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Acta Cryst. (2012). E68, m40  [ doi:10.1107/S1600536811052524 ]

Bis[[mu]3-N'-oxidopyridine-2-carboximidamidato(2-)]bis[[mu]2-N'-oxidopyridine-2-carboximidamidato(1-)]tetrapyridinetetranickel(II) dinitrate

X.-H. Deng and J.-W. Ran

Online 10 December 2011


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Alert level C PLAT230_ALERT_2_C Hirshfeld Test Diff for N4 -- C12 .. 5.8 su PLAT230_ALERT_2_C Hirshfeld Test Diff for N5 -- C17 .. 6.0 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ni2 -- N7 .. 6.8 su PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of N9 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 24 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 3 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 = 3 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 8 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 56 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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