# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' cu_Kristerson_R96_131210_0m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 108.78 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.8228 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' _cell_length_a 6.6241 _cell_length_b 13.6873 _cell_length_c 13.9726 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 460.51 413.66 4.94 o 6 0 0 469.39 432.97 3.63 o 2 1 0 530.36 538.95 4.38 o 3 1 0 930.93 986.64 11.36 o 4 1 0 373.83 476.17 4.55 o 5 1 0 581.92 578.79 4.79 o 6 1 0 30.91 22.75 0.35 o 7 1 0 7.27 9.54 0.21 o 0 2 0 3341.92 2952.45 96.06 o 2 2 0 6.48 6.02 0.18 o 3 2 0 2496.97 2703.46 19.47 o 4 2 0 624.80 601.85 4.49 o 5 2 0 416.52 405.80 3.96 o 6 2 0 901.99 888.03 5.38 o 7 2 0 5.55 5.28 0.15 o 1 3 0 13.40 8.34 0.23 o 2 3 0 1099.40 1149.77 10.44 o 3 3 0 125.96 153.27 2.05 o 4 3 0 1484.05 1569.32 10.51 o 5 3 0 559.60 542.60 4.38 o 6 3 0 301.84 302.49 1.77 o 7 3 0 0.12 0.15 0.06 o 2 4 0 910.83 954.11 12.08 o 3 4 0 2.68 2.08 0.15 o 4 4 0 1.26 1.77 0.19 o 5 4 0 48.52 46.06 0.74 o 6 4 0 32.72 33.37 0.73 o 7 4 0 3.79 2.91 0.13 o 1 5 0 254.00 278.21 3.84 o 2 5 0 1246.69 1364.44 16.31 o 3 5 0 368.79 420.09 3.99 o 4 5 0 117.25 125.89 1.30 o 5 5 0 65.87 64.13 0.79 o 6 5 0 137.94 145.68 1.37 o 7 5 0 31.96 24.07 0.35 o 0 6 0 21.85 23.91 0.49 o 1 6 0 290.20 295.25 4.42 o 2 6 0 644.73 682.92 9.33 o 3 6 0 23.31 19.60 0.28 o 4 6 0 12.66 16.54 0.28 o 5 6 0 238.11 235.65 2.07 o 6 6 0 104.14 106.75 1.44 o 7 6 0 98.80 108.17 1.13 o 1 7 0 593.96 609.40 9.06 o 2 7 0 671.25 702.82 5.94 o 3 7 0 346.16 363.56 3.62 o 4 7 0 25.42 24.86 0.37 o 5 7 0 369.15 338.57 2.42 o 6 7 0 0.03 0.28 0.09 o 7 7 0 7.34 7.94 0.43 o 0 8 0 780.41 794.15 9.51 o 1 8 0 3.02 5.44 0.18 o 2 8 0 254.32 260.75 2.47 o 3 8 0 45.52 50.58 0.61 o 4 8 0 174.31 185.36 2.60 o 5 8 0 233.41 219.04 1.88 o 6 8 0 2.93 2.52 0.20 o 7 8 0 99.97 98.64 3.03 o 1 9 0 519.55 515.48 5.05 o 2 9 0 361.35 377.69 4.13 o 3 9 0 2.05 1.12 0.11 o 4 9 0 27.51 28.64 0.34 o 5 9 0 51.50 49.21 0.65 o 6 9 0 19.25 26.07 0.66 o 0 10 0 138.49 149.48 2.69 o 1 10 0 210.70 219.56 2.28 o 2 10 0 24.12 27.05 0.59 o 3 10 0 2.04 1.21 0.10 o 4 10 0 35.60 35.50 0.42 o 5 10 0 20.39 20.67 0.39 o 6 10 0 10.86 12.10 0.30 o 1 11 0 99.29 103.41 1.19 o 2 11 0 71.26 64.42 0.76 o 3 11 0 116.14 112.51 0.94 o 4 11 0 3.74 2.08 0.11 o 5 11 0 78.90 92.42 0.91 o 6 11 0 3.40 5.27 0.41 o 0 12 0 337.53 357.25 3.78 o 1 12 0 1.38 1.42 0.10 o 2 12 0 19.43 18.48 0.27 o 3 12 0 54.23 55.03 0.66 o 4 12 0 59.06 63.87 0.63 o 5 12 0 66.98 65.94 0.77 o 1 13 0 204.35 203.38 1.71 o 2 13 0 393.26 390.09 3.19 o 3 13 0 0.18 0.86 0.12 o 4 13 0 10.71 9.72 0.22 o 5 13 0 22.76 24.85 1.00 o 0 14 0 256.97 248.27 3.38 o 1 14 0 83.49 87.03 1.01 o 2 14 0 32.41 31.09 0.45 o 3 14 0 214.64 228.93 2.53 o 4 14 0 0.05 0.02 0.09 o 1 15 0 192.71 192.05 2.18 o 2 15 0 32.00 38.52 0.77 o 3 15 0 13.94 16.05 0.53 o 1 16 0 81.95 81.90 1.62 o 1 0 1 507.77 61.71 2.25 o 3 0 1 548.25 615.17 4.62 o 4 0 1 17.88 21.09 0.50 o 5 0 1 158.69 160.18 1.46 o 6 0 1 356.81 349.83 2.14 o 7 0 1 113.80 124.24 1.00 o -7 1 1 57.79 53.18 0.50 o -6 1 1 171.09 164.23 1.03 o -5 1 1 111.32 106.98 0.99 o -4 1 1 797.10 852.31 6.64 o -3 1 1 52.93 52.19 0.47 o -2 1 1 868.10 814.66 7.17 o -1 1 1 988.29 961.18 15.20 o 0 1 1 80.59 61.15 1.04 o 1 1 1 989.20 959.61 14.30 o 2 1 1 866.69 810.84 7.51 o 3 1 1 53.06 51.84 1.21 o 4 1 1 795.50 848.32 6.53 o 5 1 1 111.85 106.90 1.03 o 6 1 1 169.83 162.64 1.03 o 7 1 1 57.66 53.03 0.48 o -7 2 1 26.12 27.19 0.31 o -6 2 1 152.50 151.85 1.40 o -5 2 1 6.57 6.83 0.38 o -4 2 1 245.50 264.40 2.00 o -3 2 1 750.24 741.34 6.09 o -2 2 1 462.34 448.53 3.77 o -1 2 1 1134.37 1133.69 14.71 o 0 2 1 3750.69 3442.61 28.45 o 1 2 1 1133.54 1151.87 11.46 o 2 2 1 459.88 448.82 3.92 o 3 2 1 751.87 745.52 6.51 o 4 2 1 247.10 263.55 2.01 o 5 2 1 6.80 6.99 0.18 o 6 2 1 153.68 154.43 1.87 o 7 2 1 26.59 28.17 0.31 o -7 3 1 20.25 16.63 0.23 o -6 3 1 200.58 186.74 1.18 o -5 3 1 78.50 79.97 1.35 o -4 3 1 7.50 8.86 0.19 o -3 3 1 374.83 349.46 3.03 o -2 3 1 594.88 573.06 4.75 o -1 3 1 488.31 455.86 4.83 o 0 3 1 2505.84 2543.74 17.65 o 1 3 1 484.51 452.22 4.61 o 2 3 1 592.35 565.11 4.76 o 3 3 1 379.68 355.54 3.06 o 4 3 1 7.73 9.81 0.20 o 5 3 1 77.19 77.15 0.72 o 6 3 1 200.50 187.97 1.15 o 7 3 1 20.60 17.11 0.24 o -7 4 1 16.63 14.45 0.24 o -6 4 1 214.06 205.74 1.75 o -5 4 1 43.09 46.99 0.72 o -4 4 1 123.11 122.18 1.29 o -3 4 1 58.81 52.26 0.90 o -2 4 1 375.68 372.00 4.74 o -1 4 1 1269.87 1233.65 17.32 o 0 4 1 1033.40 977.41 15.52 o 1 4 1 1269.49 1249.53 17.47 o 2 4 1 375.41 367.41 5.01 o 3 4 1 57.71 54.75 0.93 o 4 4 1 123.81 126.79 1.35 o 5 4 1 43.85 43.92 0.64 o 6 4 1 214.16 202.85 1.73 o 7 4 1 15.93 14.05 0.22 o -7 5 1 8.08 7.72 0.19 o -6 5 1 83.24 84.29 0.84 o -5 5 1 182.33 176.79 1.80 o -4 5 1 291.25 282.53 2.79 o -3 5 1 665.38 717.86 6.40 o -2 5 1 1024.28 1068.57 13.38 o -1 5 1 47.82 49.27 0.89 o 0 5 1 51.47 50.06 0.66 o 1 5 1 48.39 48.91 0.73 o 2 5 1 1025.55 1059.43 13.48 o 3 5 1 663.19 721.08 6.52 o 4 5 1 287.81 278.09 2.92 o 5 5 1 181.38 178.34 1.78 o 6 5 1 82.09 83.01 0.91 o 7 5 1 7.81 7.67 0.19 o -7 6 1 7.64 7.23 0.24 o -6 6 1 102.98 105.85 0.98 o -5 6 1 220.35 204.94 1.88 o -4 6 1 42.93 37.23 0.55 o -3 6 1 42.89 49.09 0.50 o -2 6 1 1110.10 1124.81 15.36 o -1 6 1 861.89 877.32 10.66 o 0 6 1 49.26 45.78 0.54 o 1 6 1 860.17 853.36 11.15 o 2 6 1 1117.90 1163.94 14.23 o 3 6 1 42.74 50.79 0.57 o 4 6 1 43.41 39.64 0.63 o 5 6 1 222.86 212.60 1.91 o 6 6 1 101.99 105.61 1.00 o 7 6 1 7.31 6.98 0.17 o -7 7 1 18.98 19.31 0.39 o -6 7 1 64.06 77.06 0.80 o -5 7 1 4.92 7.08 0.18 o -4 7 1 134.43 126.82 1.19 o -3 7 1 552.07 559.32 4.79 o -2 7 1 357.04 397.84 3.45 o -1 7 1 206.87 219.55 3.03 o 0 7 1 102.52 103.32 1.32 o 1 7 1 203.78 214.84 3.74 o 2 7 1 361.11 402.02 3.51 o 3 7 1 549.54 551.03 5.07 o 4 7 1 135.85 126.60 1.22 o 5 7 1 4.88 6.99 0.28 o 6 7 1 64.81 77.89 0.81 o 7 7 1 19.43 20.37 0.52 o -7 8 1 33.50 34.10 1.26 o -6 8 1 106.85 116.78 0.96 o -5 8 1 157.85 157.05 1.37 o -4 8 1 349.44 337.89 2.86 o -3 8 1 385.79 394.76 3.51 o -2 8 1 105.01 114.38 1.14 o -1 8 1 313.55 351.63 3.37 o 0 8 1 2875.33 2983.04 24.93 o 1 8 1 312.15 356.65 3.27 o 2 8 1 106.60 117.30 1.11 o 3 8 1 382.07 386.74 3.71 o 4 8 1 348.33 327.84 2.77 o 5 8 1 158.59 160.32 1.51 o 6 8 1 107.46 119.27 1.11 o -6 9 1 129.97 145.65 1.39 o -5 9 1 259.58 259.48 2.31 o -4 9 1 99.29 100.50 0.83 o -3 9 1 190.38 185.89 1.70 o -2 9 1 336.67 327.75 3.52 o -1 9 1 404.18 427.54 4.41 o 0 9 1 7.18 5.79 0.16 o 1 9 1 405.96 433.87 4.06 o 2 9 1 338.39 341.61 3.37 o 3 9 1 189.57 185.42 1.76 o 4 9 1 99.70 99.32 0.87 o 5 9 1 258.64 261.58 2.41 o 6 9 1 130.79 146.07 1.48 o -6 10 1 67.03 72.77 0.82 o -5 10 1 56.95 59.34 0.66 o -4 10 1 157.63 150.30 1.16 o -3 10 1 63.73 58.51 0.58 o -2 10 1 256.78 255.87 2.78 o -1 10 1 271.21 273.82 2.92 o 0 10 1 291.38 276.13 3.12 o 1 10 1 268.86 279.11 2.96 o 2 10 1 257.76 269.83 3.38 o 3 10 1 63.12 54.56 0.62 o 4 10 1 155.69 151.96 1.18 o 5 10 1 55.87 58.00 0.67 o 6 10 1 67.34 72.90 0.86 o -6 11 1 1.39 0.71 0.20 o -5 11 1 7.73 6.15 0.17 o -4 11 1 95.23 89.84 0.79 o -3 11 1 131.34 125.46 0.94 o -2 11 1 105.09 105.51 1.08 o -1 11 1 31.92 33.00 0.53 o 0 11 1 25.14 23.17 0.44 o 1 11 1 32.73 35.06 0.49 o 2 11 1 106.53 107.22 1.12 o 3 11 1 132.71 126.53 1.09 o 4 11 1 94.13 90.42 0.82 o 5 11 1 7.56 5.81 0.17 o 6 11 1 1.40 0.59 0.20 o -5 12 1 147.76 153.04 1.56 o -4 12 1 145.60 142.33 1.16 o -3 12 1 159.65 162.23 1.21 o -2 12 1 113.26 102.75 0.99 o -1 12 1 36.13 36.00 0.45 o 0 12 1 72.87 77.98 0.73 o 1 12 1 36.09 36.95 0.42 o 2 12 1 114.77 109.81 0.93 o 3 12 1 159.67 160.53 1.38 o 4 12 1 144.70 141.28 1.19 o 5 12 1 149.39 151.43 1.82 o -4 13 1 10.51 10.35 0.21 o -3 13 1 34.22 35.22 0.49 o -2 13 1 143.77 138.87 1.28 o -1 13 1 14.14 13.55 0.26 o 0 13 1 421.18 396.49 3.06 o 1 13 1 14.24 13.54 0.25 o 2 13 1 144.24 142.89 1.27 o 3 13 1 34.09 35.86 0.48 o 4 13 1 11.19 11.08 0.25 o 5 13 1 0.01 0.31 0.17 o -4 14 1 37.84 45.07 0.90 o -3 14 1 19.66 22.48 0.45 o -2 14 1 115.83 115.97 1.45 o -1 14 1 450.12 453.55 4.28 o 0 14 1 2.48 2.86 0.18 o 1 14 1 444.76 445.51 3.86 o 2 14 1 115.93 117.07 1.23 o 3 14 1 19.92 23.50 0.41 o 4 14 1 38.09 42.37 0.94 o -3 15 1 42.17 45.89 1.53 o -2 15 1 32.41 33.02 0.82 o -1 15 1 10.21 8.71 0.26 o 0 15 1 259.16 282.65 3.10 o 1 15 1 10.75 9.69 0.22 o 2 15 1 32.61 32.74 0.49 o 3 15 1 42.49 47.54 0.88 o -1 16 1 90.46 90.58 1.49 o 0 16 1 0.67 1.05 0.17 o 1 16 1 90.77 93.97 1.75 o 3 0 2 2605.22 2728.76 22.59 o 4 0 2 42.17 44.43 0.56 o 5 0 2 342.97 329.26 2.62 o 6 0 2 126.83 100.83 0.74 o 7 0 2 16.24 13.88 0.24 o -7 1 2 20.63 21.67 0.31 o -6 1 2 44.79 49.76 0.45 o -5 1 2 101.53 97.12 0.99 o -4 1 2 120.83 132.33 1.36 o -3 1 2 623.91 659.85 5.11 o -2 1 2 532.76 514.95 4.55 o -1 1 2 3454.04 3651.60 34.46 o 0 1 2 78.31 65.97 0.73 o 1 1 2 3458.11 3704.87 34.54 o 2 1 2 532.07 510.98 4.64 o 3 1 2 627.23 658.06 5.74 o 4 1 2 118.52 130.69 1.21 o 5 1 2 100.58 96.34 0.87 o 6 1 2 45.07 49.42 0.65 o 7 1 2 20.32 21.79 0.26 o -7 2 2 54.63 56.39 0.53 o -6 2 2 78.64 75.82 0.59 o -5 2 2 162.61 146.97 1.40 o -4 2 2 574.75 612.48 4.67 o -3 2 2 168.52 203.67 1.70 o -2 2 2 961.75 937.62 7.60 o -1 2 2 5340.98 5681.90 53.47 o 0 2 2 4585.34 4344.34 51.57 o 1 2 2 5324.21 5673.14 66.40 o 2 2 2 958.54 935.94 7.72 o 3 2 2 169.85 201.12 1.76 o 4 2 2 571.64 615.25 5.15 o 5 2 2 162.30 149.66 1.32 o 6 2 2 79.10 75.62 0.55 o 7 2 2 54.45 55.55 0.48 o -7 3 2 43.28 40.80 0.42 o -6 3 2 39.82 39.11 0.44 o -5 3 2 186.26 178.30 1.58 o -4 3 2 685.89 676.85 4.50 o -3 3 2 101.64 102.60 1.48 o -2 3 2 984.91 1048.89 7.32 o -1 3 2 654.90 652.37 5.01 o 0 3 2 11664.83 10894.40 95.10 o 1 3 2 659.98 654.04 5.90 o 2 3 2 989.38 1061.23 8.03 o 3 3 2 104.45 103.65 1.07 o 4 3 2 684.72 684.15 5.01 o 5 3 2 186.90 177.83 1.49 o 6 3 2 40.11 39.54 0.43 o 7 3 2 43.93 41.53 0.40 o -7 4 2 7.90 5.78 0.17 o -6 4 2 6.62 7.23 0.21 o -5 4 2 708.67 696.59 7.09 o -4 4 2 107.74 104.75 1.05 o -3 4 2 305.42 324.84 3.32 o -2 4 2 282.35 270.31 2.97 o -1 4 2 2952.92 2996.04 37.78 o 0 4 2 142.73 139.15 1.66 o 1 4 2 2952.73 3012.47 36.85 o 2 4 2 282.86 270.86 3.13 o 3 4 2 303.92 333.13 3.21 o 4 4 2 105.80 106.65 1.51 o 5 4 2 714.32 706.45 7.89 o 6 4 2 6.53 7.04 0.18 o 7 4 2 8.04 6.04 0.18 o -7 5 2 1.81 2.51 0.13 o -6 5 2 254.17 261.29 2.23 o -5 5 2 126.58 116.38 1.19 o -4 5 2 178.81 172.37 1.68 o -3 5 2 29.49 40.58 0.57 o -2 5 2 150.94 154.18 2.07 o -1 5 2 236.54 235.08 2.94 o 0 5 2 112.13 111.02 1.19 o 1 5 2 236.71 234.62 3.07 o 2 5 2 153.50 152.75 1.84 o 3 5 2 30.60 40.31 0.48 o 4 5 2 176.36 175.38 2.39 o 5 5 2 127.92 121.32 1.25 o 6 5 2 251.93 256.18 2.22 o 7 5 2 1.94 2.54 0.12 o -7 6 2 7.46 6.79 0.16 o -6 6 2 49.41 46.34 0.53 o -5 6 2 656.84 654.48 4.50 o -4 6 2 296.60 286.12 2.60 o -3 6 2 240.65 247.45 2.06 o -2 6 2 534.77 536.00 5.48 o -1 6 2 307.05 322.34 3.43 o 0 6 2 954.17 968.53 9.06 o 1 6 2 304.58 323.01 4.13 o 2 6 2 534.29 543.79 5.53 o 3 6 2 242.50 253.39 2.35 o 4 6 2 297.42 287.85 2.76 o 5 6 2 655.93 660.90 5.04 o 6 6 2 47.87 45.35 0.56 o 7 6 2 7.29 6.99 0.18 o -7 7 2 1.78 1.83 0.11 o -6 7 2 17.30 17.68 0.26 o -5 7 2 123.74 114.90 0.94 o -4 7 2 215.00 203.62 1.75 o -3 7 2 55.07 66.52 0.89 o -2 7 2 131.72 140.98 1.28 o -1 7 2 315.42 348.25 4.37 o 0 7 2 1330.46 1423.73 17.75 o 1 7 2 318.70 353.42 4.82 o 2 7 2 131.94 144.15 1.40 o 3 7 2 56.57 64.55 0.84 o 4 7 2 214.66 205.66 2.00 o 5 7 2 122.69 114.61 1.05 o 6 7 2 17.58 17.32 0.30 o 7 7 2 1.77 1.70 0.12 o -6 8 2 33.17 32.04 0.51 o -5 8 2 55.51 56.10 0.57 o -4 8 2 123.42 117.05 1.08 o -3 8 2 5.44 6.10 0.18 o -2 8 2 1278.12 1364.83 11.59 o -1 8 2 84.71 92.34 0.93 o 0 8 2 6.86 12.29 0.21 o 1 8 2 85.72 98.62 1.03 o 2 8 2 1274.80 1342.94 12.68 o 3 8 2 5.18 6.40 0.21 o 4 8 2 123.56 122.96 1.40 o 5 8 2 55.42 57.13 0.69 o 6 8 2 34.36 33.46 0.64 o -6 9 2 107.60 110.62 1.04 o -5 9 2 216.49 204.40 1.63 o -4 9 2 67.45 62.86 0.56 o -3 9 2 465.69 444.78 3.70 o -2 9 2 2.24 4.45 0.19 o -1 9 2 90.74 94.10 1.05 o 0 9 2 887.46 913.98 8.41 o 1 9 2 90.55 92.80 1.12 o 2 9 2 2.31 4.46 0.20 o 3 9 2 466.18 459.23 4.17 o 4 9 2 68.33 61.03 0.63 o 5 9 2 216.40 205.51 2.00 o 6 9 2 106.26 110.64 1.06 o -6 10 2 140.13 138.66 1.35 o -5 10 2 44.01 47.90 0.56 o -4 10 2 191.41 187.19 1.23 o -3 10 2 100.08 101.36 0.86 o -2 10 2 70.31 68.93 0.91 o -1 10 2 90.95 88.08 1.09 o 0 10 2 343.05 329.60 3.89 o 1 10 2 92.06 93.65 1.12 o 2 10 2 71.11 73.87 0.99 o 3 10 2 99.77 102.18 0.93 o 4 10 2 190.47 183.61 1.56 o 5 10 2 43.85 46.01 0.59 o 6 10 2 140.02 141.71 1.52 o -5 11 2 3.66 2.25 0.12 o -4 11 2 76.01 73.40 0.66 o -3 11 2 284.20 279.53 1.98 o -2 11 2 303.12 298.97 2.73 o -1 11 2 217.38 209.62 2.42 o 0 11 2 3.17 2.20 0.17 o 1 11 2 216.08 211.05 2.34 o 2 11 2 304.17 294.67 2.39 o 3 11 2 284.15 277.25 2.26 o 4 11 2 75.66 71.22 0.73 o 5 11 2 3.40 2.15 0.12 o -5 12 2 46.37 50.79 0.65 o -4 12 2 19.32 19.51 0.29 o -3 12 2 91.79 91.76 0.81 o -2 12 2 127.89 130.33 1.17 o -1 12 2 109.33 105.88 1.09 o 0 12 2 160.98 171.84 1.48 o 1 12 2 109.33 106.99 0.99 o 2 12 2 126.39 127.92 1.10 o 3 12 2 91.42 90.10 0.89 o 4 12 2 19.73 19.72 0.37 o 5 12 2 46.30 49.78 0.66 o -4 13 2 96.22 96.68 1.05 o -3 13 2 49.72 53.89 0.66 o -2 13 2 49.46 53.70 0.67 o -1 13 2 234.90 223.82 1.98 o 0 13 2 238.28 240.76 2.02 o 1 13 2 237.31 232.90 1.83 o 2 13 2 49.35 52.46 0.54 o 3 13 2 49.79 51.96 0.67 o 4 13 2 95.96 96.19 1.21 o -3 14 2 2.10 1.95 0.14 o -2 14 2 38.93 34.79 0.58 o -1 14 2 15.73 14.88 0.35 o 0 14 2 57.92 57.02 0.69 o 1 14 2 15.97 15.40 0.31 o 2 14 2 37.95 35.54 0.49 o 3 14 2 1.98 1.60 0.14 o 4 14 2 2.27 1.41 0.17 o -3 15 2 22.93 23.58 0.49 o -2 15 2 5.47 5.25 0.17 o -1 15 2 37.31 34.31 0.56 o 0 15 2 245.35 246.11 2.41 o 1 15 2 37.79 35.18 0.57 o 2 15 2 5.38 5.25 0.17 o 3 15 2 23.15 23.68 0.61 o -1 16 2 45.71 43.50 2.24 o 0 16 2 29.35 30.52 0.57 o 1 16 2 46.56 44.44 1.49 o 1 0 3 5.20 7.10 0.24 o 2 0 3 930.50 963.47 7.32 o 3 0 3 499.52 535.25 4.54 o 4 0 3 151.05 179.56 1.53 o 5 0 3 446.16 470.73 3.87 o 6 0 3 112.09 103.17 0.79 o 7 0 3 15.94 20.90 0.30 o -7 1 3 43.22 44.85 0.46 o -6 1 3 419.53 430.37 2.98 o -5 1 3 84.68 77.23 0.81 o -4 1 3 171.83 197.95 1.67 o -3 1 3 530.04 561.36 4.43 o -2 1 3 228.25 227.20 1.71 o -1 1 3 28.58 38.12 0.47 o 0 1 3 4402.90 4086.31 40.35 o 1 1 3 28.14 36.73 0.67 o 2 1 3 226.67 222.67 1.84 o 3 1 3 527.17 548.91 4.47 o 4 1 3 172.15 198.17 1.61 o 5 1 3 84.67 78.63 0.78 o 6 1 3 420.18 430.51 2.64 o 7 1 3 43.10 44.53 0.46 o -7 2 3 37.01 33.46 0.39 o -6 2 3 74.90 68.13 0.65 o -5 2 3 81.83 81.60 0.84 o -4 2 3 63.72 60.86 1.36 o -3 2 3 244.81 246.00 2.04 o -2 2 3 2241.50 2340.14 15.81 o -1 2 3 4250.89 4520.12 45.64 o 0 2 3 11701.46 11243.75 107.20 o 1 2 3 4250.76 4542.47 46.99 o 2 2 3 2238.42 2338.13 17.03 o 3 2 3 244.28 244.78 2.05 o 4 2 3 63.85 63.82 0.95 o 5 2 3 80.68 81.40 0.79 o 6 2 3 75.35 69.04 0.59 o 7 2 3 36.12 33.70 0.36 o -7 3 3 13.09 12.84 0.21 o -6 3 3 419.15 413.57 3.00 o -5 3 3 34.45 31.65 0.43 o -4 3 3 65.88 66.05 0.97 o -3 3 3 572.97 625.95 4.49 o -2 3 3 1030.60 1043.27 7.91 o -1 3 3 830.53 825.03 7.68 o 0 3 3 1349.44 1368.28 12.66 o 1 3 3 836.67 862.90 8.43 o 2 3 3 1024.35 1023.46 7.43 o 3 3 3 574.68 616.93 4.61 o 4 3 3 65.91 66.84 0.81 o 5 3 3 34.70 32.68 0.60 o 6 3 3 424.17 414.96 2.86 o 7 3 3 13.34 13.33 0.20 o -7 4 3 68.34 72.87 0.76 o -6 4 3 13.69 11.85 0.26 o -5 4 3 477.61 470.52 5.31 o -4 4 3 81.31 77.72 0.84 o -3 4 3 298.80 302.31 2.64 o -2 4 3 790.13 836.26 8.87 o -1 4 3 607.91 594.84 6.64 o 0 4 3 335.36 328.34 3.97 o 1 4 3 615.45 611.84 6.80 o 2 4 3 796.06 841.98 10.30 o 3 4 3 297.49 300.49 2.90 o 4 4 3 82.38 81.55 1.02 o 5 4 3 472.95 458.60 5.37 o 6 4 3 13.66 11.26 0.23 o 7 4 3 69.24 73.88 0.62 o -7 5 3 17.39 14.88 0.27 o -6 5 3 39.17 41.93 0.75 o -5 5 3 132.09 130.49 1.29 o -4 5 3 415.75 429.50 3.80 o -3 5 3 610.84 634.47 4.93 o -2 5 3 61.18 65.51 0.99 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