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Acta Cryst. (2012). E68, o22  [ doi:10.1107/S1600536811051051 ]

2,8-Dimesitylboranyl-6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine

C.-X. Yuan

Online 3 December 2011


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 18
Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.1 Ratio PLAT480_ALERT_4_C Long H...A H-Bond Reported H14C .. N2 .. 2.64 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 13
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.65 mm PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00300 Deg. PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C11 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C14 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C17 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C20 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C23 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C26 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C42 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C38 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C41 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C45 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C48 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C51
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 17 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 14 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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