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[Contents scheme]

Acta Cryst. (2012). E68, m1224-m1225
[ doi:10.1107/S1600536812036665 ]

rac-cis-Dicarbonylchlorido{1-[2-(diphenylphosphanyl-[kappa]P)benzyl]-3-(phenyl-[kappa]C1)imidazol-2-ylidene-[kappa]C2}ruthenium(II) dichloromethane monosolvate

G. J. Domski, W. H. Pecak and D. C. Swenson


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X) Ru1 -- C1 .. 11.3 su
Alert level C PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 5 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 4
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 6 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00500 Deg. PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 = 3 PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ru1 -- Cl1 .. 6.4 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ru1 -- C2 .. 5.5 su PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C51' PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 C H2 Cl2 PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 3 C H2 Cl2 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 22 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 62
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 13 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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