# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' I C c R = 0.02' _shelx_refln_list_code 4 _shelx_F_calc_maximum 568.02 _exptl_crystal_F_000 2224.00 _reflns_d_resolution_high 0.7474 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' _cell_length_a 16.8600 _cell_length_b 16.6300 _cell_length_c 16.2200 _cell_angle_alpha 90.000 _cell_angle_beta 105.410 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -21 11.22 47.54 61.35 o 3 1 -21 83.09 136.11 66.72 o 5 1 -21 126.71 200.15 72.08 o 9 1 -21 49.49 17.25 57.90 o 2 2 -21 51.23 90.01 43.58 o 4 2 -21 20.91 116.56 64.80 o 6 2 -21 31.83 29.14 58.66 o 8 2 -21 110.74 159.89 69.78 o 3 3 -21 514.62 434.57 53.25 o 5 3 -21 716.74 750.74 107.74 o 7 3 -21 685.82 663.32 99.69 o 9 3 -21 276.63 218.55 73.62 o 4 4 -21 7.11 15.72 59.81 o 6 4 -21 77.76 144.55 67.87 o 8 4 -21 113.24 34.51 58.28 o 5 5 -21 1103.25 1423.26 142.25 o 7 5 -21 819.43 915.23 118.86 o 0 0 -20 1171.82 1519.88 148.00 o 2 0 -20 501.05 542.54 103.91 o 4 0 -20 8.53 -56.36 56.36 o 10 0 -20 1720.65 1847.32 143.40 o 12 0 -20 1564.01 1694.34 138.42 o -1 1 -20 937.87 967.36 91.46 o 1 1 -20 1211.74 1212.12 74.31 o 3 1 -20 2317.33 2546.63 105.57 o 5 1 -20 3086.04 3084.24 176.76 o 7 1 -20 3306.26 3679.69 192.09 o 9 1 -20 2990.22 3221.50 180.21 o 11 1 -20 1618.83 1786.16 101.51 o 13 1 -20 1399.13 1435.12 131.32 o 0 2 -20 642.44 692.76 61.19 o 2 2 -20 327.63 381.18 50.81 o 4 2 -20 31.55 30.67 59.05 o 6 2 -20 132.87 124.23 69.78 o 8 2 -20 228.50 178.67 70.93 o 10 2 -20 714.44 691.40 67.88 o 12 2 -20 715.08 844.29 109.28 o -1 3 -20 721.69 550.59 106.97 o 1 3 -20 1103.67 960.38 68.38 o 3 3 -20 1039.65 1152.92 71.62 o 5 3 -20 1411.57 1487.67 135.73 o 7 3 -20 1514.35 1344.27 120.39 o 9 3 -20 1253.49 1491.89 129.98 o 11 3 -20 1108.67 1252.14 86.74 o 13 3 -20 1068.38 1060.16 121.16 o 0 4 -20 336.07 353.11 52.22 o 2 4 -20 366.54 309.12 47.00 o 4 4 -20 128.49 130.76 41.15 o 6 4 -20 311.48 318.24 81.29 o 8 4 -20 294.61 428.66 86.27 o 10 4 -20 252.41 189.41 69.40 o 12 4 -20 832.42 867.04 76.85 o 1 5 -20 448.18 559.61 68.44 o 3 5 -20 291.89 354.28 89.72 o 5 5 -20 307.66 292.55 80.14 o 7 5 -20 381.21 382.65 87.80 o 9 5 -20 144.36 157.20 66.72 o 11 5 -20 679.01 672.87 116.75 o 0 6 -20 281.45 242.32 78.60 o 2 6 -20 410.35 506.12 101.22 o 4 6 -20 841.80 815.92 111.96 o 6 6 -20 786.00 829.34 111.19 o 8 6 -20 479.41 592.77 98.92 o 10 6 -20 652.38 687.86 103.91 o 1 7 -20 228.94 263.03 84.74 o 3 7 -20 245.61 240.79 80.90 o 5 7 -20 117.81 216.25 79.75 o 7 7 -20 50.08 29.52 65.57 o 9 7 -20 145.22 170.24 76.30 o 4 8 -20 1031.41 1165.60 135.73 o 6 8 -20 1108.71 1303.25 136.88 o 8 8 -20 1068.65 1114.61 128.06 o -3 1 -19 7.77 35.23 34.51 o -1 1 -19 37.14 -21.02 30.98 o 1 1 -19 51.03 99.34 33.92 o 3 1 -19 578.54 579.68 52.99 o 5 1 -19 721.08 764.98 152.22 o 7 1 -19 117.65 203.60 62.88 o 9 1 -19 59.49 52.64 54.64 o 11 1 -19 260.43 216.46 49.19 o 13 1 -19 8.16 19.80 37.95 o 15 1 -19 56.51 7.39 117.33 o -2 2 -19 336.01 346.20 49.94 o 0 2 -19 137.28 122.46 37.78 o 2 2 -19 132.51 134.31 38.60 o 4 2 -19 52.86 54.53 32.99 o 6 2 -19 418.77 387.64 79.37 o 8 2 -19 96.75 159.65 42.56 o 10 2 -19 178.94 116.32 39.85 o 12 2 -19 816.23 761.09 99.69 o 14 2 -19 237.51 171.64 50.98 o -3 3 -19 280.17 208.58 86.65 o -1 3 -19 280.50 284.93 47.22 o 1 3 -19 563.23 539.56 53.91 o 3 3 -19 1841.93 1891.53 82.80 o 5 3 -19 2223.41 2530.58 161.80 o 7 3 -19 589.59 657.95 92.02 o 9 3 -19 562.07 580.26 61.27 o 11 3 -19 1085.64 1137.96 80.38 o 13 3 -19 366.56 357.09 57.23 o 15 3 -19 383.67 412.31 68.44 o -2 4 -19 424.76 579.97 59.98 o 0 4 -19 309.91 313.94 48.50 o 2 4 -19 191.53 199.38 73.62 o 4 4 -19 38.76 11.50 57.90 o 6 4 -19 259.68 254.98 74.38 o 8 4 -19 218.54 152.22 64.80 o 10 4 -19 299.09 361.18 54.49 o 12 4 -19 910.18 908.14 78.03 o 14 4 -19 1257.15 1228.46 89.55 o -1 5 -19 720.46 748.82 112.34 o 1 5 -19 1224.86 1370.35 138.03 o 3 5 -19 1677.71 1719.26 139.95 o 5 5 -19 1947.50 2152.53 152.22 o 7 5 -19 1971.08 1965.03 147.62 o 9 5 -19 969.12 925.96 105.44 o 11 5 -19 972.14 1060.16 82.15 o 13 5 -19 1384.86 1584.16 99.71 o -2 6 -19 232.48 282.96 83.20 o 0 6 -19 82.77 143.78 70.93 o 2 6 -19 42.99 101.22 67.10 o 4 6 -19 327.67 419.08 90.87 o 6 6 -19 201.61 297.53 76.30 o 8 6 -19 252.73 111.19 61.73 o 10 6 -19 366.17 297.03 55.71 o 12 6 -19 525.18 592.28 71.71 o -1 7 -19 830.89 796.75 114.64 o 1 7 -19 1114.48 1026.81 88.77 o 3 7 -19 1286.47 1309.00 131.90 o 5 7 -19 1212.14 1559.76 141.48 o 7 7 -19 1812.58 2016.03 151.07 o 9 7 -19 992.20 975.42 113.88 o 11 7 -19 899.88 901.56 79.84 o 13 7 -19 854.82 891.84 115.41 o 0 8 -19 325.28 224.53 61.04 o 2 8 -19 150.94 100.07 72.47 o 4 8 -19 8.85 -45.24 61.73 o 6 8 -19 222.18 216.63 82.44 o 8 8 -19 476.20 456.27 93.55 o 10 8 -19 220.04 258.43 83.59 o 12 8 -19 349.94 226.99 85.12 o 1 9 -19 548.37 516.85 104.29 o 3 9 -19 832.81 712.01 113.88 o 5 9 -19 1254.05 1154.48 129.98 o 7 9 -19 1260.89 1407.92 134.96 o 9 9 -19 730.55 700.51 110.43 o 2 10 -19 493.42 584.33 110.43 o 4 10 -19 1156.62 1378.40 138.80 o 6 10 -19 1054.57 1054.41 129.21 o 8 10 -19 762.37 726.20 113.11 o -4 0 -18 1784.66 1774.47 166.40 o -2 0 -18 1373.43 1508.77 95.60 o 0 0 -18 1297.61 1229.36 84.60 o 2 0 -18 118.51 66.50 85.31 o 4 0 -18 171.17 163.42 37.19 o 6 0 -18 406.63 368.47 75.53 o 8 0 -18 2013.96 1777.92 126.53 o 10 0 -18 2210.34 2406.73 148.00 o 12 0 -18 2287.32 2409.80 159.12 o 14 0 -18 1018.59 1026.80 116.56 o 16 0 -18 1473.07 1564.36 138.03 o -5 1 -18 1170.79 1131.19 76.98 o -3 1 -18 1148.47 1105.28 89.08 o -1 1 -18 3273.34 3239.91 131.13 o 1 1 -18 5263.97 5590.70 223.86 o 3 1 -18 6085.58 5735.53 143.25 o 5 1 -18 7624.83 7364.96 190.23 o 7 1 -18 3886.54 4148.03 134.87 o 9 1 -18 1722.39 1851.10 144.36 o 11 1 -18 2179.58 2306.47 104.06 o 13 1 -18 1382.79 1459.59 122.50 o 15 1 -18 577.08 522.65 66.56 o -4 2 -18 926.12 920.50 82.00 o -2 2 -18 502.14 537.53 55.81 o 0 2 -18 366.51 341.80 47.48 o 2 2 -18 292.50 347.87 47.45 o 4 2 -18 138.35 8.37 35.05 o 6 2 -18 386.35 325.52 76.30 o 8 2 -18 1131.31 1051.50 73.20 o 10 2 -18 2239.94 2288.45 109.47 o 12 2 -18 2152.00 2346.27 109.85 o 14 2 -18 1138.95 1072.56 82.48 o 16 2 -18 1650.64 1698.96 127.30 o -3 3 -18 1179.63 1032.59 70.38 o -1 3 -18 1422.62 1504.53 81.31 o 1 3 -18 1775.56 1765.64 98.28 o 3 3 -18 2282.46 2361.65 115.22 o 5 3 -18 1942.96 2047.47 141.87 o 7 3 -18 3365.74 3619.64 127.28 o 9 3 -18 2531.15 2636.98 143.40 o 11 3 -18 692.09 702.69 82.24 o 13 3 -18 1429.51 1489.80 122.12 o 15 3 -18 683.70 879.29 76.09 o -4 4 -18 506.40 545.58 59.44 o -2 4 -18 178.40 154.79 42.89 o 0 4 -18 87.32 107.74 67.48 o 2 4 -18 566.82 513.02 89.72 o 4 4 -18 322.69 253.44 67.48 o 6 4 -18 284.59 305.59 72.85 o 8 4 -18 1460.76 1457.39 135.73 o 10 4 -18 1069.33 1136.68 91.83 o 12 4 -18 853.83 771.58 70.15 o 14 4 -18 1642.80 1767.13 98.97 o 16 4 -18 1195.82 1317.65 91.00 o -3 5 -18 618.30 528.71 69.84 o -1 5 -18 403.69 407.58 90.87 o 1 5 -18 772.30 795.22 106.59 o 3 5 -18 560.75 700.89 100.07 o 5 5 -18 489.56 456.65 85.12 o 7 5 -18 999.20 1002.65 105.82 o 9 5 -18 712.98 793.59 114.07 o 11 5 -18 586.88 646.65 66.17 o 13 5 -18 1811.12 2089.20 107.46 o 15 5 -18 952.27 1016.96 94.90 o -2 6 -18 587.64 730.42 110.43 o 0 6 -18 644.76 693.99 102.37 o 2 6 -18 1351.52 1409.86 93.78 o 4 6 -18 1479.10 1836.20 141.87 o 6 6 -18 967.40 1035.24 111.96 o 8 6 -18 914.98 838.54 103.14 o 10 6 -18 1404.81 1686.29 96.23 o 12 6 -18 442.49 394.66 81.86 o 14 6 -18 584.76 553.74 94.32 o -3 7 -18 133.72 148.38 76.30 o -1 7 -18 162.56 107.36 64.80 o 1 7 -18 134.49 108.67 50.43 o 3 7 -18 15.06 41.41 63.26 o 5 7 -18 314.23 304.82 78.98 o 7 7 -18 443.71 483.49 87.42 o 9 7 -18 478.71 386.47 58.24 o 11 7 -18 1518.16 1386.81 89.60 o 13 7 -18 1040.48 1079.86 83.84 o -2 8 -18 655.59 710.48 113.49 o 0 8 -18 1313.28 1198.96 133.05 o 2 8 -18 2201.83 2442.01 169.86 o 4 8 -18 2289.00 2185.88 159.50 o 6 8 -18 1890.37 1869.56 146.08 o 8 8 -18 535.87 641.85 97.77 o 10 8 -18 1338.67 1339.12 89.77 o 12 8 -18 800.13 847.93 79.10 o 14 8 -18 65.75 90.25 51.91 o -1 9 -18 323.11 432.12 93.94 o 1 9 -18 164.46 186.73 55.58 o 3 9 -18 133.57 54.06 70.17 o 5 9 -18 103.80 82.44 61.73 o 7 9 -18 858.28 1032.17 116.94 o 9 9 -18 635.73 618.08 99.31 o 11 9 -18 938.23 1111.99 87.69 o 13 9 -18 861.55 1000.03 125.57 o 0 10 -18 525.83 498.19 72.31 o 2 10 -18 1040.12 947.82 122.31 o 4 10 -18 1695.06 1957.37 157.59 o 6 10 -18 1402.89 1317.44 131.90 o 8 10 -18 787.85 644.15 106.21 o 10 10 -18 776.47 880.34 115.41 o 1 11 -18 181.53 239.25 86.65 o 5 11 -18 202.57 263.79 85.50 o 7 11 -18 6.73 -10.35 55.98 o 9 11 -18 382.39 432.12 96.62 o 4 12 -18 274.88 279.51 84.35 o 6 12 -18 568.68 547.91 105.44 o -5 1 -17 290.63 269.16 47.55 o -3 1 -17 159.88 118.95 36.85 o -1 1 -17 302.48 253.27 40.25 o 1 1 -17 442.27 466.83 40.16 o 3 1 -17 487.90 546.23 40.03 o 5 1 -17 310.73 358.26 32.93 o 7 1 -17 15.53 20.52 23.06 o 9 1 -17 240.94 263.24 45.63 o 11 1 -17 615.90 621.22 58.15 o 13 1 -17 142.30 104.73 42.86 o 15 1 -17 215.38 206.06 50.16 o 17 1 -17 85.06 116.37 48.80 o -6 2 -17 776.16 813.28 65.76 o -4 2 -17 169.49 168.48 39.95 o -2 2 -17 194.98 174.78 38.71 o 0 2 -17 116.45 90.53 34.31 o 2 2 -17 519.15 573.79 59.01 o 4 2 -17 908.86 978.00 55.52 o 6 2 -17 1651.01 1719.24 84.14 o 8 2 -17 702.28 747.68 58.91 o 10 2 -17 188.93 214.96 43.29 o 12 2 -17 758.09 679.34 63.19 o 14 2 -17 731.53 869.81 83.39 o 16 2 -17 42.14 75.26 41.11 o -5 3 -17 1160.41 1156.61 73.55 o -3 3 -17 678.06 712.55 60.07 o -1 3 -17 1235.43 1124.12 81.18 o 1 3 -17 3408.88 3507.92 199.76 o 3 3 -17 3955.99 4131.75 207.43 o 5 3 -17 1884.71 2159.81 137.65 o 7 3 -17 501.26 523.78 52.82 o 9 3 -17 707.26 692.78 67.29 o 11 3 -17 1463.01 1501.25 85.79 o 13 3 -17 232.74 252.63 48.62 o 15 3 -17 1023.03 1023.84 80.90 o 17 3 -17 472.60 470.81 66.61 o -6 4 -17 720.91 807.12 67.31 o -4 4 -17 297.41 354.48 49.90 o -2 4 -17 299.95 291.40 81.67 o 0 4 -17 815.59 867.68 105.44 o 2 4 -17 480.71 412.18 80.14 o 4 4 -17 628.15 469.69 78.98 o 6 4 -17 1112.06 983.09 102.37 o 8 4 -17 1329.18 1347.13 78.98 o 10 4 -17 831.08 765.66 65.82 o 12 4 -17 837.58 905.36 73.13 o 14 4 -17 1045.52 1148.27 80.13 o 16 4 -17 794.09 682.72 70.51 o -5 5 -17 1403.01 1370.46 80.24 o -3 5 -17 849.51 841.23 116.18 o -1 5 -17 1170.89 1168.67 128.06 o 1 5 -17 3041.75 3141.75 188.64 o 3 5 -17 3748.94 3999.80 148.58 o 5 5 -17 2172.85 2636.02 154.52 o 7 5 -17 2165.14 2254.17 123.85 o 9 5 -17 3274.68 3416.72 125.46 o 11 5 -17 1704.21 1724.06 93.26 o 13 5 -17 362.71 399.17 58.02 o 15 5 -17 72.74 98.16 46.36 o 17 5 -17 270.23 306.47 59.72 o -4 6 -17 322.95 376.14 89.72 o -2 6 -17 97.71 199.00 77.07 o 0 6 -17 148.22 142.25 68.63 o 2 6 -17 344.07 353.55 57.13 o 4 6 -17 338.55 560.56 87.42 o 6 6 -17 311.77 399.52 78.22 o 8 6 -17 1136.68 1116.66 75.37 o 10 6 -17 2594.66 2903.98 119.83 o 12 6 -17 1841.82 2029.21 104.51 o 14 6 -17 1668.25 1744.78 138.80 o 16 6 -17 2450.00 2625.04 125.92 o -5 7 -17 864.72 939.00 125.76 o -3 7 -17 1096.52 1103.87 129.98 o -1 7 -17 1886.58 1811.67 153.75 o 1 7 -17 1790.07 1765.27 146.85 o 3 7 -17 2553.98 2751.43 166.40 o 5 7 -17 2046.71 2190.87 151.45 o 7 7 -17 1835.96 2035.97 141.10 o 9 7 -17 2522.83 2851.50 118.69 o 11 7 -17 798.04 804.11 73.20 o 13 7 -17 746.06 744.72 73.53 o 15 7 -17 639.47 607.37 70.16 o -4 8 -17 241.27 272.23 87.42 o -2 8 -17 625.87 716.23 107.74 o 0 8 -17 321.43 401.44 87.80 o 2 8 -17 6.52 -14.69 36.82 o 4 8 -17 109.68 114.64 68.25 o 6 8 -17 714.61 651.43 95.09 o 8 8 -17 1059.28 961.24 109.28 o 10 8 -17 423.87 481.10 63.31 o 12 8 -17 265.83 215.39 54.49 o 14 8 -17 1171.45 1313.02 92.15 o -3 9 -17 1627.19 1878.00 165.25 o -1 9 -17 1569.75 1958.52 161.42 o 1 9 -17 1234.28 1373.04 95.16 o 3 9 -17 950.14 1025.65 114.64 o 5 9 -17 1395.17 1557.84 129.21 o 7 9 -17 1395.46 1354.63 127.30 o 9 9 -17 606.59 691.55 70.22 o 11 9 -17 303.13 276.93 106.21 o 13 9 -17 451.13 361.76 65.92 o -2 10 -17 1637.24 1666.35 157.59 o 0 10 -17 2013.70 2164.43 130.36 o 2 10 -17 717.49 785.25 107.36 o 4 10 -17 577.61 616.54 99.69 o 6 10 -17 1155.67 1200.11 125.00 o 8 10 -17 721.33 541.77 95.47 o 10 10 -17 289.50 299.08 57.85 o 12 10 -17 419.20 288.08 191.33 o -1 11 -17 577.18 711.88 121.74 o 1 11 -17 376.64 405.12 66.29 o 3 11 -17 208.83 180.21 75.15 o 5 11 -17 767.62 854.65 110.81 o 7 11 -17 690.19 516.85 94.71 o 9 11 -17 513.05 309.42 84.74 o 11 11 -17 321.05 263.30 62.31 o 0 12 -17 1843.78 1911.47 113.48 o 2 12 -17 2237.58 2409.42 172.92 o 4 12 -17 2638.86 2976.88 191.33 o 6 12 -17 1513.00 1540.97 139.57 o 8 12 -17 647.21 616.54 102.37 o 10 12 -17 600.64 707.41 110.43 o 1 13 -17 42.48 3.45 67.10 o 3 13 -17 102.77 192.86 76.30 o 5 13 -17 370.81 300.99 86.27 o 7 13 -17 348.35 532.19 102.76 o -8 0 -16 1095.17 1080.48 139.95 o -6 0 -16 2039.83 1983.82 165.64 o -4 0 -16 1480.02 1449.68 91.65 o -2 0 -16 958.07 933.94 72.79 o 0 0 -16 607.72 569.68 58.59 o 2 0 -16 85.41 39.38 36.53 o 4 0 -16 147.10 146.26 35.48 o 6 0 -16 3772.95 3802.77 166.40 o 8 0 -16 7966.07 7947.55 260.73 o 10 0 -16 5639.75 5615.97 209.35 o 12 0 -16 2955.32 3071.97 167.94 o 14 0 -16 7048.74 7622.03 292.93 o 16 0 -16 2419.36 2287.49 160.27 o 18 0 -16 2108.88 1832.37 148.38 o -7 1 -16 2109.48 2166.55 113.94 o -5 1 -16 2839.66 2659.21 121.58 o -3 1 -16 4578.18 4347.32 126.34 o -1 1 -16 5410.71 5922.96 123.76 o 1 1 -16 10217.73 10242.39 170.04 o 3 1 -16 8347.09 8315.73 160.81 o 5 1 -16 3971.41 3838.63 74.95 o 7 1 -16 2822.58 3032.73 104.00 o 9 1 -16 1320.96 1214.17 72.87 o 11 1 -16 2260.68 2253.05 207.05 o 13 1 -16 2770.23 2880.63 92.89 o 15 1 -16 333.99 299.80 80.71 o 17 1 -16 23.43 -9.05 33.57 o -8 2 -16 988.83 1041.54 86.79 o -6 2 -16 1072.80 1047.59 69.51 o -4 2 -16 925.30 1047.42 67.71 o -2 2 -16 522.65 495.99 51.21 o 0 2 -16 151.91 129.22 36.05 o 2 2 -16 63.56 108.51 57.90 o 4 2 -16 293.75 278.94 44.42 o 6 2 -16 2273.13 2296.45 75.36 o 8 2 -16 2991.28 3092.42 174.65 o 10 2 -16 3438.55 3585.16 122.22 o 12 2 -16 4685.08 4470.33 139.45 o 14 2 -16 4291.39 4319.60 142.59 o 16 2 -16 2529.51 2550.18 221.81 o 18 2 -16 2145.59 2256.05 141.48 o -7 3 -16 1287.73 1331.36 77.15 o -5 3 -16 1537.00 1377.57 77.81 o -3 3 -16 1943.89 1793.41 96.24 o -1 3 -16 3928.55 3645.19 205.51 o 1 3 -16 5866.73 5931.53 262.64 o 3 3 -16 5559.73 5721.79 245.77 o 5 3 -16 3516.15 3756.03 249.80 o 7 3 -16 2193.71 2327.16 95.49 o 9 3 -16 4007.97 4285.88 135.01 o 11 3 -16 1638.91 1804.64 121.35 o 13 3 -16 1250.24 1406.84 84.28 o 15 3 -16 512.52 356.85 54.02 o 17 3 -16 349.84 384.44 47.43 o -8 4 -16 554.41 557.64 60.95 o -6 4 -16 394.08 447.55 54.87 o -4 4 -16 370.78 238.83 44.98 o -2 4 -16 568.77 471.61 88.95 o 0 4 -16 238.86 202.83 68.63 o 2 4 -16 433.83 447.07 79.37 o 4 4 -16 1872.58 2063.68 111.77 o 6 4 -16 2219.95 2170.14 93.02 o 8 4 -16 2055.22 2009.56 90.01 o 10 4 -16 3553.61 3660.82 127.29 o 12 4 -16 3637.95 3598.09 129.16 o 14 4 -16 603.63 545.83 60.96 o 16 4 -16 1390.23 1505.34 93.57 o 18 4 -16 1020.96 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