# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1 in space group P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 296.84 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.7896 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.6973 _cell_length_b 12.2804 _cell_length_c 22.8523 _cell_angle_alpha 90.588 _cell_angle_beta 101.573 _cell_angle_gamma 110.687 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4443.73 4457.56 44.80 o 2 0 0 27836.95 29211.37 328.13 o 3 0 0 11591.50 11252.10 113.29 o 4 0 0 7396.08 7446.81 84.87 o 5 0 0 5564.17 5808.48 75.15 o 6 0 0 169.17 194.41 9.85 o 7 0 0 9931.77 10044.03 151.99 o 8 0 0 95.43 111.83 16.76 o 9 0 0 1002.90 966.01 35.30 o 10 0 0 595.03 677.70 36.27 o 11 0 0 128.35 110.31 21.25 o -11 1 0 66.59 50.48 17.96 o -10 1 0 1239.03 1272.05 48.49 o -9 1 0 4132.50 4251.57 93.76 o -8 1 0 0.28 2.31 7.62 o -7 1 0 1904.09 2017.80 34.48 o -6 1 0 2183.64 2101.87 33.49 o -5 1 0 1418.25 1309.10 21.01 o -4 1 0 160.90 250.30 7.10 o -3 1 0 2220.85 2271.27 24.18 o -2 1 0 15368.75 15180.09 107.61 o -1 1 0 188.20 236.38 7.18 o 1 1 0 10629.47 9908.88 107.13 o 2 1 0 3381.35 3138.03 31.41 o 3 1 0 677.99 807.78 17.30 o 4 1 0 8261.96 8634.65 109.59 o 5 1 0 14592.04 14113.48 218.73 o 6 1 0 13.47 36.36 6.27 o 7 1 0 12.57 9.67 7.70 o 8 1 0 2177.50 2178.98 68.77 o 9 1 0 1583.98 1460.96 45.69 o 10 1 0 253.77 236.00 23.14 o -11 2 0 1178.14 1294.43 53.07 o -10 2 0 265.54 277.68 27.71 o -9 2 0 3195.34 3048.40 74.05 o -8 2 0 876.17 945.25 33.35 o -7 2 0 3636.24 3566.97 44.35 o -6 2 0 171.29 213.35 8.53 o -5 2 0 1294.46 1275.07 19.20 o -4 2 0 10166.90 9951.20 83.49 o -3 2 0 78.84 81.45 2.76 o -2 2 0 9310.93 9551.36 106.56 o -1 2 0 2501.63 2578.87 26.34 o 0 2 0 17198.86 17224.47 160.86 o 1 2 0 647.69 610.27 10.02 o 2 2 0 837.75 752.99 17.63 o 3 2 0 6679.91 6310.40 139.21 o 4 2 0 506.31 443.22 10.24 o 5 2 0 6873.61 7280.75 86.61 o 6 2 0 842.43 796.91 19.08 o 7 2 0 1060.05 1128.59 36.47 o 8 2 0 435.70 432.22 24.38 o 9 2 0 708.96 652.60 31.68 o 10 2 0 2600.97 2724.57 79.72 o -11 3 0 989.32 915.07 43.45 o -10 3 0 0.47 10.68 9.55 o -9 3 0 232.37 254.80 14.54 o -8 3 0 1276.19 1309.52 24.09 o -7 3 0 2200.00 2249.73 30.66 o -6 3 0 5651.62 5673.16 63.65 o -5 3 0 237.03 263.49 7.49 o -4 3 0 8014.90 7986.72 73.37 o -3 3 0 6545.32 6914.40 74.11 o -2 3 0 1199.93 1343.27 14.32 o -1 3 0 4385.44 4805.95 55.22 o 0 3 0 8897.97 9148.81 164.52 o 1 3 0 12203.68 11975.26 240.13 o 2 3 0 718.57 670.04 14.26 o 3 3 0 4625.11 4506.30 115.51 o 4 3 0 1188.55 1138.39 40.20 o 5 3 0 1940.67 2026.89 49.11 o 6 3 0 3.93 5.66 9.08 o 7 3 0 2272.03 2165.85 54.54 o 8 3 0 2892.49 2888.06 67.71 o 9 3 0 15.67 22.92 13.28 o 10 3 0 601.93 591.22 33.25 o -11 4 0 35.69 43.56 15.69 o -10 4 0 826.47 824.64 39.34 o -9 4 0 1133.12 1087.29 27.43 o -8 4 0 1118.65 1220.22 26.95 o -7 4 0 1287.85 1290.10 21.74 o -6 4 0 12608.26 12766.30 110.41 o -5 4 0 526.20 528.01 14.38 o -4 4 0 1920.40 2061.98 28.75 o -3 4 0 137.44 142.04 4.93 o -2 4 0 54812.11 54782.13 603.44 o -1 4 0 2990.68 2939.77 47.07 o 0 4 0 431.05 422.17 11.37 o 1 4 0 31261.67 30767.12 330.27 o 2 4 0 58.94 40.21 4.99 o 3 4 0 2953.00 3289.42 50.66 o 4 4 0 330.75 330.34 19.26 o 5 4 0 7671.17 7269.78 122.17 o 6 4 0 1970.79 1838.19 54.38 o 7 4 0 104.67 96.05 13.91 o 8 4 0 1521.51 1654.76 51.67 o 9 4 0 85.44 109.00 22.74 o -12 5 0 2.94 8.83 17.59 o -11 5 0 479.71 483.29 23.06 o -10 5 0 11.68 12.40 8.42 o -9 5 0 1431.61 1572.51 34.05 o -8 5 0 12205.34 12699.92 137.41 o -7 5 0 35.83 47.06 5.27 o -6 5 0 11.07 15.87 4.82 o -5 5 0 4186.97 4328.26 53.26 o -4 5 0 10624.63 10582.13 101.22 o -3 5 0 7575.67 8058.19 91.92 o -2 5 0 4216.68 4316.87 49.22 o -1 5 0 21651.81 21897.21 256.86 o 0 5 0 2509.48 2516.56 39.87 o 1 5 0 261.55 218.32 10.75 o 2 5 0 3447.54 3282.37 61.11 o 3 5 0 8515.63 8177.21 126.25 o 4 5 0 5855.64 5683.28 101.84 o 5 5 0 15.26 27.82 10.54 o 6 5 0 513.64 501.94 41.75 o 7 5 0 32.96 35.74 11.92 o 8 5 0 181.73 173.08 22.31 o 9 5 0 110.16 142.36 18.14 o -12 6 0 20.01 -17.10 20.51 o -11 6 0 709.21 616.91 28.91 o -10 6 0 2072.48 2079.52 64.02 o -9 6 0 457.08 510.89 20.38 o -8 6 0 1355.62 1355.46 27.02 o -7 6 0 368.31 352.65 13.66 o -6 6 0 9131.51 8869.78 122.30 o -5 6 0 53.35 66.94 6.13 o -4 6 0 4511.08 4764.49 65.12 o -3 6 0 19221.11 19806.31 180.37 o -2 6 0 1230.92 1242.29 16.14 o -1 6 0 54.16 46.71 4.44 o 0 6 0 3645.92 3447.65 49.37 o 1 6 0 11926.77 11785.70 162.00 o 2 6 0 1477.11 1390.55 27.81 o 3 6 0 24.15 19.51 7.70 o 4 6 0 9031.25 9023.43 291.88 o 5 6 0 627.98 597.21 31.17 o 6 6 0 362.04 322.49 26.60 o 7 6 0 144.55 152.42 20.72 o 8 6 0 1829.99 1838.56 80.10 o -11 7 0 41.18 28.47 14.18 o -10 7 0 1845.33 1843.09 59.49 o -9 7 0 259.94 234.74 15.73 o -8 7 0 2694.19 2766.03 55.95 o -7 7 0 753.32 679.36 18.87 o -6 7 0 166.00 170.42 9.75 o -5 7 0 16630.63 17006.71 174.96 o -4 7 0 1711.08 1764.24 26.97 o -3 7 0 5.53 27.00 5.49 o -2 7 0 12.76 40.57 4.44 o -1 7 0 2470.29 2277.84 42.83 o 0 7 0 469.21 490.59 20.01 o 1 7 0 1240.25 1239.46 29.68 o 2 7 0 15263.25 14988.59 194.33 o 3 7 0 616.75 583.86 24.78 o 4 7 0 397.25 392.32 25.19 o 5 7 0 98.48 93.37 17.12 o 6 7 0 1307.47 1273.08 56.65 o 7 7 0 82.78 74.77 16.24 o 8 7 0 722.39 768.02 44.09 o -11 8 0 0.43 13.19 11.68 o -10 8 0 87.09 106.26 24.93 o -9 8 0 874.65 840.69 33.76 o -8 8 0 2988.74 3145.06 52.21 o -7 8 0 6063.14 6098.84 78.51 o -6 8 0 906.29 885.35 29.15 o -5 8 0 2528.45 2536.93 45.39 o -4 8 0 119.71 122.44 9.21 o -3 8 0 3312.36 3438.65 42.82 o -2 8 0 11.20 11.05 3.44 o -1 8 0 14088.97 14007.78 153.33 o 0 8 0 6791.35 6667.50 84.50 o 1 8 0 301.99 338.48 14.37 o 2 8 0 335.57 311.75 18.10 o 3 8 0 123.17 135.05 13.27 o 4 8 0 3454.00 3564.08 84.32 o 5 8 0 0.51 -2.23 11.49 o 6 8 0 1372.29 1440.56 56.43 o 7 8 0 2019.56 2116.67 72.70 o -11 9 0 5.95 7.65 13.97 o -10 9 0 2336.00 2472.06 71.91 o -9 9 0 842.27 883.81 35.06 o -8 9 0 45.75 41.28 11.01 o -7 9 0 871.37 845.47 26.24 o -6 9 0 243.55 250.22 14.05 o -5 9 0 730.49 715.34 19.79 o -4 9 0 2446.23 2466.83 40.19 o -3 9 0 9058.74 9222.72 144.37 o -2 9 0 719.33 756.77 21.37 o -1 9 0 107.67 120.16 9.42 o 0 9 0 4240.62 4220.42 63.16 o 1 9 0 264.03 297.66 14.16 o 2 9 0 4630.92 4677.73 82.90 o 3 9 0 14.25 7.88 9.08 o 4 9 0 720.17 658.52 35.59 o 5 9 0 386.01 384.43 29.44 o 6 9 0 75.40 43.78 15.55 o -11 10 0 186.89 184.44 22.21 o -10 10 0 247.52 215.30 24.88 o -9 10 0 2113.77 2106.92 56.80 o -8 10 0 859.81 861.38 33.89 o -7 10 0 277.20 266.75 17.81 o -6 10 0 207.79 214.01 14.08 o -5 10 0 6121.11 6291.59 97.07 o -4 10 0 380.86 394.07 15.48 o -3 10 0 472.37 416.70 16.10 o -2 10 0 4038.34 4123.70 62.99 o -1 10 0 127.41 153.00 10.25 o 0 10 0 532.01 546.88 20.53 o 1 10 0 97.22 99.23 11.77 o 2 10 0 3273.36 3202.87 68.33 o 3 10 0 1070.78 995.83 37.42 o 4 10 0 24.39 24.23 11.31 o 5 10 0 1621.04 1549.08 60.14 o -11 11 0 819.24 874.02 62.81 o -10 11 0 588.42 611.36 36.76 o -9 11 0 117.18 76.63 16.21 o -8 11 0 445.16 454.16 22.88 o -7 11 0 5020.38 5005.11 90.36 o -6 11 0 107.38 125.36 14.82 o -5 11 0 35.57 42.60 8.67 o -4 11 0 4035.30 4121.52 66.02 o -3 11 0 6.03 9.17 5.92 o -2 11 0 289.16 294.65 15.14 o -1 11 0 627.14 619.63 23.50 o 0 11 0 5436.66 5632.75 125.90 o 1 11 0 1552.00 1574.74 45.37 o 2 11 0 289.12 262.45 20.08 o 3 11 0 1724.12 1821.70 53.92 o 4 11 0 204.05 206.96 22.40 o -10 12 0 75.55 52.70 12.69 o -9 12 0 1072.23 1148.03 51.80 o -8 12 0 11.80 17.39 15.86 o -7 12 0 1687.50 1741.35 50.17 o -6 12 0 5161.84 5248.89 94.82 o -5 12 0 469.58 464.73 24.02 o -4 12 0 8.70 -1.96 9.71 o -3 12 0 0.09 -2.78 6.92 o -2 12 0 3879.00 3899.02 62.43 o -1 12 0 498.80 491.25 28.72 o 0 12 0 665.04 737.70 36.02 o 1 12 0 1078.35 1094.89 45.99 o 2 12 0 1337.25 1289.37 51.49 o 3 12 0 108.43 135.16 26.29 o -9 13 0 1070.30 1055.99 43.19 o -8 13 0 1213.61 1160.11 49.77 o -7 13 0 435.69 434.97 26.83 o -6 13 0 7.03 5.26 10.33 o -5 13 0 77.54 86.08 12.80 o -4 13 0 1687.83 1656.73 43.92 o -3 13 0 261.78 263.18 15.87 o -2 13 0 2199.15 2230.16 56.81 o -1 13 0 910.79 856.46 39.40 o 0 13 0 298.63 272.06 23.62 o 1 13 0 97.17 78.61 18.11 o 2 13 0 46.30 36.29 13.62 o -8 14 0 362.39 313.73 30.34 o -7 14 0 807.51 852.86 34.44 o -6 14 0 1423.22 1396.21 43.47 o -5 14 0 46.50 50.39 11.18 o -4 14 0 316.37 321.10 20.52 o -3 14 0 234.38 222.12 18.94 o -2 14 0 2.95 4.90 11.32 o -1 14 0 868.12 913.28 37.61 o 0 14 0 673.22 733.88 39.86 o -7 15 0 191.85 195.74 31.51 o -6 15 0 1342.62 1318.40 47.99 o -5 15 0 180.18 171.11 17.71 o -4 15 0 4.81 12.58 11.93 o -3 15 0 621.97 629.48 32.85 o -2 15 0 469.80 474.94 38.14 o 2 -15 1 15.93 23.69 27.49 o 3 -15 1 109.05 96.46 15.26 o 4 -15 1 150.23 158.38 16.92 o 5 -15 1 10.18 26.99 9.94 o 6 -15 1 248.38 255.65 22.20 o 7 -15 1 1328.60 1279.28 59.50 o -1 -14 1 18.00 27.08 16.96 o 0 -14 1 36.00 18.55 14.36 o 1 -14 1 1892.82 1916.29 86.72 o 2 -14 1 16.88 -3.04 9.60 o 3 -14 1 515.93 544.26 26.29 o 4 -14 1 164.02 150.15 19.32 o 5 -14 1 545.12 526.00 32.55 o 6 -14 1 369.60 425.08 26.64 o 7 -14 1 18.19 26.53 14.13 o 8 -14 1 1423.47 1420.39 51.30 o -2 -13 1 274.35 236.47 28.01 o -1 -13 1 2562.91 2595.76 75.51 o 0 -13 1 7.11 -4.44 12.72 o 1 -13 1 74.93 94.25 14.94 o 2 -13 1 370.38 359.93 18.28 o 3 -13 1 363.54 345.64 16.75 o 4 -13 1 201.84 237.35 25.16 o 5 -13 1 1163.73 1202.63 41.03 o 6 -13 1 2618.01 2576.43 64.39 o 7 -13 1 373.12 333.89 22.79 o 8 -13 1 69.13 69.10 13.72 o 9 -13 1 94.75 106.98 19.29 o -3 -12 1 563.41 586.73 35.96 o -2 -12 1 23.61 4.03 13.59 o -1 -12 1 1448.66 1412.55 51.65 o 0 -12 1 17.35 33.96 12.41 o 1 -12 1 5107.29 5157.67 92.06 o 2 -12 1 225.83 203.61 13.33 o 3 -12 1 1068.16 1011.91 33.08 o 4 -12 1 1982.53 1917.98 50.49 o 5 -12 1 37.51 44.20 10.62 o 6 -12 1 328.39 286.48 20.58 o 7 -12 1 396.89 370.08 23.51 o 8 -12 1 3740.05 3775.73 73.26 o 9 -12 1 27.96 30.86 14.15 o 10 -12 1 16.29 3.67 12.51 o -4 -11 1 119.03 122.87 18.89 o -3 -11 1 766.71 827.47 35.46 o -2 -11 1 888.90 890.71 34.93 o -1 -11 1 1714.91 1787.49 48.28 o 0 -11 1 296.87 312.91 20.07 o 1 -11 1 2397.09 2386.20 48.72 o 2 -11 1 2250.18 2298.22 46.88 o 3 -11 1 296.72 283.64 13.62 o 4 -11 1 2020.94 1918.02 38.38 o 5 -11 1 130.69 160.01 14.56 o 6 -11 1 3668.53 3802.32 75.16 o 7 -11 1 183.73 195.68 23.06 o 8 -11 1 664.20 660.96 27.59 o 9 -11 1 2578.20 2594.32 66.20 o 10 -11 1 248.96 245.72 21.51 o -5 -10 1 276.14 309.20 30.41 o -4 -10 1 483.74 549.53 33.45 o -3 -10 1 234.69 233.16 18.52 o -2 -10 1 28.57 20.88 8.70 o -1 -10 1 7478.70 8026.01 118.86 o 0 -10 1 10.41 16.52 6.03 o 1 -10 1 1618.55 1585.28 38.73 o 2 -10 1 6805.87 7231.98 85.05 o 3 -10 1 7.02 1.41 4.98 o 4 -10 1 2936.94 3057.35 58.45 o 5 -10 1 295.68 278.82 16.21 o 6 -10 1 3903.25 3881.73 73.44 o 7 -10 1 1353.75 1223.14 35.53 o 8 -10 1 333.88 399.35 21.42 o 9 -10 1 2149.56 2170.60 58.37 o 10 -10 1 233.14 228.87 20.79 o 11 -10 1 1774.53 1900.21 66.93 o -6 -9 1 522.84 507.57 34.77 o -5 -9 1 41.44 50.35 17.69 o -4 -9 1 364.15 356.47 26.28 o -3 -9 1 4684.12 4706.11 86.05 o -2 -9 1 982.01 995.40 33.59 o -1 -9 1 5.73 -0.34 5.48 o 0 -9 1 5417.54 5482.23 75.43 o 1 -9 1 409.43 377.76 15.59 o 2 -9 1 1701.94 1690.49 30.20 o 3 -9 1 8.47 13.98 5.22 o 4 -9 1 4605.97 4901.94 68.50 o 5 -9 1 4879.13 5032.37 72.55 o 6 -9 1 685.98 702.29 22.87 o 7 -9 1 1213.26 1273.54 34.79 o 8 -9 1 1489.38 1334.51 36.94 o 9 -9 1 1261.16 1247.77 42.11 o 10 -9 1 51.46 31.86 16.79 o 11 -9 1 893.16 797.18 61.36 o -7 -8 1 8.28 25.32 14.23 o -6 -8 1 118.88 105.33 17.61 o -5 -8 1 2208.41 2208.35 66.76 o -4 -8 1 1002.77 1009.58 41.96 o -3 -8 1 863.01 779.19 29.74 o -2 -8 1 3410.16 3234.58 62.41 o -1 -8 1 3245.89 3081.93 49.81 o 0 -8 1 1439.15 1280.38 29.71 o 1 -8 1 1222.48 1224.90 27.13 o 2 -8 1 11375.88 11767.26 101.12 o 3 -8 1 5519.31 5277.24 70.16 o 4 -8 1 14.48 20.15 5.00 o 5 -8 1 1440.71 1433.12 22.58 o 6 -8 1 2844.88 2747.61 52.68 o 7 -8 1 439.55 472.87 17.91 o 8 -8 1 183.11 213.55 14.98 o 9 -8 1 5439.95 5576.50 97.76 o 10 -8 1 539.14 544.27 32.25 o 11 -8 1 112.92 100.67 16.67 o -8 -7 1 81.45 89.34 20.25 o -7 -7 1 2988.84 2958.04 84.32 o -6 -7 1 230.69 258.74 23.55 o -5 -7 1 600.74 689.55 46.19 o -4 -7 1 958.73 935.43 38.32 o -3 -7 1 1042.85 993.66 39.29 o -2 -7 1 2.15 6.54 3.70 o -1 -7 1 1107.60 1056.61 24.49 o 0 -7 1 9276.85 9313.50 107.42 o 1 -7 1 1.07 11.19 3.67 o 2 -7 1 1316.12 1316.97 19.67 o 3 -7 1 5380.03 5482.15 69.87 o 4 -7 1 93.85 73.18 6.98 o 5 -7 1 503.44 506.49 12.58 o 6 -7 1 628.06 588.11 16.26 o 7 -7 1 2444.27 2464.10 56.58 o 8 -7 1 9.74 12.44 5.76 o 9 -7 1 665.62 722.87 29.01 o 10 -7 1 1299.03 1297.30 49.87 o 11 -7 1 454.57 456.76 30.99 o -8 -6 1 12.25 13.14 12.50 o -7 -6 1 1339.85 1310.37 52.00 o -6 -6 1 489.64 437.57 28.37 o -5 -6 1 158.57 187.84 18.25 o -4 -6 1 824.38 826.13 34.29 o -3 -6 1 6903.49 7087.10 102.41 o -2 -6 1 3612.00 3566.76 58.22 o -1 -6 1 1552.63 1631.09 35.07 o 0 -6 1 4995.16 4831.07 62.47 o 1 -6 1 5005.57 5324.98 82.82 o 2 -6 1 4514.88 4582.52 46.63 o 3 -6 1 1309.27 1353.76 25.20 o 4 -6 1 1133.40 1113.17 16.78 o 5 -6 1 5148.27 5204.79 57.16 o 6 -6 1 869.69 840.63 23.15 o 7 -6 1 3111.32 3050.14 47.02 o 8 -6 1 6601.96 6709.21 78.89 o 9 -6 1 3813.12 3925.98 57.17 o 10 -6 1 124.65 134.08 16.46 o 11 -6 1 36.87 42.09 12.49 o -9 -5 1 1406.11 1458.08 52.76 o -8 -5 1 1.37 -4.97 11.60 o -7 -5 1 159.37 169.40 17.59 o -6 -5 1 1783.31 1783.84 55.70 o -5 -5 1 791.07 700.92 31.71 o -4 -5 1 1253.20 1246.71 32.09 o -3 -5 1 48.87 56.64 9.33 o -2 -5 1 16179.87 15194.37 286.14 o -1 -5 1 3145.23 3361.75 58.05 o 0 -5 1 376.79 252.74 10.86 o 1 -5 1 8400.62 8579.09 96.30 o 2 -5 1 5840.61 6051.35 91.11 o 3 -5 1 20381.44 20864.72 336.26 o 4 -5 1 1371.17 1495.33 30.15 o 5 -5 1 6920.43 6868.90 74.09 o 6 -5 1 5264.73 5118.09 77.52 o 7 -5 1 966.84 1040.15 20.93 o 8 -5 1 300.67 296.88 14.23 o 9 -5 1 633.72 608.83 30.00 o 10 -5 1 3514.66 3656.99 77.48 o 11 -5 1 0.95 -14.01 11.38 o -9 -4 1 0.68 5.61 14.77 o -8 -4 1 1099.88 1023.01 39.94 o -7 -4 1 2425.36 2424.92 60.14 o -6 -4 1 471.39 494.46 27.35 o -5 -4 1 959.18 903.55 26.98 o -4 -4 1 18383.99 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