[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1153-m1154
[ doi:10.1107/S1600536812033880 ]

[[mu]-N,N'-Bis(2-aminoethyl)ethane-1,2-diamine-[kappa]4N1,N1':N2,N2']bis{[N,N'-bis(2-aminoethyl)ethane-1,2-diamine-[kappa]4N,N',N'',N''']cadmium} tetrakis(perchlorate)

H. Goudarziafshar, Y. Abbasityula, V. Eigner and M. Dusek


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 16
Author Response: Weak reflections with no significant impact on refinement.

Alert level C GOODF01_ALERT_2_C The least squares goodness of fit parameter lies outside the range 0.80 <> 2.00 Goodness of fit given = 2.020 PLAT022_ALERT_3_C Ratio Unique / Expected Reflections (too) Low .. 0.920 PLAT127_ALERT_1_C Implicit Hall Symbol Inconsistent with Explicit -P 2yabc PLAT165_ALERT_3_C Nr. of Status R Flagged Non-Hydrogen Atoms ..... 10 PLAT352_ALERT_3_C Short N-H Bond (0.87A) N14 - H1N14 ... 0.70 Ang. PLAT353_ALERT_3_C Long N-H Bond (0.87A) N10 - H1N10 ... 1.06 Ang. PLAT353_ALERT_3_C Long N-H Bond (0.87A) N10 - H2N10 ... 1.01 Ang. PLAT420_ALERT_2_C D-H Without Acceptor N10 - H2N10 ... ? PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 6
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.70 mm PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of Cl1A PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of Cl1B PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 50 Perc. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 27 PLAT793_ALERT_4_G The Model has Chirality at N4 (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at N7 (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at N14 (Verify) .... R PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 401 PLAT960_ALERT_3_G Number of Intensities with I .LT. - 2*sig(I) ... 3
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 8 ALERT type 3 Indicator that the structure quality may be low 9 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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