Acta Crystallographica Section E

Structure Reports Online

Volume 68, Part 9 (September 2012)


organic compounds



mw2063 scheme

Acta Cryst. (2012). E68, o2614    [ doi:10.1107/S1600536812033363 ]

1-[(Pyridin-3-yl)(pyrrolidin-1-yl)methyl]naphthalen-2-ol

Q.-Q. Zhou

Abstract: The title compound, C20H20N2O, was synthesized by a solvent-free one-pot three-component domino reaction of naphthalen-2-ol, nicotinaldehyde and pyrrolidine. The dihedral angle between the naphthalene ring system and the pyridine ring is 74.22 (6)°. The pyrrolidine ring assumes an envelope conformation with the N atom as the flap. An intramolecular O-H...N hydrogen bond stabilizes the molecular conformation.


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