Acta Cryst. (2012). E68, m79-m80  [ doi:10.1107/S160053681105392X ]

Di-n-butylbis(N-ethyl-N-phenyldithiocarbamato-S)tin(IV)

N. F. Kamaludin, I. Baba, N. Awang, M. I. Mohamed Tahir and E. R. T. Tiekink

Online 23 December 2011

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.005 Å
• Disorder in main residue
• R factor = 0.030
• wR factor = 0.074
• Data-to-parameter ratio = 19.6

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Sn     --  S2      ..       15.3 su   
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Sn     --  S4      ..       17.5 su   

Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...        3.8 Ratio
PLAT222_ALERT_3_C Large Non-Solvent    H    Uiso(max)/Uiso(min) ..        4.2 Ratio
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C25     
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          4      

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large.       5.92      
PLAT301_ALERT_3_G Note: Main Residue  Disorder ...................          6 Perc.

   0 ALERT level A = Most likely a serious problem - resolve or explain
   2 ALERT level B = A potentially serious problem, consider carefully
   4 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   3 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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