Acta Cryst. (2012). E68, m1210-m1211
[ doi:10.1107/S1600536812036410 ]

Trichlorido[4-methoxy-2,6-bis(2-pyrimidin-2-yl-N)phenyl-C¹]platinum(IV) acetonitrile monosolvate

Y. Wu, D. Xie, D. Zhang, X. Li and W. Jin

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.010 Å
• R factor = 0.033
• wR factor = 0.085
• Data-to-parameter ratio = 14.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         C17     
PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor ....        2.1      
PLAT342_ALERT_3_C Low Bond Precision on  C-C Bonds ...............     0.0097 Ang  
PLAT480_ALERT_4_C Long H...A H-Bond Reported H4     ..  CL2     ..       2.84 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600          6      

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal ..........    0.00200 Deg. 
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported   _diffrn_ambient_temperature        293 K    
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         36     
            CL1 -PT1 -C5  -C10  -175.00 25.00   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         41     
            CL1 -PT1 -C5  -C6      4.00 14.00   1.555   1.555   1.555   1.555  

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   5 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   6 ALERT level G = General information/check it is not something unexpected

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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