Acta Cryst. (2012). E68, m54  [ doi:10.1107/S1600536811053335 ]

trans-Bis(acridine-N)dichloridopalladium(II)

K. Ha

Online 17 December 2011

Key indicators

• Single-crystal X-ray study
• T = 200 K
• Mean (C-C) = 0.009 Å
• R factor = 0.059
• wR factor = 0.107
• Data-to-parameter ratio = 15.0

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT973_ALERT_2_B Large Calcd. Positive Residual Density on    Pd1       1.98 eA-3 

Alert level C
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......      0.977      
PLAT342_ALERT_3_C Low Bond Precision on  C-C Bonds ...............     0.0091 Ang  
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         18      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         31      
PLAT925_ALERT_1_C The Reported and Calculated Rho(max) Differ by .       1.15 eA-3 

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal ..........    0.00400 Deg. 

   0 ALERT level A = Most likely a serious problem - resolve or explain
   1 ALERT level B = A potentially serious problem, consider carefully
   5 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   2 ALERT level G = General information/check it is not something unexpected

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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