Acta Cryst. (2012). E68, m1103
[ doi:10.1107/S1600536812032308 ]

cis-Dichlorido[2-(3,5-dimethyl-1H-pyrazol-1-yl-N²)ethanamine-N]palladium(II) dichloromethane monosolvate

C. Obuah, J. Darkwa and A. Muller

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.005 Å
• R factor = 0.032
• wR factor = 0.085
• Data-to-parameter ratio = 23.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.04      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600          7      

Alert level G
PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite          3      
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          2      
PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L=  0.600         12      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   2 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   4 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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