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Acta Cryst. (2012). E68, o8  [ doi:10.1107/S1600536811050653 ]

(3-{[N-(5-Chloro-2-hydroxyphenyl)oxamoyl]amino}propyl)dimethylazanium perchlorate

X.-T. Yue, X.-W. Li and Z.-Y. Wu

Online 3 December 2011


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Alert level C PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.13 PLAT230_ALERT_2_C Hirshfeld Test Diff for N2 -- C9B .. 5.4 su PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0043 Ang PLAT369_ALERT_2_C Long C(sp2)-C(sp2) Bond C7 - C8 ... 1.53 Ang. PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 37 A   3 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 5 PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 77
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 15 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for N3B PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 30 Perc. PLAT431_ALERT_2_G Short Inter HL..A Contact Cl1 .. Cl1 .. 3.25 Ang. PLAT432_ALERT_2_G Short Inter X...Y Contact O6 .. C12B .. 2.85 Ang. PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 Cl O4 PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 16
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 8 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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