[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1201
[ doi:10.1107/S1600536812035957 ]

fac-Bromidotricarbonyl[2-(diisopropylphosphanyl)benzaldehyde-[kappa]2O,P]rhenium(I)

C. Apostolidis, M. Ahlmann and O. Walter


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT919_ALERT_3_B Reflection # Likely Affected by the Beamstop ... 1 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1
Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.975 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT164_ALERT_4_G Nr. of Refined C-H H-Atoms in Heavy-Atom Struct. 1 PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Re1 -- Br1 .. 6.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Re1 -- C14 .. 6.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Re1 -- C15 .. 6.5 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Re1 -- C16 .. 5.8 su PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 90
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster