(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2012). E68, o2247-o2248
[ doi:10.1107/S1600536812028644 ]

N'-(Adamantan-2-ylidene)benzohydrazide

M. S. Almutairi, A. A. El-Emam, N. R. El-Brollosy, M. Said-Abdelbaky and S. García-Granda

Key indicators

Single-crystal X-ray study
T = 120 K
Mean (C-C) = 0.003 Å
R factor = 0.051
wR factor = 0.139
Data-to-parameter ratio = 14.2

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT414_ALERT_2_C Short Intra D-H..H-X       H1N    ..  H9      ..       1.96 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         11      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         49      
PLAT920_ALERT_1_C Theta(Max)  in CIF and FCF Differ by ...........       0.13 Deg. 

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   4 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   1 ALERT level G = General information/check it is not something unexpected

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check