# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 100.55 _exptl_crystal_F_000 300.00 _reflns_d_resolution_high 0.7697 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 3.6477 _cell_length_b 16.9661 _cell_length_c 9.5465 _cell_angle_alpha 90.000 _cell_angle_beta 97.465 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 55.95 41.45 0.86 o 2 0 0 231.67 249.84 4.95 o 3 0 0 24.07 22.55 0.97 o 4 0 0 2.87 3.87 0.32 o 1 1 0 1278.06 1343.90 21.21 o 2 1 0 40.21 38.87 0.59 o 3 1 0 31.54 30.18 0.58 o 4 1 0 2.09 1.47 0.32 o 1 2 0 4100.40 3995.66 65.59 o 2 2 0 114.83 111.05 1.58 o 3 2 0 6.66 5.94 0.20 o 4 2 0 1.10 0.98 0.15 o 1 3 0 138.50 135.84 1.90 o 2 3 0 22.49 22.30 0.33 o 3 3 0 0.15 0.11 0.09 o 4 3 0 12.10 13.32 0.41 o 0 4 0 1200.01 1016.41 142.77 o 1 4 0 386.36 409.83 5.11 o 2 4 0 0.91 1.35 0.17 o 3 4 0 33.05 34.51 0.65 o 4 4 0 10.31 9.97 0.45 o 1 5 0 1092.00 1168.90 14.49 o 2 5 0 5.58 4.34 0.12 o 3 5 0 89.69 86.84 2.90 o 4 5 0 0.30 0.36 0.14 o 0 6 0 5.23 1.60 0.06 o 1 6 0 4.39 3.83 0.19 o 2 6 0 0.75 0.17 0.05 o 3 6 0 2.83 2.23 0.19 o 4 6 0 15.34 15.36 0.50 o 1 7 0 207.36 181.77 2.29 o 2 7 0 260.17 276.59 3.87 o 3 7 0 5.40 6.39 0.27 o 4 7 0 2.52 2.75 0.25 o 0 8 0 42.84 32.75 0.68 o 1 8 0 205.96 246.12 3.61 o 2 8 0 16.05 17.49 0.60 o 3 8 0 5.03 3.93 0.24 o 4 8 0 22.73 25.31 0.71 o 1 9 0 26.45 28.36 0.40 o 2 9 0 113.57 118.57 1.71 o 3 9 0 120.11 124.14 2.60 o 4 9 0 0.78 0.47 0.17 o 0 10 0 1059.98 996.61 38.41 o 1 10 0 0.74 1.20 0.08 o 2 10 0 22.63 22.58 0.64 o 3 10 0 22.87 20.36 0.59 o 4 10 0 10.41 11.56 0.45 o 1 11 0 73.83 71.07 0.95 o 2 11 0 40.50 37.04 0.72 o 3 11 0 1.52 1.84 0.25 o 4 11 0 15.19 16.90 0.87 o 0 12 0 0.20 0.66 0.06 o 1 12 0 8.86 7.96 0.20 o 2 12 0 14.62 15.31 0.38 o 3 12 0 91.12 92.49 2.37 o 1 13 0 20.13 16.96 0.32 o 2 13 0 28.01 26.33 0.56 o 3 13 0 0.14 0.27 0.25 o 0 14 0 94.24 87.10 1.89 o 1 14 0 2.71 2.49 0.12 o 2 14 0 2.58 2.06 0.15 o 3 14 0 4.97 5.34 0.29 o 1 15 0 56.77 61.58 0.96 o 2 15 0 0.66 1.24 0.13 o 3 15 0 29.69 34.22 0.87 o 0 16 0 1.23 0.47 0.19 o 1 16 0 33.05 28.30 0.77 o 2 16 0 19.11 16.85 0.41 o 3 16 0 1.31 2.00 0.20 o 1 17 0 4.01 2.31 0.23 o 2 17 0 70.35 75.15 1.36 o 0 18 0 47.12 47.64 1.64 o 1 18 0 1.38 0.52 0.16 o 2 18 0 1.65 1.80 0.15 o 1 19 0 29.55 28.40 1.08 o 2 19 0 18.17 20.52 0.75 o 0 20 0 4.05 4.51 0.43 o 1 20 0 17.79 14.76 0.53 o 1 21 0 7.12 5.66 0.50 o -4 1 1 0.70 0.91 0.14 o -3 1 1 19.69 20.77 0.51 o -2 1 1 5.48 5.23 0.13 o -1 1 1 3842.40 3579.77 51.51 o 0 1 1 847.65 833.28 41.89 o 1 1 1 827.65 789.66 21.12 o 2 1 1 148.43 152.15 2.46 o 3 1 1 1.33 1.65 0.19 o 4 1 1 10.31 10.38 0.35 o -4 2 1 33.23 35.47 0.84 o -3 2 1 17.01 16.95 0.37 o -2 2 1 12.68 9.78 0.20 o -1 2 1 10110.13 8475.53 151.40 o 0 2 1 147.84 163.98 3.11 o 1 2 1 65.95 68.94 1.91 o 2 2 1 94.14 89.49 1.47 o 3 2 1 120.77 122.47 2.03 o 4 2 1 0.66 0.26 0.11 o -4 3 1 14.11 13.13 0.41 o -3 3 1 15.31 14.91 0.40 o -2 3 1 1717.14 1797.77 22.34 o -1 3 1 7.43 3.86 0.16 o 0 3 1 1144.01 949.91 21.86 o 1 3 1 58.04 76.81 1.23 o 2 3 1 59.10 54.13 0.94 o 3 3 1 57.17 53.83 0.96 o 4 3 1 43.48 39.98 1.30 o -4 4 1 0.08 0.10 0.12 o -3 4 1 3.77 3.12 0.15 o -2 4 1 18.25 18.50 0.33 o -1 4 1 1057.62 1038.86 14.36 o 0 4 1 2638.40 1941.59 72.68 o 1 4 1 131.78 142.36 2.25 o 2 4 1 64.21 62.80 0.92 o 3 4 1 1.23 1.31 0.23 o 4 4 1 8.14 8.21 0.45 o -4 5 1 0.11 0.15 0.10 o -3 5 1 38.46 38.87 0.73 o -2 5 1 204.89 196.50 2.76 o -1 5 1 2987.04 2988.07 48.16 o 0 5 1 961.99 830.66 17.14 o 1 5 1 474.60 468.14 5.81 o 2 5 1 15.98 17.42 0.31 o 3 5 1 13.15 12.71 0.31 o 4 5 1 27.19 28.07 0.75 o -4 6 1 0.55 0.46 0.14 o -3 6 1 5.44 4.99 0.19 o -2 6 1 73.06 70.36 1.22 o -1 6 1 362.72 391.50 5.50 o 0 6 1 44.44 47.41 0.67 o 1 6 1 258.46 286.62 3.57 o 2 6 1 119.83 128.46 1.83 o 3 6 1 2.08 2.59 0.20 o 4 6 1 1.93 1.38 0.18 o -4 7 1 42.24 43.90 1.07 o -3 7 1 38.81 39.27 0.93 o -2 7 1 5.00 4.82 0.15 o -1 7 1 310.03 313.23 3.90 o 0 7 1 2431.65 2121.98 72.29 o 1 7 1 101.43 100.22 1.28 o 2 7 1 34.80 39.35 0.61 o 3 7 1 71.09 70.16 1.54 o 4 7 1 5.65 5.25 0.31 o -4 8 1 35.71 33.82 0.87 o -3 8 1 6.87 7.04 0.30 o -2 8 1 0.92 0.53 0.14 o -1 8 1 257.07 287.32 3.58 o 0 8 1 3.92 5.47 0.11 o 1 8 1 155.30 170.75 2.15 o 2 8 1 1.97 2.14 0.12 o 3 8 1 97.37 101.46 2.16 o 4 8 1 30.36 30.31 0.82 o -4 9 1 0.05 0.13 0.14 o -3 9 1 72.57 67.71 1.50 o -2 9 1 4.40 3.10 0.12 o -1 9 1 17.08 20.31 0.44 o 0 9 1 340.19 299.96 12.82 o 1 9 1 75.22 86.19 1.11 o 2 9 1 41.55 43.47 0.99 o 3 9 1 6.48 5.32 0.22 o 4 9 1 1.97 1.83 0.21 o -4 10 1 1.64 1.42 0.41 o -3 10 1 1.27 0.92 0.13 o -2 10 1 33.39 34.52 0.87 o -1 10 1 21.96 18.11 0.27 o 0 10 1 169.28 172.30 2.45 o 1 10 1 36.76 37.36 0.59 o 2 10 1 72.27 82.13 1.75 o 3 10 1 49.49 53.73 1.24 o 4 10 1 0.09 0.09 0.25 o -4 11 1 0.00 -0.12 0.25 o -3 11 1 15.13 15.02 0.39 o -2 11 1 4.02 2.89 0.16 o -1 11 1 429.70 461.53 6.50 o 0 11 1 131.47 141.62 2.03 o 1 11 1 99.97 108.66 1.59 o 2 11 1 179.74 172.86 2.90 o 3 11 1 18.53 16.30 0.50 o 4 11 1 4.87 4.79 0.51 o -3 12 1 1.68 2.59 0.21 o -2 12 1 9.99 9.40 0.42 o -1 12 1 3.10 4.55 0.17 o 0 12 1 0.80 0.54 0.07 o 1 12 1 15.78 19.20 0.35 o 2 12 1 19.23 16.67 0.40 o 3 12 1 16.92 18.01 0.55 o -3 13 1 19.70 19.32 0.62 o -2 13 1 17.97 20.03 0.45 o -1 13 1 24.56 22.75 0.49 o 0 13 1 31.88 28.62 0.44 o 1 13 1 0.50 0.50 0.07 o 2 13 1 294.38 296.24 4.90 o 3 13 1 20.16 22.54 0.64 o -3 14 1 0.44 0.25 0.13 o -2 14 1 10.89 9.91 0.29 o -1 14 1 12.61 12.64 0.30 o 0 14 1 3.58 4.12 0.12 o 1 14 1 3.57 4.56 0.16 o 2 14 1 77.31 78.14 1.40 o 3 14 1 24.03 27.98 0.75 o -3 15 1 0.28 0.51 0.13 o -2 15 1 3.16 4.21 0.19 o -1 15 1 0.24 0.01 0.14 o 0 15 1 1.30 0.70 0.06 o 1 15 1 335.90 332.36 4.74 o 2 15 1 1.16 2.05 0.15 o 3 15 1 4.59 6.47 0.37 o -3 16 1 0.01 -0.05 0.18 o -2 16 1 0.75 1.36 0.13 o -1 16 1 42.73 43.91 1.08 o 0 16 1 10.92 11.11 0.40 o 1 16 1 0.87 1.24 0.11 o 2 16 1 91.80 97.34 1.72 o 3 16 1 20.18 20.50 0.60 o -3 17 1 0.15 0.58 0.13 o -2 17 1 4.75 3.61 0.19 o -1 17 1 81.57 75.84 2.13 o 0 17 1 3.17 3.59 0.25 o 1 17 1 76.93 74.20 1.63 o 2 17 1 0.04 0.67 0.21 o -2 18 1 0.54 0.09 0.16 o -1 18 1 2.93 2.88 0.25 o 0 18 1 76.97 73.56 1.68 o 1 18 1 68.25 71.82 2.49 o 2 18 1 6.13 7.59 0.27 o -2 19 1 10.22 11.44 0.48 o -1 19 1 14.22 13.27 0.49 o 0 19 1 84.93 78.09 1.97 o 1 19 1 2.57 3.05 0.26 o 2 19 1 25.86 26.13 0.58 o -1 20 1 2.76 2.54 0.35 o 0 20 1 23.74 28.11 0.80 o 1 20 1 27.61 30.02 1.21 o -1 21 1 4.89 5.65 0.50 o 0 21 1 4.59 5.65 0.47 o 1 21 1 11.88 12.73 0.72 o -4 0 2 4.88 3.58 0.31 o -3 0 2 13.64 14.04 0.56 o -2 0 2 3.48 3.04 0.15 o -1 0 2 5337.50 4430.81 90.72 o 0 0 2 435.69 416.83 8.14 o 1 0 2 1618.94 1466.29 42.85 o 2 0 2 563.10 588.52 15.68 o 3 0 2 0.59 0.39 0.10 o 4 0 2 15.77 15.19 0.62 o -4 1 2 3.13 3.11 0.22 o -3 1 2 47.04 45.96 0.83 o -2 1 2 102.10 111.06 1.42 o -1 1 2 217.33 185.43 2.57 o 0 1 2 1558.35 1396.25 22.52 o 1 1 2 137.19 133.14 2.11 o 2 1 2 30.06 30.42 0.77 o 3 1 2 32.12 33.66 0.63 o 4 1 2 2.35 3.38 0.24 o -4 2 2 5.65 6.39 0.28 o -3 2 2 79.85 82.36 1.40 o -2 2 2 197.96 175.44 2.22 o -1 2 2 633.92 617.69 9.78 o 0 2 2 291.65 333.64 7.30 o 1 2 2 169.95 168.09 2.66 o 2 2 2 5.41 3.02 0.40 o 3 2 2 23.22 23.01 0.41 o 4 2 2 27.50 28.59 0.98 o -4 3 2 0.04 0.15 0.12 o -3 3 2 19.44 17.55 0.39 o -2 3 2 41.44 40.76 0.56 o -1 3 2 894.90 893.23 12.40 o 0 3 2 1487.08 1302.88 22.78 o 1 3 2 821.73 804.92 15.35 o 2 3 2 55.35 61.43 1.02 o 3 3 2 93.18 97.60 2.06 o 4 3 2 3.14 2.27 0.26 o -4 4 2 0.66 0.84 0.14 o -3 4 2 19.32 20.66 0.44 o -2 4 2 1377.61 1388.28 21.87 o -1 4 2 641.05 662.30 9.14 o 0 4 2 442.96 457.42 7.18 o 1 4 2 117.93 132.00 2.31 o 2 4 2 153.53 156.47 2.50 o 3 4 2 15.36 17.07 0.42 o 4 4 2 15.23 14.35 0.62 o -4 5 2 0.92 0.97 0.13 o -3 5 2 53.80 49.31 0.89 o -2 5 2 303.85 295.62 4.12 o -1 5 2 0.02 0.06 0.04 o 0 5 2 22.39 19.64 0.37 o 1 5 2 5.07 6.29 0.48 o 2 5 2 590.37 598.01 10.20 o 3 5 2 17.15 17.31 0.50 o 4 5 2 3.60 4.24 0.27 o -4 6 2 15.98 15.14 0.49 o -3 6 2 24.53 19.99 0.38 o -2 6 2 839.50 892.16 12.31 o -1 6 2 228.96 235.78 3.27 o 0 6 2 46.30 47.83 0.62 o 1 6 2 8.68 8.09 0.17 o 2 6 2 11.35 12.04 0.24 o 3 6 2 69.14 67.92 1.50 o 4 6 2 10.29 10.98 0.68 o -4 7 2 19.69 17.41 0.54 o -3 7 2 58.43 58.80 0.92 o -2 7 2 134.14 133.48 1.91 o -1 7 2 136.94 131.01 1.65 o 0 7 2 0.02 0.05 0.03 o 1 7 2 8.40 11.86 0.29 o 2 7 2 0.09 0.43 0.08 o 3 7 2 1.45 2.34 0.38 o 4 7 2 15.80 15.25 0.55 o -4 8 2 3.38 3.27 0.54 o -3 8 2 108.43 110.78 1.63 o -2 8 2 40.00 43.65 0.68 o -1 8 2 76.77 96.75 1.24 o 0 8 2 56.18 55.91 0.72 o 1 8 2 167.06 182.32 3.00 o 2 8 2 21.35 25.05 0.50 o 3 8 2 89.00 90.07 2.09 o 4 8 2 1.97 2.16 0.42 o -4 9 2 2.10 1.59 0.20 o -3 9 2 0.78 1.19 0.12 o -2 9 2 152.19 148.77 2.49 o -1 9 2 801.60 826.11 10.24 o 0 9 2 63.07 62.28 0.81 o 1 9 2 49.64 55.62 0.85 o 2 9 2 616.67 630.05 10.19 o 3 9 2 0.43 0.82 0.15 o 4 9 2 2.46 2.62 0.40 o -4 10 2 2.12 1.96 0.22 o -3 10 2 1.45 2.22 0.17 o -2 10 2 45.27 40.71 0.77 o -1 10 2 52.05 54.65 0.83 o 0 10 2 0.03 0.52 0.30 o 1 10 2 19.70 21.20 0.37 o 2 10 2 35.32 37.20 0.71 o 3 10 2 36.68 34.38 0.86 o 4 10 2 0.76 0.41 0.28 o -4 11 2 6.52 5.26 0.49 o -3 11 2 0.00 -0.07 0.09 o -2 11 2 8.69 9.43 0.22 o -1 11 2 114.87 117.43 1.71 o 0 11 2 85.96 93.83 1.37 o 1 11 2 666.90 709.08 9.97 o 2 11 2 19.00 15.98 0.46 o 3 11 2 43.37 39.65 0.97 o -3 12 2 2.95 3.54 0.20 o -2 12 2 1.36 1.14 0.09 o -1 12 2 36.06 31.69 0.54 o 0 12 2 10.14 9.04 0.19 o 1 12 2 14.31 13.50 0.27 o 2 12 2 12.76 13.70 0.41 o 3 12 2 35.36 36.41 1.00 o -3 13 2 3.04 3.11 0.20 o -2 13 2 136.42 131.51 2.45 o -1 13 2 1.05 1.26 0.15 o 0 13 2 497.14 507.73 9.06 o 1 13 2 89.16 80.56 1.22 o 2 13 2 0.49 0.58 0.14 o 3 13 2 5.11 5.03 0.27 o -3 14 2 2.85 2.46 0.18 o -2 14 2 0.24 0.55 0.11 o -1 14 2 56.89 48.14 0.88 o 0 14 2 15.72 14.16 0.28 o 1 14 2 219.55 220.67 3.18 o 2 14 2 39.85 41.09 0.97 o 3 14 2 5.55 5.70 0.30 o -3 15 2 2.89 3.46 0.21 o -2 15 2 131.32 133.48 2.29 o -1 15 2 17.55 15.81 0.50 o 0 15 2 42.27 40.14 0.74 o 1 15 2 22.25 22.58 0.42 o 2 15 2 32.47 35.64 0.86 o 3 15 2 1.08 4.35 0.33 o -3 16 2 3.96 4.86 0.27 o -2 16 2 1.49 0.97 0.18 o -1 16 2 32.44 34.54 0.89 o 0 16 2 316.82 290.98 13.47 o 1 16 2 62.44 61.99 0.98 o 2 16 2 12.71 11.24 0.38 o 3 16 2 7.44 8.26 0.62 o -2 17 2 13.82 13.32 0.49 o -1 17 2 55.84 50.26 1.22 o 0 17 2 2.86 3.42 0.36 o 1 17 2 16.10 18.65 0.37 o 2 17 2 0.00 -0.09 0.11 o -2 18 2 1.84 2.24 0.24 o -1 18 2 8.94 8.83 0.38 o 0 18 2 24.78 26.12 0.88 o 1 18 2 18.15 15.72 0.34 o 2 18 2 17.17 18.20 0.53 o -2 19 2 0.27 0.04 0.14 o -1 19 2 4.28 4.24 0.29 o 0 19 2 1.83 0.92 0.19 o 1 19 2 1.13 1.21 0.20 o 2 19 2 15.75 19.39 0.56 o -1 20 2 0.41 0.45 0.16 o 0 20 2 0.00 -0.18 0.20 o 1 20 2 7.34 9.68 0.61 o -1 21 2 1.16 0.00 0.22 o 0 21 2 0.26 -0.01 0.24 o 1 21 2 1.65 1.23 0.31 o -4 1 3 17.63 17.27 0.50 o -3 1 3 18.55 19.80 0.42 o -2 1 3 116.09 122.22 1.73 o -1 1 3 757.98 729.33 11.49 o 0 1 3 5.73 7.10 0.12 o 1 1 3 91.57 104.11 1.66 o 2 1 3 221.90 228.22 3.62 o 3 1 3 128.02 125.20 2.05 o 4 1 3 4.26 4.59 0.39 o -4 2 3 0.65 0.21 0.11 o -3 2 3 2.33 2.34 0.14 o -2 2 3 1282.86 1223.23 16.88 o -1 2 3 1371.52 1326.26 30.99 o 0 2 3 1233.62 1278.90 26.51 o 1 2 3 20.00 22.50 0.39 o 2 2 3 0.21 0.50 0.06 o 3 2 3 7.88 8.57 0.30 o 4 2 3 1.43 2.26 0.29 o -4 3 3 5.04 5.49 0.26 o -3 3 3 50.91 47.52 0.88 o -2 3 3 195.53 195.08 2.74 o -1 3 3 36.48 39.16 0.58 o 0 3 3 185.58 205.94 3.42 o 1 3 3 254.33 280.52 4.41 o 2 3 3 176.14 192.78 3.07 o 3 3 3 44.49 48.37 0.89 o 4 3 3 0.51 0.73 0.23 o -4 4 3 1.22 1.44 0.16 o -3 4 3 43.69 46.16 0.84 o -2 4 3 103.03 101.06 1.67 o -1 4 3 43.52 46.90 0.69 o 0 4 3 357.83 339.16 5.33 o 1 4 3 258.84 324.95 5.10 o 2 4 3 77.02 76.61 1.26 o 3 4 3 4.91 5.13 0.21 o 4 4 3 24.15 24.93 0.91 o -4 5 3 0.66 0.53 0.14 o -3 5 3 111.43 106.20 1.65 o -2 5 3 11.09 8.80 0.26 o -1 5 3 98.73 97.81 1.39 o 0 5 3 203.70 210.19 3.31 o 1 5 3 11.63 13.94 0.25 o 2 5 3 6.62 8.39 0.33 o 3 5 3 0.27 0.25 0.13 o 4 5 3 48.29 51.25 1.21 o -4 6 3 0.36 0.33 0.20 o -3 6 3 75.65 75.89 1.32 o -2 6 3 47.25 46.77 0.72 o -1 6 3 0.32 0.97 0.10 o 0 6 3 1002.90 1055.37 16.60 o 1 6 3 640.48 667.33 12.94 o 2 6 3 1.01 0.97 0.10 o 3 6 3 21.38 21.30 0.59 o 4 6 3 1.48 0.97 0.21 o -4 7 3 5.27 3.34 0.19 o -3 7 3 101.76 97.74 1.45 o -2 7 3 12.87 13.70 0.27 o -1 7 3 18.66 20.11 0.33 o 0 7 3 118.60 122.44 1.94 o 1 7 3 1398.79 1458.86 51.88 o 2 7 3 36.54 32.99 0.94 o 3 7 3 3.68 3.87 0.24 o 4 7 3 0.12 0.39 0.20 o -4 8 3 5.85 5.02 0.23 o -3 8 3 57.23 59.56 0.93 o -2 8 3 184.29 190.80 2.70 o -1 8 3 14.89 17.55 0.30 o 0 8 3 51.46 47.19 0.77 o 1 8 3 149.32 155.03 3.06 o 2 8 3 23.75 20.07 0.42 o 3 8 3 61.52 63.93 1.43 o 4 8 3 0.18 0.25 0.26 o -4 9 3 24.17 22.28 0.65 o -3 9 3 25.93 27.49 0.49 o -2 9 3 11.39 12.08 0.25 o -1 9 3 75.83 78.55 1.14 o 0 9 3 231.19 245.60 3.40 o 1 9 3 20.41 18.78 0.44 o 2 9 3 0.40 0.73 0.10 o 3 9 3 2.23 2.98 0.23 o -4 10 3 23.07 23.04 0.67 o -3 10 3 13.14 13.95 0.31 o -2 10 3 71.63 74.36 1.11 o -1 10 3 15.96 15.88 0.28 o 0 10 3 90.69 97.21 1.62 o 1 10 3 7.04 5.61 0.17 o 2 10 3 430.79 441.25 7.19 o 3 10 3 0.01 0.08 0.22 o -4 11 3 5.27 6.13 0.49 o -3 11 3 22.54 22.18 0.51 o -2 11 3 0.79 0.66 0.08 o -1 11 3 240.91 234.80 3.29 o 0 11 3 0.01 0.10 0.04 o 1 11 3 378.54 378.39 6.17 o 2 11 3 0.66 0.72 0.10 o 3 11 3 7.15 8.26 0.34 o -3 12 3 11.88 9.93 0.31 o -2 12 3 41.64 38.34 0.63 o -1 12 3 197.35 191.20 3.16 o 0 12 3 235.62 234.35 3.83 o 1 12 3 34.09 37.28 0.70 o 2 12 3 13.40 13.14 0.49 o 3 12 3 11.66 11.68 0.47 o -3 13 3 33.06 37.17 0.81 o -2 13 3 2.09 1.15 0.13 o -1 13 3 5.09 4.15 0.16 o 0 13 3 7.44 5.58 0.14 o 1 13 3 39.48 44.33 0.82 o 2 13 3 38.76 39.70 0.94 o 3 13 3 10.20 9.25 0.36 o -3 14 3 18.92 18.21 0.53 o -2 14 3 64.49 66.34 1.21 o -1 14 3 237.99 228.87 3.78 o 0 14 3 0.04 -0.11 0.08 o 1 14 3 174.18 174.85 2.92 o 2 14 3 152.69 157.70 3.24 o 3 14 3 3.90 4.23 0.25 o -3 15 3 28.29 27.64 0.62 o -2 15 3 25.81 23.80 1.30 o -1 15 3 0.54 0.61 0.14 o 0 15 3 5.03 4.37 0.17 o 1 15 3 65.32 69.15 1.23 o 2 15 3 0.02 0.22 0.13 o 3 15 3 12.57 13.74 0.80 o -3 16 3 0.33 0.61 0.13 o -2 16 3 1.98 1.75 0.37 o -1 16 3 18.88 19.37 0.57 o 0 16 3 5.43 4.35 0.23 o 1 16 3 106.08 106.57 1.83 o 2 16 3 35.31 35.24 0.86 o -2 17 3 7.32 5.83 0.32 o -1 17 3 4.89 5.20 0.29 o 0 17 3 29.36 29.11 0.58 o 1 17 3 98.67 102.23 1.77 o 2 17 3 9.76 12.49 0.40 o -2 18 3 0.68 0.31 0.15 o -1 18 3 36.51 35.08 1.04 o 0 18 3 73.90 76.04 3.04 o 1 18 3 0.12 0.00 0.12 o 2 18 3 7.56 9.27 0.66 o -2 19 3 4.18 5.84 0.35 o -1 19 3 0.04 0.28 0.21 o 0 19 3 25.75 24.77 1.04 o 1 19 3 12.60 13.45 0.35 o -1 20 3 16.89 18.47 0.60 o 0 20 3 2.06 1.48 0.30 o -1 21 3 32.85 36.71 1.44 o 0 21 3 11.36 11.73 0.68 o -4 0 4 11.18 9.31 0.48 o -3 0 4 50.67 50.08 1.53 o -2 0 4 336.40 333.46 7.01 o -1 0 4 484.74 513.36 9.99 o 0 0 4 1009.39 1045.36 20.39 o 1 0 4 1.05 2.27 0.09 o 2 0 4 152.99 151.76 4.11 o 3 0 4 8.52 8.76 0.30 o -4 1 4 16.04 16.33 0.49 o -3 1 4 119.93 113.45 1.89 o -2 1 4 79.64 81.63 1.18 o -1 1 4 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