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Acta Cryst. (2012). E68, m19  [ doi:10.1107/S1600536811051853 ]

catena-Poly[1-[(2-fluorobenzylidene)amino]quinolinium [plumbate(II)-tri-[mu]-iodido]]

H.-R. Zhao

Online 7 December 2011


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C RINTA01_ALERT_3_C The value of Rint is greater than 0.12 Rint given 0.156 PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 43 Perc. PLAT213_ALERT_2_C Atom C7 has ADP max/min Ratio ..... 3.2 prola PLAT234_ALERT_4_C Large Hirshfeld Difference C3 -- C4 .. 0.20 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C15 -- C16 .. 0.20 Ang. PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C6 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.4 PLAT334_ALERT_2_C Small Average Benzene C-C Dist. C11 -C16 1.37 Ang. PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0199 Ang PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2
Alert level G PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT194_ALERT_1_G Missing _cell_measurement_reflns_used datum .... ? PLAT195_ALERT_1_G Missing _cell_measurement_theta_max datum .... ? PLAT196_ALERT_1_G Missing _cell_measurement_theta_min datum .... ? PLAT233_ALERT_4_G Hirshfeld (M-X Solvent) Pb1 -- I3 .. 6.3 su PLAT233_ALERT_4_G Hirshfeld (M-X Solvent) Pb1 -- I2_b .. 11.2 su PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.11 Ratio PLAT794_ALERT_5_G Note: Tentative Bond Valency for Pb1 (II) 2.07 PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... !
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 10 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 4 ALERT type 5 Informative message, check

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