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Acta Cryst. (2012). E68, m1206-m1207
[ doi:10.1107/S1600536812036367 ]

Bis[(1,10-phenanthroline-[kappa]2N,N')bis(triphenylphosphane-[kappa]P)copper(I)] nonadecaoxidohexamolybdate(VI)

F. Gschwind and M. Jansen


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT731_ALERT_1_C Bond Calc 2.3247(5), Rep 2.3248(11) ...... 2 su-Ra O9 -MO1 1.555 2.666 # 124 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.281 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 16 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT152_ALERT_1_G The Supplied and Calc. Volume s.u. Differ by ... 2 Units PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.03000 Deg. PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Cu1 -- P1 .. 9.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Mo3 -- O8 .. 5.7 su PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 197 O2 -MO2 -O9 -MO2 1.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 198 O10 -MO2 -O9 -MO2 10.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 199 O6 -MO2 -O9 -MO2 1.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 200 O3 -MO2 -O9 -MO2 17.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 201 O1 -MO2 -O9 -MO2 8.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 202 O2 -MO2 -O9 -MO3 -106.00 10.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 207 O2 -MO2 -O9 -MO3 74.00 10.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 212 O2 -MO2 -O9 -MO1 -16.00 10.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 217 O2 -MO2 -O9 -MO1 164.00 32.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 222 O8 -MO3 -O9 -MO2 -106.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 227 O8 -MO3 -O9 -MO2 74.00 2.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 232 O8 -MO3 -O9 -MO3 6.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 233 O5 -MO3 -O9 -MO3 10.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 234 O1 -MO3 -O9 -MO3 17.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 235 O10 -MO3 -O9 -MO3 1.00 0.00 2.666 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 236 O4 -MO3 -O9 -MO3 8.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 237 O8 -MO3 -O9 -MO1 -16.00 2.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 242 O8 -MO3 -O9 -MO1 164.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 247 O7 -MO1 -O9 -MO2 -90.00 4.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 252 O7 -MO1 -O9 -MO2 90.00 4.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 257 O7 -MO1 -O9 -MO3 18.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 262 O7 -MO1 -O9 -MO3 0.00 4.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 267 O7 -MO1 -O9 -MO1 9.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 268 O4 -MO1 -O9 -MO1 9.00 0.00 2.666 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 269 O3 -MO1 -O9 -MO1 18.00 0.00 1.555 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 270 O6 -MO1 -O9 -MO1 0.00 0.00 2.666 1.555 1.555 2.666 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 271 O5 -MO1 -O9 -MO1 9.00 0.00 1.555 1.555 1.555 2.666 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 52
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 33 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 28 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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