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Acta Cryst. (2012). E68, m33-m34  [ doi:10.1107/S160053681105207X ]

Bis(tetraphenylphosphonium) bis[N-(trifluoromethylsulfonyl)dithiocarbimato(2-)-[kappa]2S,S']zincate(II)

P. S. Pinto, M. M. M. Rubinger, S. Guilardi, D. A. Paixão and M. R. L. Oliveira

Online 10 December 2011


Key indicators

checkCIF/PLATON results

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Alert level B Crystal system given = monoclinic PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 15
Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.979 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C7 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C21 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for S1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C4 PLAT480_ALERT_4_C Long H...A H-Bond Reported H9 .. O1 .. 2.68 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H31 .. O4 .. 2.62 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 80 PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 157 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 39
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT432_ALERT_2_G Short Inter X...Y Contact S2 .. C12 .. 3.29 Ang. PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 3 C4 F6 N2 O4 S6 Zn
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 11 ALERT level C = Check. Ensure it is not caused by an omission or oversight 3 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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