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Acta Cryst. (2012). E68, m58  [ doi:10.1107/S1600536811053475 ]

Bis(O-ethyl dithiocarbonato-[kappa]2S,S')bis(pyridine-3-carbonitrile-[kappa]N1)nickel(II)

S. Kapoor, R. Kour, R. Sachar, R. Kant, V. K. Gupta and K. Kapoor

Online 17 December 2011


Key indicators

checkCIF/PLATON results

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Alert level C PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ni1 -- S1 .. 5.3 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ni1 -- S2 .. 9.0 su PLAT480_ALERT_4_C Long H...A H-Bond Reported H10C .. N2 .. 2.65 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 5
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C3 - C7 ... 1.44 Ang. PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 78 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
checkCIF publication errors
Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
Author Response: As the reported work is a part of collaboration between two departments, hence the number of authors are greater than 5. Synthesis has been carried out by Sanjay Kapoor and Renu Sachar while Ramandeep, Kamini, Vivek and Rajnikant are responsible for the single crystal growth, data collection, refinement of the structure, structure completion in the form of paper and for bearing the financial load for the publication.

1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing

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