# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' JAB061_0m in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 389.42 _exptl_crystal_F_000 1240.00 _reflns_d_resolution_high 0.8368 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.7631 _cell_length_b 13.6077 _cell_length_c 14.2614 _cell_angle_alpha 102.785 _cell_angle_beta 96.943 _cell_angle_gamma 104.316 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 113397.52 133950.33 1234.85 o 2 0 0 31537.33 31526.30 446.20 o 3 0 0 5921.32 6341.98 206.70 o 4 0 0 11672.53 11631.04 314.62 o 5 0 0 561.98 363.43 131.93 o 6 0 0 4152.25 4078.69 212.96 o 7 0 0 8902.16 9115.38 261.24 o 8 0 0 7727.81 6885.22 229.92 o 9 0 0 3496.53 3596.24 199.44 o 10 0 0 1077.68 747.52 154.81 o 11 0 0 3319.34 3287.32 290.20 o 12 0 0 758.05 1085.72 294.13 o 13 0 0 41.18 161.76 280.00 o 14 0 0 149.00 138.11 255.36 o -14 1 0 4034.87 4011.59 365.21 o -13 1 0 5709.31 5627.90 386.81 o -12 1 0 3595.07 3195.67 305.38 o -11 1 0 1082.19 791.44 256.93 o -10 1 0 1129.14 1152.16 181.31 o -9 1 0 87.58 196.29 134.95 o -8 1 0 2117.78 2400.08 172.56 o -7 1 0 13108.58 12621.28 424.54 o -6 1 0 37067.43 35308.30 494.81 o -5 1 0 13397.20 12951.53 282.02 o -4 1 0 4152.53 4205.48 187.53 o -3 1 0 1228.22 2326.78 160.37 o -2 1 0 3352.61 3231.57 157.99 o -1 1 0 2859.73 1975.07 34.25 o 0 1 0 3808.98 3463.85 64.29 o 1 1 0 689.59 1252.11 111.50 o 2 1 0 2218.77 2049.76 162.40 o 3 1 0 71.05 228.90 118.53 o 4 1 0 3329.46 2944.32 192.95 o 5 1 0 336.35 306.01 118.01 o 6 1 0 2.09 53.83 130.35 o 7 1 0 252.21 189.96 108.64 o 8 1 0 411.25 564.41 132.50 o 9 1 0 14.79 122.32 133.87 o 10 1 0 1233.66 1158.90 171.89 o 11 1 0 482.65 708.68 236.88 o 12 1 0 595.12 868.25 287.31 o 13 1 0 707.20 748.80 290.23 o 14 1 0 1295.36 1242.56 347.75 o -14 2 0 256.49 208.55 251.68 o -13 2 0 2046.78 2088.95 288.43 o -12 2 0 4632.89 4218.64 322.73 o -11 2 0 7144.66 7490.56 432.62 o -10 2 0 5005.20 5607.11 289.89 o -9 2 0 1014.67 1138.37 176.28 o -8 2 0 3324.16 3739.48 180.39 o -7 2 0 7.04 66.52 102.42 o -6 2 0 376.16 407.86 101.53 o -5 2 0 172.93 144.47 95.90 o -4 2 0 5345.40 5205.05 142.00 o -3 2 0 2073.39 2810.26 103.47 o -2 2 0 45.21 9.84 123.35 o -1 2 0 12892.01 15545.07 260.33 o 0 2 0 4959.90 4604.31 159.68 o 1 2 0 1741.19 2018.96 125.90 o 2 2 0 1696.41 2022.61 154.76 o 3 2 0 5125.79 6245.58 272.54 o 4 2 0 8899.59 8838.97 374.85 o 5 2 0 11434.71 11030.51 346.12 o 6 2 0 10720.24 9508.00 344.57 o 7 2 0 19275.80 19169.88 346.45 o 8 2 0 20387.19 18918.38 387.03 o 9 2 0 7594.64 7570.15 295.35 o 10 2 0 2977.00 2309.61 255.84 o 11 2 0 1716.84 1542.94 260.90 o 12 2 0 143.47 73.81 220.04 o 13 2 0 21.00 168.16 245.54 o -15 3 0 4.61 124.56 363.18 o -14 3 0 38.62 153.20 244.04 o -13 3 0 66.66 123.79 214.12 o -12 3 0 9.16 141.71 239.34 o -11 3 0 1389.38 1732.51 271.64 o -10 3 0 16.27 55.81 153.07 o -9 3 0 1413.34 1480.74 151.14 o -8 3 0 4544.90 5185.36 212.92 o -7 3 0 12153.16 12098.48 269.60 o -6 3 0 20648.21 22068.89 373.69 o -5 3 0 20472.29 21589.02 350.16 o -4 3 0 13484.83 14346.44 241.00 o -3 3 0 7639.90 7753.88 181.65 o -2 3 0 3099.66 2862.56 108.41 o -1 3 0 25366.23 26575.90 485.41 o 0 3 0 1543.25 1394.31 117.57 o 1 3 0 16384.83 16868.62 345.64 o 2 3 0 27010.26 22677.34 374.90 o 3 3 0 25021.66 23276.96 426.73 o 4 3 0 7772.73 7097.27 270.81 o 5 3 0 8575.00 8515.43 261.63 o 6 3 0 2692.86 2690.84 241.33 o 7 3 0 4.22 87.57 131.56 o 8 3 0 1849.73 1771.46 174.43 o 9 3 0 6302.82 5958.45 306.86 o 10 3 0 6512.56 6407.11 924.32 o 11 3 0 3988.24 3353.69 363.38 o 12 3 0 1790.62 1759.80 268.64 o 13 3 0 988.56 705.74 247.89 o -15 4 0 724.34 726.20 375.50 o -14 4 0 1415.45 1378.94 352.35 o -13 4 0 2361.88 2642.05 359.59 o -12 4 0 3260.14 3155.74 356.30 o -11 4 0 8090.73 8913.30 453.07 o -10 4 0 5304.82 5061.21 354.80 o -9 4 0 933.15 800.25 191.45 o -8 4 0 1468.95 1657.52 155.61 o -7 4 0 4830.18 5347.31 198.79 o -6 4 0 4964.42 5573.76 166.96 o -5 4 0 15431.90 14405.31 262.54 o -4 4 0 33780.01 37250.55 543.14 o -3 4 0 29706.17 31745.07 466.48 o -2 4 0 18575.00 18896.49 296.08 o -1 4 0 1577.44 1768.27 158.89 o 0 4 0 10024.44 7972.79 253.50 o 1 4 0 1815.12 2352.78 156.13 o 2 4 0 131.17 227.72 125.38 o 3 4 0 14688.72 14468.69 329.82 o 4 4 0 14580.68 15065.73 389.58 o 5 4 0 6315.50 6767.20 279.30 o 6 4 0 829.24 882.03 169.19 o 7 4 0 2121.18 1852.71 175.97 o 8 4 0 101.21 361.35 165.94 o 9 4 0 36.85 59.12 170.00 o 10 4 0 56.91 234.19 189.74 o 11 4 0 5.87 83.07 213.13 o 12 4 0 277.74 411.46 236.58 o -15 5 0 1315.87 1038.13 448.35 o -14 5 0 369.49 1.89 336.20 o -13 5 0 42.30 217.35 267.58 o -12 5 0 170.60 142.51 240.11 o -11 5 0 4696.22 4206.75 362.88 o -10 5 0 10733.59 10572.20 443.52 o -9 5 0 14077.24 14613.89 482.55 o -8 5 0 6677.01 7188.88 211.75 o -7 5 0 6260.94 5778.52 186.91 o -6 5 0 8294.80 9124.21 235.71 o -5 5 0 3740.02 4015.74 185.14 o -4 5 0 598.05 462.98 125.87 o -3 5 0 5116.54 5312.54 214.23 o -2 5 0 10.20 24.28 105.77 o -1 5 0 531.19 759.78 132.41 o 0 5 0 1115.05 1033.91 154.77 o 1 5 0 543.03 399.84 217.08 o 2 5 0 1334.67 1494.50 191.60 o 3 5 0 2771.57 3048.59 218.72 o 4 5 0 1504.19 1431.14 182.27 o 5 5 0 713.04 609.53 168.43 o 6 5 0 529.05 248.06 170.14 o 7 5 0 322.90 465.15 194.25 o 8 5 0 2508.39 2561.04 231.63 o 9 5 0 3566.38 3445.41 257.92 o 10 5 0 5576.72 5053.25 309.63 o 11 5 0 2097.15 2119.82 287.74 o 12 5 0 894.87 766.71 267.11 o -15 6 0 1553.68 1880.94 676.42 o -14 6 0 1050.55 1642.39 417.63 o -13 6 0 438.01 182.77 323.57 o -12 6 0 82.94 15.97 242.59 o -11 6 0 1.54 124.54 231.50 o -10 6 0 120.20 287.16 219.89 o -9 6 0 718.95 912.15 164.45 o -8 6 0 448.99 514.37 126.46 o -7 6 0 4264.39 4668.42 196.95 o -6 6 0 5851.10 6274.04 226.84 o -5 6 0 1898.72 2228.20 191.31 o -4 6 0 4159.03 4478.63 182.93 o -3 6 0 3663.62 4023.47 189.99 o -2 6 0 9373.55 9134.81 308.42 o -1 6 0 2378.56 2247.90 154.67 o 0 6 0 1531.63 1637.44 177.33 o 1 6 0 245.35 218.89 138.31 o 2 6 0 6306.07 6300.73 247.53 o 3 6 0 7808.61 7573.15 303.00 o 4 6 0 21236.13 21418.38 469.69 o 5 6 0 13679.23 14339.59 407.11 o 6 6 0 7105.65 6912.82 388.49 o 7 6 0 1327.21 1362.66 223.08 o 8 6 0 123.36 229.23 182.09 o 9 6 0 301.56 412.53 207.52 o 10 6 0 534.41 575.50 221.62 o 11 6 0 2718.27 2552.51 279.40 o -14 7 0 135.28 188.61 373.93 o -13 7 0 1324.58 914.08 391.25 o -12 7 0 3330.06 4030.15 476.88 o -11 7 0 4028.51 4477.20 488.60 o -10 7 0 4592.46 4723.06 344.08 o -9 7 0 2996.92 3491.65 238.38 o -8 7 0 5950.20 6128.70 276.57 o -7 7 0 2182.05 2512.34 162.12 o -6 7 0 159.80 198.40 130.70 o -5 7 0 1776.24 1865.72 203.41 o -4 7 0 9408.41 9682.50 272.72 o -3 7 0 30897.32 34197.43 552.20 o -2 7 0 38542.39 38157.50 680.03 o -1 7 0 29810.44 29326.73 565.90 o 0 7 0 20029.59 19317.59 385.63 o 1 7 0 4721.21 4953.59 266.21 o 2 7 0 1986.48 1948.57 194.14 o 3 7 0 1357.32 1423.50 206.39 o 4 7 0 272.26 401.95 179.73 o 5 7 0 3836.30 3899.50 277.08 o 6 7 0 7033.70 6755.83 344.48 o 7 7 0 1471.77 979.93 238.00 o 8 7 0 428.02 487.60 206.73 o 9 7 0 628.91 606.80 222.41 o 10 7 0 64.35 173.16 224.28 o 11 7 0 0.02 35.98 229.75 o -14 8 0 3888.65 4120.18 545.85 o -13 8 0 2855.75 3185.85 493.18 o -12 8 0 461.37 714.97 349.49 o -11 8 0 21.38 0.94 281.49 o -10 8 0 134.69 16.06 273.90 o -9 8 0 4022.12 4493.25 371.38 o -8 8 0 9489.38 10176.48 338.15 o -7 8 0 11194.57 11508.94 333.30 o -6 8 0 9554.25 9789.90 364.81 o -5 8 0 2646.16 2578.19 193.71 o -4 8 0 3088.32 2800.14 185.27 o -3 8 0 3397.36 3480.30 194.62 o -2 8 0 23.16 84.38 129.16 o -1 8 0 2347.71 2248.97 206.22 o 0 8 0 4482.17 4839.54 283.83 o 1 8 0 190.23 275.77 156.76 o 2 8 0 188.63 196.33 168.50 o 3 8 0 189.36 213.62 175.02 o 4 8 0 0.63 100.27 184.80 o 5 8 0 144.10 507.52 211.46 o 6 8 0 1045.35 877.78 232.36 o 7 8 0 6.99 3.78 208.60 o 8 8 0 113.60 307.46 252.27 o 9 8 0 443.40 288.66 217.33 o 10 8 0 308.74 493.46 234.01 o -14 9 0 2544.56 3201.31 526.86 o -13 9 0 3860.83 3073.56 481.93 o -12 9 0 1835.22 1738.98 467.16 o -11 9 0 1255.79 1493.38 396.83 o -10 9 0 1149.51 931.77 343.75 o -9 9 0 2036.30 2389.12 403.25 o -8 9 0 491.21 349.26 168.32 o -7 9 0 344.76 297.58 155.44 o -6 9 0 851.73 407.29 172.36 o -5 9 0 39.43 91.01 148.70 o -4 9 0 317.02 322.96 141.79 o -3 9 0 1246.06 1228.26 169.01 o -2 9 0 188.35 132.89 140.82 o -1 9 0 1836.88 1595.11 183.34 o 0 9 0 2110.21 2243.33 220.75 o 1 9 0 5.74 50.75 176.72 o 2 9 0 560.25 719.90 209.18 o 3 9 0 2831.77 2624.67 264.55 o 4 9 0 4825.44 4468.45 362.71 o 5 9 0 7023.12 7114.78 386.27 o 6 9 0 6334.78 6721.29 379.93 o 7 9 0 5359.28 5809.85 395.20 o 8 9 0 4839.13 4824.96 367.97 o 9 9 0 1275.81 1339.87 273.00 o -13 10 0 98.34 29.29 357.79 o -12 10 0 24.46 333.98 359.24 o -11 10 0 134.17 333.01 350.71 o -10 10 0 1818.77 1792.37 395.83 o -9 10 0 5478.72 5626.93 651.86 o -8 10 0 5309.88 5461.13 363.09 o -7 10 0 5574.96 5706.23 752.94 o -6 10 0 8045.58 8069.55 394.97 o -5 10 0 4094.29 3980.02 242.18 o -4 10 0 124.42 186.49 167.97 o -3 10 0 2188.58 2111.40 200.68 o -2 10 0 3748.52 3733.54 238.12 o -1 10 0 10797.92 10636.07 351.02 o 0 10 0 7922.17 9473.57 507.39 o 1 10 0 10735.40 10837.13 404.79 o 2 10 0 10978.63 11578.53 447.16 o 3 10 0 3982.42 4183.44 319.58 o 4 10 0 839.78 624.93 231.77 o 5 10 0 61.94 150.70 230.36 o 6 10 0 34.54 125.23 247.33 o 7 10 0 950.46 1068.07 295.23 o 8 10 0 2045.45 2199.35 296.57 o -13 11 0 3574.49 3233.65 555.50 o -12 11 0 3933.75 4147.62 576.28 o -11 11 0 2960.47 2330.88 451.29 o -10 11 0 328.39 608.58 361.24 o -9 11 0 28.16 173.41 318.03 o -8 11 0 363.97 523.88 318.51 o -7 11 0 3100.85 3131.45 598.17 o -6 11 0 6131.64 5673.03 401.56 o -5 11 0 8691.21 8003.51 349.35 o -4 11 0 8077.57 8152.93 457.07 o -3 11 0 4710.20 4527.38 296.44 o -2 11 0 2322.85 2213.68 226.28 o -1 11 0 986.11 1100.31 236.91 o 0 11 0 348.58 256.56 184.42 o 1 11 0 979.06 1190.09 243.28 o 2 11 0 1199.09 1376.34 253.73 o 3 11 0 908.67 972.76 252.76 o 4 11 0 222.47 560.27 259.16 o 5 11 0 589.21 431.09 262.53 o 6 11 0 773.91 700.91 282.96 o 7 11 0 135.54 279.85 287.14 o -12 12 0 1512.14 1866.73 460.92 o -11 12 0 3954.00 3460.28 513.62 o -10 12 0 2754.41 2162.72 449.16 o -9 12 0 1558.62 1712.36 403.11 o -8 12 0 629.05 831.39 375.61 o -7 12 0 641.08 482.59 260.85 o -6 12 0 173.88 145.49 245.43 o -5 12 0 141.48 181.97 258.82 o -4 12 0 436.43 291.48 212.79 o -3 12 0 37.39 103.91 196.10 o -2 12 0 394.91 362.50 200.41 o -1 12 0 475.92 285.45 200.70 o 0 12 0 33.42 74.06 194.77 o 1 12 0 424.12 643.29 223.03 o 2 12 0 1939.88 1793.65 282.50 o 3 12 0 1120.33 945.59 268.19 o 4 12 0 16.43 143.76 253.34 o 5 12 0 194.45 571.56 291.26 o 6 12 0 828.75 678.93 311.90 o -11 13 0 13.04 0.94 360.21 o -10 13 0 0.07 34.82 375.75 o -9 13 0 438.66 80.01 344.04 o -8 13 0 1238.67 1731.34 416.53 o -7 13 0 1858.74 2241.87 1086.90 o -6 13 0 1531.15 1437.86 315.88 o -5 13 0 2270.60 2561.46 351.60 o -4 13 0 3529.51 3040.28 355.59 o -3 13 0 1850.87 1959.68 274.89 o -2 13 0 2.02 104.62 219.15 o -1 13 0 394.32 475.47 252.40 o 0 13 0 1674.77 1914.24 261.78 o 1 13 0 3522.62 3727.18 303.68 o 2 13 0 4524.83 4236.20 373.57 o 3 13 0 4317.81 4537.34 383.24 o 4 13 0 3585.28 3552.96 373.21 o -10 14 0 2968.74 2112.62 481.19 o -9 14 0 2053.78 1879.28 568.72 o -8 14 0 753.51 186.55 374.42 o -7 14 0 3.81 45.62 355.57 o -6 14 0 465.61 482.46 301.43 o -5 14 0 2734.18 2191.53 373.15 o -4 14 0 4372.89 3442.97 380.57 o -3 14 0 5011.75 4218.17 402.42 o -2 14 0 4666.11 4370.94 357.42 o -1 14 0 3657.10 4280.65 403.62 o 0 14 0 1629.31 1515.79 340.96 o 1 14 0 1010.96 563.23 284.29 o 2 14 0 34.08 213.74 278.81 o 3 14 0 87.45 2.83 516.76 o -8 15 0 2584.48 2128.37 1231.44 o -7 15 0 1251.69 1184.86 428.61 o -6 15 0 833.19 625.56 401.74 o -5 15 0 572.40 167.26 303.70 o -4 15 0 385.97 575.21 327.60 o -3 15 0 0.02 34.22 375.55 o -2 15 0 283.11 18.19 373.53 o -1 15 0 103.09 99.55 369.39 o 0 15 0 37.30 478.08 331.31 o 4 -16 1 652.01 410.01 543.21 o -1 -15 1 98.54 526.34 332.49 o 0 -15 1 4.33 20.64 279.75 o 1 -15 1 66.34 73.84 290.14 o 2 -15 1 19.99 216.46 358.74 o 3 -15 1 723.50 551.33 308.09 o 4 -15 1 2098.42 2253.92 395.65 o 5 -15 1 2333.30 2450.18 384.20 o 6 -15 1 3174.02 3741.88 524.81 o 7 -15 1 3464.51 3300.95 506.51 o 8 -15 1 2101.83 2461.92 487.66 o -3 -14 1 87.84 121.46 273.91 o -2 -14 1 1344.48 1655.97 399.39 o -1 -14 1 2773.96 3131.72 393.67 o 0 -14 1 3355.64 3745.09 399.26 o 1 -14 1 4370.60 4320.25 376.50 o 2 -14 1 3764.50 3834.86 323.01 o 3 -14 1 2502.51 2704.91 290.59 o 4 -14 1 860.20 905.69 302.91 o 5 -14 1 145.76 150.46 281.75 o 6 -14 1 550.46 302.32 345.33 o 7 -14 1 1264.67 1331.32 404.30 o 8 -14 1 2988.60 2223.84 741.61 o 9 -14 1 3792.52 4132.90 846.00 o 10 -14 1 2564.03 1716.71 462.97 o -5 -13 1 3087.86 3608.76 384.31 o -4 -13 1 4739.45 4727.29 391.41 o -3 -13 1 2570.96 2952.43 408.29 o -2 -13 1 1387.75 1290.85 284.64 o -1 -13 1 486.30 266.51 249.58 o 0 -13 1 115.99 89.87 209.69 o 1 -13 1 1151.32 1475.11 259.00 o 2 -13 1 3193.60 3219.82 344.17 o 3 -13 1 5858.54 6135.86 519.63 o 4 -13 1 4439.21 3885.92 301.94 o 5 -13 1 3068.54 3677.48 526.25 o 6 -13 1 2169.30 2119.98 330.88 o 7 -13 1 2221.84 2318.15 433.60 o 8 -13 1 198.38 364.08 395.84 o 9 -13 1 5.74 206.69 339.90 o 10 -13 1 6.41 57.15 339.56 o 11 -13 1 29.37 39.81 354.85 o -6 -12 1 151.84 41.74 269.40 o -5 -12 1 1.89 94.42 257.25 o -4 -12 1 812.08 608.47 263.48 o -3 -12 1 1391.09 2005.20 297.43 o -2 -12 1 1039.01 747.65 253.40 o -1 -12 1 8.35 14.17 223.02 o 0 -12 1 9.14 110.03 224.32 o 1 -12 1 420.19 456.62 200.40 o 2 -12 1 50.05 48.20 187.55 o 3 -12 1 184.73 269.64 202.36 o 4 -12 1 369.67 144.85 186.14 o 5 -12 1 167.32 457.89 254.17 o 6 -12 1 1822.97 1353.99 296.23 o 7 -12 1 1130.05 797.40 348.03 o 8 -12 1 941.83 1727.81 400.14 o 9 -12 1 1733.05 2000.36 412.33 o 10 -12 1 2238.26 1782.71 421.31 o 11 -12 1 1791.12 1615.00 854.03 o 12 -12 1 64.26 7.56 359.59 o -7 -11 1 349.17 263.19 265.89 o -6 -11 1 231.14 391.61 256.36 o -5 -11 1 28.72 131.54 251.17 o -4 -11 1 244.46 79.04 225.13 o -3 -11 1 354.42 332.12 230.72 o -2 -11 1 70.82 105.55 218.38 o -1 -11 1 819.02 707.22 232.32 o 0 -11 1 3071.17 3157.40 283.46 o 1 -11 1 3428.08 3666.06 296.40 o 2 -11 1 6154.96 6634.93 309.81 o 3 -11 1 10262.04 10880.62 556.94 o 4 -11 1 13039.27 14146.58 478.07 o 5 -11 1 6439.77 6470.14 421.00 o 6 -11 1 1739.35 1687.92 213.99 o 7 -11 1 65.09 32.47 178.40 o 8 -11 1 1181.99 1599.43 377.69 o 9 -11 1 1825.26 1877.45 671.22 o 10 -11 1 5201.28 4434.30 1132.72 o 11 -11 1 8106.46 7349.06 625.55 o 12 -11 1 5557.62 5447.70 586.53 o 13 -11 1 3432.11 3608.08 546.90 o -8 -10 1 706.14 778.86 287.41 o -7 -10 1 5.75 125.72 246.41 o -6 -10 1 326.93 355.92 248.81 o -5 -10 1 2195.73 2051.16 279.04 o -4 -10 1 5241.36 5051.06 352.01 o -3 -10 1 10794.07 10951.78 428.94 o -2 -10 1 14934.83 14638.36 438.57 o -1 -10 1 7492.72 7317.63 616.07 o 0 -10 1 5195.64 5239.60 313.76 o 1 -10 1 1631.07 1958.25 262.76 o 2 -10 1 102.42 124.06 156.96 o 3 -10 1 677.72 814.27 169.56 o 4 -10 1 3766.59 3895.39 225.10 o 5 -10 1 7545.70 7672.55 349.39 o 6 -10 1 9793.94 10533.07 457.74 o 7 -10 1 3767.36 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