Acta Cryst. (2012). E68, m11  [ doi:10.1107/S1600536811051476 ]

Bis[2-(1-iminoethyl)phenolato-²N,O]nickel(II)

N. Wang

Online 3 December 2011

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.010 Å
• R factor = 0.062
• wR factor = 0.146
• Data-to-parameter ratio = 14.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT125_ALERT_4_C No '_symmetry_space_group_name_Hall' Given .....          ?
PLAT341_ALERT_3_C Low Bond Precision on  C-C Bonds ...............     0.0097 Ang  
PLAT420_ALERT_2_C D-H Without Acceptor       N2     -   H2     ...          ?      
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .         37 A   3 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         41      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         17      

Alert level G
PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite          6      
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal ..........    0.00300 Deg. 
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          3      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   6 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   4 ALERT level G = General information/check it is not something unexpected

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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