[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1032
[ doi:10.1107/S1600536812029984 ]

Tris(ethylenediamine-[kappa]2N,N')nickel(II) bis(dimethyl phosphate)

M. Rafizadeh, H. R. Saadati Moshtaghin and V. Amani


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C REFLT03_ALERT_3_C Reflection count < 95% complete From the CIF: _diffrn_reflns_theta_max 29.15 From the CIF: _diffrn_reflns_theta_full 29.00 From the CIF: _reflns_number_total 5205 TEST2: Reflns within _diffrn_reflns_theta_max Count of symmetry unique reflns 5677 Completeness (_total/calc) 91.69% PLAT420_ALERT_2_C D-H Without Acceptor N5 - H5D ... ? PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 235 PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 232 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 4
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c ....... P21/n PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N1 .. 5.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N4 .. 5.6 su
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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