1440.89 1580.29 26.66 o 6 1 1 548.97 551.02 39.79 o 7 1 1 17.29 9.08 9.21 o 8 1 1 674.87 682.48 34.92 o 9 1 1 55.39 53.48 15.30 o 10 1 1 929.63 944.64 68.61 o 11 1 1 247.29 291.15 43.16 o -11 2 1 35.30 -11.44 14.39 o -10 2 1 64.57 66.40 25.55 o -9 2 1 276.74 217.28 39.01 o -8 2 1 443.68 466.84 45.10 o -7 2 1 1440.82 1397.00 66.59 o -6 2 1 97.46 73.69 19.37 o -5 2 1 815.48 712.70 40.67 o -4 2 1 31.73 20.47 5.33 o -3 2 1 4920.88 4923.77 109.05 o -2 2 1 720.82 650.93 18.57 o -1 2 1 12436.98 12844.84 167.57 o 0 2 1 292.55 283.71 17.43 o 1 2 1 1.41 9.07 2.38 o 2 2 1 34.75 40.06 4.53 o 3 2 1 3102.47 3425.62 41.57 o 4 2 1 571.53 478.03 14.89 o 5 2 1 702.62 700.59 18.92 o 6 2 1 176.23 194.71 17.85 o 7 2 1 2345.93 2319.50 58.36 o 8 2 1 615.25 573.52 38.36 o 9 2 1 1112.36 1040.65 69.08 o 10 2 1 444.50 410.21 48.60 o -11 3 1 98.76 -13.56 13.56 o -10 3 1 1.30 -1.94 17.15 o -9 3 1 15.16 11.53 19.55 o -8 3 1 192.60 200.12 35.69 o -7 3 1 31.93 36.15 18.17 o -6 3 1 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