[HTML version][PDF version][Article Abstract][CIF][3d view][Structure Factors][Supplementary Material][Issue contents]  [Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m83  [ doi:10.1107/S1600536811054274 ]

Bis(4-fluorobenzyl)bis(4-phenyl-5-sulfanylidene-4,5-dihydro-1,3,4-thiodiazole-2-thiolato)tin(IV)

L. Li, S. Zeng and N. Yan

Online 23 December 2011


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1
Alert level C PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 43 Perc. PLAT048_ALERT_1_C MoietyFormula Not Given ........................ ? PLAT125_ALERT_4_C No '_symmetry_space_group_name_Hall' Given ..... ? PLAT234_ALERT_4_C Large Hirshfeld Difference C4 -- C5 .. 0.17 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C25 -- C26 .. 0.16 Ang. PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for S1 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for S4 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C13 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C17 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C28 PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C3 -C8 1.36 Ang. PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C11 -C16 1.36 Ang. PLAT334_ALERT_2_C Small Average Benzene C-C Dist. C18 -C23 1.37 Ang. PLAT334_ALERT_2_C Small Average Benzene C-C Dist. C25 -C30 1.37 Ang. PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0146 Ang PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 58 PLAT973_ALERT_2_C Large Calcd. Positive Residual Density on Sn1 1.26 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 6
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 18 ALERT level C = Check. Ensure it is not caused by an omission or oversight 3 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 12 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster