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[Contents scheme]

Acta Cryst. (2012). E68, m1155
[ doi:10.1107/S1600536812032692 ]

(Ethylenediamine-[kappa]2N,N)bis[2-(pyridin-2-yl-[kappa]N)-1,3-imidazol-1-ido-[kappa]N1]cobalt(III) nitrate monohydrate

X.-L. Feng and Y.-P. Zhang


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of N9 PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -1.713 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 68 PLAT976_ALERT_2_C Negative Residual Density at 0.97A from O4 . -0.41 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 0.87A from O4 . -0.40 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 6 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 1 N4 -CO1 -N1 -C1 39.50 1.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 6 N4 -CO1 -N1 -C3 -137.40 0.80 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 13 N8 -CO1 -N3 -C8 -167.70 1.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 18 N8 -CO1 -N3 -C4 16.10 1.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 21 N1 -CO1 -N4 -C9 43.20 1.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 26 N1 -CO1 -N4 -C11 -131.40 0.80 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 34 N7 -CO1 -N6 -C16 -142.20 1.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 39 N7 -CO1 -N6 -C12 40.50 1.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 45 N6 -CO1 -N7 -C17 71.90 1.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 49 N3 -CO1 -N8 -C18 86.70 1.60 1.555 1.555 1.555 1.555 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 60 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 14 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 11 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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