# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Bu4As in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 187.61 _exptl_crystal_F_000 676.00 _reflns_d_resolution_high 0.7494 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.0353 _cell_length_b 10.1366 _cell_length_c 18.7892 _cell_angle_alpha 94.005 _cell_angle_beta 97.749 _cell_angle_gamma 114.289 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 841.02 869.81 30.85 o 2 0 0 9374.29 9337.15 226.58 o 3 0 0 1.20 0.35 1.31 o 4 0 0 6920.34 6787.17 136.65 o 5 0 0 30.73 40.73 2.88 o 6 0 0 2635.83 2556.30 53.26 o 7 0 0 79.84 79.61 4.67 o 8 0 0 143.26 142.21 6.58 o 9 0 0 16.25 23.80 4.67 o 10 0 0 5.07 8.17 6.40 o -11 1 0 112.01 122.79 8.91 o -10 1 0 150.06 156.33 7.93 o -9 1 0 501.44 467.37 13.25 o -8 1 0 2658.01 2570.68 54.31 o -7 1 0 837.39 831.27 19.29 o -6 1 0 3220.91 3003.00 107.69 o -5 1 0 327.08 351.05 8.84 o -4 1 0 802.19 655.95 14.45 o -3 1 0 2739.88 2672.12 128.36 o -2 1 0 19067.21 17947.02 359.79 o -1 1 0 538.82 557.33 11.83 o 0 1 0 13507.37 13354.06 419.67 o 1 1 0 3967.63 4091.92 101.72 o 2 1 0 2544.51 2478.81 62.33 o 3 1 0 97.68 95.76 4.33 o 4 1 0 3233.26 3016.71 61.80 o 5 1 0 565.47 582.67 13.91 o 6 1 0 4981.16 4950.38 101.11 o 7 1 0 37.78 39.80 5.47 o 8 1 0 226.59 224.74 9.43 o 9 1 0 16.15 15.28 5.26 o 10 1 0 3.82 2.29 5.51 o -11 2 0 329.51 336.30 11.93 o -10 2 0 270.47 280.86 12.04 o -9 2 0 924.88 918.74 21.89 o -8 2 0 1184.71 1121.19 25.28 o -7 2 0 520.77 471.45 11.99 o -6 2 0 1450.27 1319.42 45.27 o -5 2 0 213.82 220.60 10.33 o -4 2 0 2367.19 2251.27 45.97 o -3 2 0 905.47 999.72 23.31 o -2 2 0 13901.59 13544.53 271.69 o -1 2 0 19.26 14.64 2.64 o 0 2 0 29513.99 27073.07 678.22 o 1 2 0 5475.47 5761.91 142.74 o 2 2 0 490.13 420.24 12.11 o 3 2 0 858.53 846.41 22.84 o 4 2 0 7351.28 7476.98 185.77 o 5 2 0 770.18 679.51 41.94 o 6 2 0 1935.08 1837.59 48.30 o 7 2 0 31.04 34.75 4.88 o 8 2 0 191.96 184.28 9.57 o 9 2 0 48.49 52.19 6.69 o -11 3 0 388.19 389.59 19.03 o -10 3 0 535.00 548.52 15.05 o -9 3 0 1594.61 1541.11 33.96 o -8 3 0 2615.09 2546.79 53.34 o -7 3 0 41.75 48.90 7.02 o -6 3 0 2056.35 1853.49 64.61 o -5 3 0 51.49 59.99 2.91 o -4 3 0 5087.63 5417.29 108.94 o -3 3 0 63.68 69.93 2.49 o -2 3 0 6671.36 6995.81 140.36 o -1 3 0 367.18 399.95 13.99 o 0 3 0 780.94 996.91 41.15 o 1 3 0 852.79 785.74 31.26 o 2 3 0 48.96 31.50 7.49 o 3 3 0 4436.01 4632.39 182.92 o 4 3 0 1372.89 1340.16 32.58 o 5 3 0 1294.82 1265.70 27.93 o 6 3 0 635.01 643.14 16.11 o 7 3 0 1152.02 1155.47 50.33 o 8 3 0 53.03 51.45 9.41 o 9 3 0 913.59 929.07 33.23 o -11 4 0 645.56 661.48 17.84 o -10 4 0 212.58 211.19 8.39 o -9 4 0 531.32 489.42 12.99 o -8 4 0 133.88 119.74 5.39 o -7 4 0 2.06 14.95 8.57 o -6 4 0 1150.13 1069.38 23.04 o -5 4 0 85.79 89.08 4.55 o -4 4 0 1853.03 2057.85 42.01 o -3 4 0 342.81 316.13 7.16 o -2 4 0 5917.35 6348.14 154.33 o -1 4 0 1764.73 1943.18 93.00 o 0 4 0 681.89 810.80 34.70 o 1 4 0 2909.40 2489.20 255.73 o 2 4 0 32.44 23.37 3.30 o 3 4 0 1960.07 1940.78 107.17 o 4 4 0 917.38 927.94 25.76 o 5 4 0 708.67 662.64 19.56 o 6 4 0 2.14 -0.43 3.59 o 7 4 0 679.00 664.72 21.02 o 8 4 0 1.69 0.08 5.61 o -11 5 0 401.75 395.70 12.69 o -10 5 0 1.94 2.79 3.81 o -9 5 0 401.25 387.38 11.01 o -8 5 0 170.75 166.63 6.36 o -7 5 0 94.49 89.03 6.46 o -6 5 0 70.91 72.55 3.57 o -5 5 0 26.74 23.91 2.45 o -4 5 0 1940.59 2081.94 42.49 o -3 5 0 3341.64 3483.50 85.43 o -2 5 0 2388.28 2892.66 71.13 o -1 5 0 2790.64 3078.02 68.34 o 0 5 0 70.28 81.13 3.35 o 1 5 0 2542.35 2297.75 110.20 o 2 5 0 510.41 421.24 21.23 o 3 5 0 2828.31 2828.46 158.69 o 4 5 0 117.96 113.65 9.93 o 5 5 0 2310.98 2362.24 69.33 o 6 5 0 166.28 163.31 9.31 o 7 5 0 1763.01 1811.83 49.34 o 8 5 0 23.68 16.98 6.79 o -11 6 0 209.46 202.60 10.91 o -10 6 0 22.70 25.73 4.42 o -9 6 0 77.56 64.37 4.64 o -8 6 0 634.37 577.62 13.96 o -7 6 0 725.04 719.97 16.43 o -6 6 0 406.35 372.75 9.28 o -5 6 0 1466.58 1437.53 29.93 o -4 6 0 30.54 26.27 3.51 o -3 6 0 3000.04 3158.30 77.81 o -2 6 0 530.10 546.34 14.93 o -1 6 0 4413.18 4669.39 94.24 o 0 6 0 60.50 61.00 3.36 o 1 6 0 2879.99 2555.48 88.42 o 2 6 0 325.74 239.47 9.70 o 3 6 0 1026.34 990.39 29.12 o 4 6 0 133.35 123.13 8.17 o 5 6 0 891.17 854.98 25.55 o 6 6 0 171.56 164.94 9.81 o 7 6 0 788.73 827.80 26.04 o -11 7 0 121.04 127.36 8.83 o -10 7 0 304.35 295.47 12.02 o -9 7 0 37.10 49.60 5.30 o -8 7 0 218.80 203.78 8.74 o -7 7 0 245.29 231.10 9.18 o -6 7 0 846.09 795.52 21.68 o -5 7 0 50.51 41.43 3.72 o -4 7 0 81.67 87.34 5.15 o -3 7 0 3550.45 3759.37 92.59 o -2 7 0 990.66 869.54 39.66 o -1 7 0 3652.97 3883.79 90.00 o 0 7 0 64.38 65.42 3.37 o 1 7 0 2190.86 2028.38 76.89 o 2 7 0 138.86 109.90 8.52 o 3 7 0 2793.76 2688.54 87.52 o 4 7 0 7.54 10.96 5.78 o 5 7 0 2101.98 2131.27 57.08 o 6 7 0 6.15 3.17 6.04 o -11 8 0 24.25 21.96 6.85 o -10 8 0 715.03 685.83 21.35 o -9 8 0 514.91 484.30 16.08 o -8 8 0 458.98 427.90 14.14 o -7 8 0 47.77 45.30 4.48 o -6 8 0 46.88 47.32 4.37 o -5 8 0 1127.84 1119.41 29.39 o -4 8 0 1527.69 1422.66 36.54 o -3 8 0 2333.97 2401.35 60.15 o -2 8 0 670.14 687.24 19.18 o -1 8 0 2852.45 2815.28 70.77 o 0 8 0 1012.55 934.11 26.20 o 1 8 0 2782.80 2531.71 131.24 o 2 8 0 7.13 13.32 9.63 o 3 8 0 1357.76 1262.73 55.76 o 4 8 0 0.13 -6.89 12.07 o 5 8 0 1101.11 1094.78 46.27 o -11 9 0 0.56 0.99 6.11 o -10 9 0 1068.03 1071.10 30.69 o -9 9 0 3.00 6.36 4.88 o -8 9 0 846.97 853.28 24.36 o -7 9 0 471.57 461.53 14.54 o -6 9 0 1223.80 1170.79 31.15 o -5 9 0 14.35 27.10 4.25 o -4 9 0 434.85 405.41 18.07 o -3 9 0 1169.79 1171.94 44.99 o -2 9 0 956.22 951.48 26.09 o -1 9 0 435.09 440.83 15.98 o 0 9 0 23.74 20.15 4.48 o 1 9 0 261.36 243.73 10.47 o 2 9 0 76.66 72.47 14.78 o 3 9 0 1113.17 1037.59 49.61 o 4 9 0 3.69 2.57 15.11 o -10 10 0 1260.16 1278.18 35.87 o -9 10 0 83.70 74.66 10.61 o -8 10 0 363.60 334.51 12.48 o -7 10 0 5.42 6.58 4.69 o -6 10 0 111.90 125.31 7.05 o -5 10 0 524.75 528.08 16.07 o -4 10 0 1114.92 1151.00 38.02 o -3 10 0 586.38 584.47 17.73 o -2 10 0 272.14 263.92 10.86 o -1 10 0 909.16 884.96 25.69 o 0 10 0 70.50 78.45 14.64 o 1 10 0 356.68 292.93 22.70 o 2 10 0 12.86 3.28 12.84 o 3 10 0 807.60 849.75 45.90 o -10 11 0 625.11 623.67 27.90 o -9 11 0 19.69 17.16 7.64 o -8 11 0 1306.05 1319.25 36.10 o -7 11 0 33.57 36.94 7.32 o -6 11 0 1092.03 1078.50 31.21 o -5 11 0 212.46 204.02 14.94 o -4 11 0 788.62 776.46 22.55 o -3 11 0 268.96 264.71 16.28 o -2 11 0 21.57 27.07 5.54 o -1 11 0 26.26 25.91 5.85 o 0 11 0 330.97 301.69 23.63 o 1 11 0 20.66 13.17 13.74 o 2 11 0 71.50 70.23 17.55 o -9 12 0 39.74 43.24 7.32 o -8 12 0 553.70 536.87 18.14 o -7 12 0 22.79 21.65 6.20 o -6 12 0 935.92 935.01 26.93 o -5 12 0 87.67 74.07 6.66 o -4 12 0 434.23 420.80 15.14 o -3 12 0 10.86 12.29 5.62 o -2 12 0 0.02 5.60 6.60 o -1 12 0 4.98 3.71 12.67 o 0 12 0 56.51 24.44 15.34 o -7 13 0 408.24 381.31 17.45 o -6 13 0 311.99 316.53 13.62 o -5 13 0 90.17 97.31 8.39 o -4 13 0 16.96 30.04 7.01 o -3 13 0 270.06 263.36 13.34 o 2 -13 1 904.67 921.59 37.44 o 3 -13 1 50.53 45.70 7.38 o 4 -13 1 1973.90 2022.50 53.81 o 5 -13 1 9.91 9.76 6.26 o 6 -13 1 624.77 647.84 35.10 o 7 -13 1 129.44 140.60 9.59 o 0 -12 1 1089.92 971.00 46.80 o 1 -12 1 23.73 22.80 6.34 o 2 -12 1 1966.10 1902.88 51.14 o 3 -12 1 74.93 66.18 8.24 o 4 -12 1 1417.12 1468.39 39.76 o 5 -12 1 338.38 308.22 12.56 o 6 -12 1 759.94 741.94 22.37 o 7 -12 1 13.87 13.86 5.60 o 8 -12 1 420.53 420.44 15.70 o 9 -12 1 60.89 58.78 8.64 o -2 -11 1 344.77 362.80 28.28 o -1 -11 1 1.18 -0.23 13.04 o 0 -11 1 809.10 749.05 32.24 o 1 -11 1 16.14 21.87 7.12 o 2 -11 1 1237.51 1257.69 34.82 o 3 -11 1 89.47 102.66 7.12 o 4 -11 1 559.32 552.25 20.22 o 5 -11 1 188.48 184.89 9.29 o 6 -11 1 550.87 524.77 16.62 o 7 -11 1 3.89 7.05 5.17 o 8 -11 1 607.48 623.58 21.38 o 9 -11 1 94.45 90.31 7.95 o 10 -11 1 133.81 151.66 9.99 o -3 -10 1 15.10 15.74 15.31 o -2 -10 1 1130.76 1093.75 50.28 o -1 -10 1 274.94 261.34 15.64 o 0 -10 1 1439.69 1331.33 37.00 o 1 -10 1 126.70 121.68 7.96 o 2 -10 1 1948.67 1896.30 88.84 o 3 -10 1 585.91 575.05 20.94 o 4 -10 1 577.20 601.88 17.86 o 5 -10 1 563.20 551.07 16.74 o 6 -10 1 638.00 618.96 18.39 o 7 -10 1 549.71 520.58 22.20 o 8 -10 1 648.51 614.18 18.99 o 9 -10 1 580.88 613.54 19.63 o 10 -10 1 0.30 7.58 6.47 o -4 -9 1 448.81 505.71 31.72 o -3 -9 1 33.67 33.13 13.64 o -2 -9 1 879.85 824.48 41.42 o -1 -9 1 174.60 177.55 8.97 o 0 -9 1 1674.24 1559.48 41.81 o 1 -9 1 363.13 354.52 12.66 o 2 -9 1 699.97 711.84 37.61 o 3 -9 1 1543.87 1596.45 41.26 o 4 -9 1 99.37 108.90 15.33 o 5 -9 1 425.22 432.13 13.42 o 6 -9 1 34.52 41.33 4.78 o 7 -9 1 1408.38 1406.85 37.21 o 8 -9 1 13.67 11.97 4.89 o 9 -9 1 2059.94 2011.22 52.63 o 10 -9 1 12.73 14.34 6.10 o 11 -9 1 675.49 670.68 21.83 o -5 -8 1 35.44 36.34 10.00 o -4 -8 1 15.84 28.15 12.67 o -3 -8 1 242.80 231.58 14.39 o -2 -8 1 150.29 121.71 7.44 o -1 -8 1 528.66 438.41 19.77 o 0 -8 1 312.86 288.93 10.83 o 1 -8 1 3827.00 3902.25 97.00 o 2 -8 1 306.28 274.89 9.57 o 3 -8 1 1227.68 1178.31 30.76 o 4 -8 1 319.37 295.78 9.80 o 5 -8 1 218.44 227.90 20.98 o 6 -8 1 978.93 972.07 26.21 o 7 -8 1 1450.13 1488.91 39.00 o 8 -8 1 33.70 39.14 7.86 o 9 -8 1 1583.50 1562.14 41.62 o 10 -8 1 134.45 125.83 8.19 o 11 -8 1 904.89 878.00 26.85 o -6 -7 1 14.67 16.39 6.08 o -5 -7 1 127.22 133.15 11.82 o -4 -7 1 0.45 -2.16 5.24 o -3 -7 1 196.85 188.80 7.25 o -2 -7 1 101.53 98.36 5.14 o -1 -7 1 2297.36 2005.43 91.22 o 0 -7 1 24.77 28.89 5.84 o 1 -7 1 5429.95 5685.22 114.60 o 2 -7 1 0.38 16.42 11.80 o 3 -7 1 2959.82 2778.04 272.31 o 4 -7 1 216.17 234.67 8.24 o 5 -7 1 4654.96 4792.02 117.73 o 6 -7 1 94.34 94.74 5.46 o 7 -7 1 3698.76 3733.38 92.82 o 8 -7 1 61.77 59.98 5.29 o 9 -7 1 2636.11 2624.76 67.09 o 10 -7 1 52.24 49.32 6.05 o 11 -7 1 703.25 689.30 21.93 o -7 -6 1 5.78 6.54 5.90 o -6 -6 1 150.96 151.36 8.83 o -5 -6 1 61.63 63.65 7.14 o -4 -6 1 37.87 35.22 5.30 o -3 -6 1 770.51 757.50 23.00 o -2 -6 1 568.25 314.02 55.91 o -1 -6 1 1768.87 1470.05 89.31 o 0 -6 1 247.08 266.83 11.41 o 1 -6 1 5304.53 5546.60 111.64 o 2 -6 1 377.29 446.70 12.65 o 3 -6 1 5937.17 6143.14 149.89 o 4 -6 1 54.66 56.76 3.57 o 5 -6 1 4698.83 4623.45 126.54 o 6 -6 1 215.93 211.71 6.35 o 7 -6 1 3849.34 3754.54 76.68 o 8 -6 1 174.39 151.28 6.09 o 9 -6 1 1058.56 1067.76 24.27 o 10 -6 1 8.45 2.34 3.84 o 11 -6 1 454.07 461.67 16.74 o -8 -5 1 329.31 363.33 15.03 o -7 -5 1 131.06 140.78 10.03 o -6 -5 1 413.81 386.74 14.06 o -5 -5 1 511.78 478.85 15.76 o -4 -5 1 824.98 749.27 30.82 o -3 -5 1 584.11 573.00 17.97 o -2 -5 1 214.53 178.50 20.74 o -1 -5 1 2130.89 1845.83 126.88 o 0 -5 1 867.72 850.79 26.61 o 1 -5 1 4829.34 4744.13 95.48 o 2 -5 1 871.50 947.29 24.16 o 3 -5 1 6756.18 7154.90 174.07 o 4 -5 1 75.25 74.80 3.17 o 5 -5 1 7346.38 7221.17 145.18 o 6 -5 1 62.41 64.57 3.32 o 7 -5 1 5216.58 5108.16 103.71 o 8 -5 1 24.93 15.08 3.06 o 9 -5 1 2889.35 2845.17 59.55 o 10 -5 1 325.37 304.86 10.19 o 11 -5 1 310.42 301.75 10.84 o -8 -4 1 718.20 724.15 31.54 o -7 -4 1 189.64 188.91 9.73 o -6 -4 1 660.36 657.31 19.95 o -5 -4 1 809.78 790.43 27.85 o -4 -4 1 781.08 676.03 46.27 o -3 -4 1 1578.58 1597.96 78.53 o -2 -4 1 69.93 66.51 5.13 o -1 -4 1 2514.27 2132.03 221.01 o 0 -4 1 1029.10 1101.82 23.79 o 1 -4 1 2237.94 2250.58 45.60 o 2 -4 1 0.86 4.53 1.62 o 3 -4 1 3281.81 3232.57 65.26 o 4 -4 1 1159.90 1295.23 26.89 o 5 -4 1 3815.02 3714.49 75.31 o 6 -4 1 23.94 29.99 2.73 o 7 -4 1 4889.10 4855.64 98.73 o 8 -4 1 286.64 279.08 12.86 o 9 -4 1 278.47 259.60 8.80 o 10 -4 1 414.05 376.12 14.60 o 11 -4 1 626.43 636.51 17.30 o -9 -3 1 1.38 -4.36 5.44 o -8 -3 1 1402.79 1371.18 46.70 o -7 -3 1 418.11 363.79 12.93 o -6 -3 1 1715.63 1716.43 49.65 o -5 -3 1 268.87 249.55 8.10 o -4 -3 1 3245.17 3302.31 67.91 o -3 -3 1 97.47 87.22 6.18 o -2 -3 1 85.67 75.32 7.15 o -1 -3 1 6670.62 6192.43 215.38 o 0 -3 1 2221.73 2250.44 45.58 o 1 -3 1 282.67 236.94 5.82 o 2 -3 1 3.57 4.30 0.91 o 3 -3 1 2821.54 2636.12 53.35 o 4 -3 1 1674.75 1791.22 36.77 o 5 -3 1 2394.07 2391.40 49.05 o 6 -3 1 329.66 311.81 8.27 o 7 -3 1 1786.60 1790.56 37.92 o 8 -3 1 1218.35 1190.89 26.51 o 9 -3 1 1260.91 1225.84 27.78 o 10 -3 1 1150.64 1145.31 26.86 o 11 -3 1 388.49 379.91 12.82 o -9 -2 1 85.31 83.75 7.22 o -8 -2 1 1052.34 1026.51 24.36 o -7 -2 1 30.23 33.82 4.14 o -6 -2 1 1396.93 1328.70 49.00 o -5 -2 1 195.40 161.72 6.08 o -4 -2 1 1173.04 1170.48 25.36 o -3 -2 1 810.21 808.23 17.74 o -2 -2 1 3099.14 3484.30 70.73 o -1 -2 1 29818.03 28104.83 767.10 o 0 -2 1 3294.49 3474.29 86.10 o 1 -2 1 228.62 263.97 6.13 o 2 -2 1 1965.12 2016.85 41.00 o 3 -2 1 1201.95 1082.84 22.47 o 4 -2 1 1851.67 2041.04 41.89 o 5 -2 1 874.08 907.19 19.67 o 6 -2 1 1310.09 1258.10 27.09 o 7 -2 1 461.10 438.52 11.46 o 8 -2 1 2886.14 2802.63 58.77 o 9 -2 1 12.16 7.12 3.97 o 10 -2 1 1150.93 1102.24 26.24 o 11 -2 1 221.87 212.32 11.02 o -10 -1 1 780.62 755.48 23.77 o -9 -1 1 16.28 18.46 4.36 o -8 -1 1 1729.07 1711.30 37.64 o -7 -1 1 6.25 14.25 4.12 o -6 -1 1 683.79 684.32 16.30 o -5 -1 1 710.55 696.61 16.05 o -4 -1 1 6166.27 6484.17 130.74 o -3 -1 1 357.12 390.05 19.20 o -2 -1 1 1702.91 1797.72 37.19 o -1 -1 1 1890.37 1826.27 45.78 o 0 -1 1 267.40 286.67 8.36 o 1 -1 1 1780.15 1805.37 36.71 o 2 -1 1 17.86 10.97 1.18 o 3 -1 1 1207.64 1299.11 26.93 o 4 -1 1 1232.62 1258.88 26.42 o 5 -1 1 848.51 868.73 19.08 o 6 -1 1 1140.61 1078.99 23.72 o 7 -1 1 3.29 6.17 3.05 o 8 -1 1 2220.63 2269.36 48.43 o 9 -1 1 51.82 55.89 5.10 o 10 -1 1 963.47 979.21 29.01 o 11 -1 1 40.58 39.95 9.13 o -10 0 1 1008.73 1028.00 25.20 o -9 0 1 188.43 184.74 7.98 o -8 0 1 875.91 801.49 19.45 o -7 0 1 309.61 286.98 8.73 o -6 0 1 1432.10 1372.34 54.30 o -5 0 1 108.77 105.68 4.40 o -4 0 1 405.20 438.81 10.31 o -3 0 1 1664.12 1835.87 37.72 o -2 0 1 2083.81 2098.80 44.49 o -1 0 1 5107.20 5038.16 187.21 o 1 0 1 694.23 781.09 19.68 o 2 0 1 624.35 520.18 19.43 o 3 0 1 30.06 18.58 2.05 o 4 0 1 730.84 722.73 19.65 o 5 0 1 760.13 695.64 27.25 o 6 0 1 2916.50 2792.88 58.01 o 7 0 1 35.95 38.33 3.82 o 8 0 1 2050.56 2060.80 44.48 o 9 0 1 11.26 6.87 4.14 o 10 0 1 1024.91 1062.25 31.19 o -11 1 1 88.90 87.81 7.88 o -10 1 1 686.26 666.38 17.69 o -9 1 1 172.97 167.05 7.51 o -8 1 1 101.61 100.76 5.29 o -7 1 1 111.94 121.48 5.50 o -6 1 1 536.27 513.03 19.57 o -5 1 1 1690.36 1652.40 34.56 o -4 1 1 424.96 484.06 10.98 o -3 1 1 5971.00 6473.40 129.89 o -2 1 1 2091.53 1958.67 47.97 o -1 1 1 3810.57 3999.17 80.42 o 0 1 1 1409.57 1612.17 114.94 o 1 1 1 408.74 430.43 9.33 o 2 1 1 3859.21 3678.32 170.50 o 3 1 1 38.66 29.80 2.29 o 4 1 1 2601.34 2611.68 53.82 o 5 1 1 226.10 217.28 12.45 o 6 1 1 4762.62 4776.79 120.22 o 7 1 1 328.78 273.16 26.58 o 8 1 1 2097.26 2067.55 44.83 o 9 1 1 11.56 12.45 5.40 o 10 1 1 614.48 594.61 20.28 o -11 2 1 684.43 704.98 18.98 o -10 2 1 749.06 744.46 19.06 o -9 2 1 431.32 438.90 12.45 o -8 2 1 578.37 575.70 14.53 o -7 2 1 659.38 616.95 14.80 o -6 2 1 655.68 656.14 15.02 o -5 2 1 2135.11 2017.52 41.64 o -4 2 1 61.63 53.37 2.47 o -3 2 1 1484.75 1487.22 30.41 o -2 2 1 1608.64 1727.38 34.94 o -1 2 1 24818.97 21259.03 1319.56 o 0 2 1 8828.35 8956.60 182.44 o 1 2 1 496.21 475.33 13.36 o 2 2 1 927.27 974.32 20.82 o 3 2 1 4571.86 4638.22 115.54 o 4 2 1 1277.23 1207.87 26.13 o 5 2 1 81.71 83.46 6.38 o 6 2 1 3183.17 3225.32 67.06 o 7 2 1 10.21 10.11 3.96 o 8 2 1 926.34 884.83 26.36 o 9 2 1 108.70 114.22 10.68 o -11 3 1 1025.96 1039.87 25.33 o -10 3 1 196.88 200.52 8.40 o -9 3 1 1796.55 1830.26 39.57 o -8 3 1 29.78 25.11 3.51 o -7 3 1 3443.18 3356.98 68.87 o -6 3 1 227.69 236.23 6.85 o -5 3 1 9145.41 8952.77 179.63 o -4 3 1 298.06 323.12 7.69 o -3 3 1 3909.46 3835.92 86.13 o -2 3 1 150.07 148.36 4.68 o -1 3 1 114.12 92.16 2.13 o 0 3 1 3703.19 3745.09 75.44 o 1 3 1 472.43 382.19 18.08 o 2 3 1 1705.68 1619.49 42.22 o 3 3 1 895.46 875.54 19.58 o 4 3 1 6004.48 5746.22 307.07 o 5 3 1 1314.45 1335.05 40.49 o 6 3 1 1862.18 1809.65 39.14 o 7 3 1 16.50 15.45 4.88 o 8 3 1 936.14 977.42 29.03 o 9 3 1 6.60 15.23 6.63 o -11 4 1 1239.13 1281.45 29.81 o -10 4 1 8.58 14.86 4.21 o -9 4 1 2028.47 1987.03 42.54 o -8 4 1 47.39 40.97 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