(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2012). E68, o1024 [ doi:10.1107/S1600536812009361 ]

2-[(E)-(Naphthalen-2-ylimino)methyl]-4-(trifluoromethoxy)phenol

M. Pekdemir, Z. S. Sahin, S. Isik, A. Alaman Agar, S. Öztürk Yildirim and R. J. Butcher

Online 10 March 2012

Key indicators

Single-crystal X-ray study
T = 123 K
Mean (C-C) = 0.003 Å
R factor = 0.049
wR factor = 0.130
Data-to-parameter ratio = 13.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C18     
PLAT480_ALERT_4_C Long H...A H-Bond Reported H5     ..  F2      ..       2.57 Ang. 
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          5      

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   3 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   1 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check


checkCIF publication errors

Alert level A
PUBL024_ALERT_1_A The number of authors is greater than 5.
              Please specify the role of each of the co-authors
              for your paper.

Author Response: A. Alaman A\<gar - did the synthesis, crystalized the title compound and prepared the chemical sections of the manuscript. R. J. Butcher and S. Ozturk Y\?ild\?ir\?im - collected the XRD data, Z. S. '\;Sahin, \;S. I\;s\?ik and M. Pekdemir - solved, refined the crystal structure, checked the structure, drawn the scheme and figures, and prepared the manuscript.


   1 ALERT level A = Data missing that is essential or data in wrong format
   0 ALERT level G = General alerts. Data that may be required is missing