# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Z in Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 100.19 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.8411 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 6.8604 _cell_length_b 9.4534 _cell_length_c 16.4789 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1218.54 1202.26 13.54 o 6 0 0 134.32 132.69 4.71 o 8 0 0 71.48 79.90 4.64 o 2 1 0 2964.15 2697.48 43.75 o 4 1 0 260.76 260.29 3.04 o 6 1 0 1.37 1.92 1.34 o 8 1 0 0.04 1.14 1.49 o 2 2 0 2714.34 2699.14 21.87 o 4 2 0 1175.79 1145.44 9.27 o 6 2 0 56.57 64.98 3.03 o 8 2 0 3.08 4.70 1.78 o 2 3 0 2017.33 2049.30 15.13 o 4 3 0 198.06 204.31 3.00 o 6 3 0 1.55 2.19 1.28 o 0 4 0 3591.11 3744.64 37.99 o 2 4 0 1414.86 1451.09 12.51 o 4 4 0 65.34 66.89 1.70 o 6 4 0 0.01 -0.06 0.97 o 2 5 0 74.51 61.94 1.55 o 4 5 0 99.49 100.52 3.19 o 6 5 0 21.90 18.88 1.56 o 0 6 0 204.94 179.79 3.38 o 2 6 0 26.97 20.52 1.16 o 4 6 0 34.27 24.48 1.38 o 6 6 0 68.15 72.21 2.61 o 2 7 0 7.32 8.75 1.06 o 4 7 0 24.99 23.77 1.83 o 6 7 0 7.99 7.06 1.49 o 0 8 0 385.66 384.22 10.71 o 2 8 0 73.92 71.88 2.30 o 4 8 0 13.02 9.93 1.34 o 2 9 0 13.70 13.87 1.59 o 4 9 0 4.04 2.00 1.28 o 0 10 0 2.20 0.27 1.66 o 2 10 0 2.78 6.91 1.45 o 1 1 1 5842.59 5720.83 38.83 o 2 1 1 2208.94 2121.42 12.10 o 3 1 1 9.78 7.11 0.39 o 4 1 1 533.86 506.99 3.33 o 5 1 1 0.08 -0.34 0.44 o 6 1 1 42.16 41.18 1.20 o 7 1 1 85.67 88.13 2.58 o 8 1 1 1.23 1.89 1.11 o 0 2 1 140.53 111.69 1.61 o 1 2 1 559.68 544.11 3.58 o 2 2 1 53.49 59.89 0.88 o 3 2 1 20.73 24.73 0.63 o 4 2 1 256.87 252.38 2.19 o 5 2 1 93.97 87.68 1.31 o 6 2 1 132.82 132.18 2.09 o 7 2 1 11.66 12.60 1.24 o 8 2 1 30.13 32.07 1.87 o 1 3 1 3.32 7.38 0.42 o 2 3 1 374.20 377.33 2.54 o 3 3 1 163.25 180.05 1.73 o 4 3 1 492.22 452.08 3.44 o 5 3 1 153.60 146.23 1.78 o 6 3 1 134.30 126.55 2.90 o 7 3 1 34.65 35.05 1.74 o 0 4 1 171.71 178.31 2.07 o 1 4 1 205.66 203.87 1.77 o 2 4 1 43.35 45.97 0.81 o 3 4 1 255.14 258.89 2.09 o 4 4 1 17.14 16.29 0.79 o 5 4 1 0.40 -0.53 0.56 o 6 4 1 14.22 13.32 1.29 o 7 4 1 4.33 4.10 1.16 o 1 5 1 59.10 65.91 1.08 o 2 5 1 1.81 1.80 0.49 o 3 5 1 5.03 5.14 0.59 o 4 5 1 33.76 35.50 1.02 o 5 5 1 0.31 -0.49 0.53 o 6 5 1 38.22 37.71 1.54 o 7 5 1 3.91 4.18 1.16 o 0 6 1 0.84 0.86 0.57 o 1 6 1 2.72 3.22 0.62 o 2 6 1 11.72 12.18 0.72 o 3 6 1 4.61 3.39 0.64 o 4 6 1 5.79 5.26 0.72 o 5 6 1 27.14 26.35 1.16 o 6 6 1 0.03 0.33 0.93 o 1 7 1 27.00 24.56 1.09 o 2 7 1 219.19 209.17 2.42 o 3 7 1 106.85 99.02 1.64 o 4 7 1 224.97 217.86 2.49 o 5 7 1 60.24 57.11 1.63 o 6 7 1 79.01 83.39 2.28 o 0 8 1 3.24 3.68 1.15 o 1 8 1 1.79 1.23 0.76 o 2 8 1 2.12 2.20 0.76 o 3 8 1 7.22 7.74 1.01 o 4 8 1 15.33 19.67 1.04 o 5 8 1 13.20 15.98 1.12 o 1 9 1 108.91 108.81 1.99 o 2 9 1 3.37 4.41 0.88 o 3 9 1 3.96 2.97 0.88 o 4 9 1 7.73 8.32 1.00 o 0 10 1 100.08 106.48 4.31 o 1 10 1 39.29 42.39 2.18 o 2 10 1 55.98 57.42 1.71 o 3 10 1 50.02 53.44 1.67 o 1 11 1 18.40 16.23 1.27 o 1 0 2 0.83 0.29 0.44 o 2 0 2 6934.67 6728.60 53.08 o 3 0 2 482.47 443.52 5.34 o 4 0 2 2207.12 2131.59 17.83 o 5 0 2 409.10 382.11 5.61 o 6 0 2 30.45 25.14 1.48 o 7 0 2 100.44 98.24 3.22 o 8 0 2 45.64 56.40 2.87 o 1 1 2 10038.25 9539.40 62.09 o 2 1 2 763.07 733.17 4.90 o 3 1 2 1867.37 1855.37 11.00 o 4 1 2 13.21 13.78 0.55 o 5 1 2 113.73 117.29 1.90 o 6 1 2 0.74 0.15 0.63 o 7 1 2 1.89 -0.24 0.88 o 8 1 2 3.76 3.12 1.15 o 0 2 2 7379.03 7380.96 74.09 o 1 2 2 769.82 771.22 4.75 o 2 2 2 2264.42 2214.36 11.72 o 3 2 2 504.02 465.91 3.27 o 4 2 2 92.68 84.01 1.12 o 5 2 2 15.77 12.09 0.77 o 6 2 2 39.68 35.36 1.46 o 7 2 2 0.14 0.90 0.90 o 1 3 2 482.26 516.35 3.26 o 2 3 2 226.98 238.64 2.17 o 3 3 2 308.93 313.64 2.52 o 4 3 2 23.43 23.41 0.71 o 5 3 2 52.34 54.98 1.40 o 6 3 2 89.79 92.61 1.82 o 7 3 2 3.46 1.06 0.98 o 0 4 2 13.85 21.18 0.90 o 1 4 2 241.65 254.19 1.90 o 2 4 2 48.37 43.84 0.97 o 3 4 2 215.54 207.59 2.00 o 4 4 2 6.91 4.43 0.63 o 5 4 2 3.63 6.32 0.75 o 6 4 2 34.69 35.01 1.50 o 7 4 2 1.83 1.28 1.04 o 1 5 2 1685.85 1705.73 9.24 o 2 5 2 9.31 13.39 0.65 o 3 5 2 127.12 128.62 1.62 o 4 5 2 16.46 15.34 0.86 o 5 5 2 2.28 0.76 0.64 o 6 5 2 7.01 7.26 0.90 o 7 5 2 4.82 6.63 1.33 o 0 6 2 128.11 128.16 2.19 o 1 6 2 0.12 -0.51 0.50 o 2 6 2 77.54 78.61 1.33 o 3 6 2 8.56 10.45 0.83 o 4 6 2 18.84 15.41 0.88 o 5 6 2 23.74 24.18 1.20 o 6 6 2 6.12 6.55 0.98 o 1 7 2 17.64 20.71 0.96 o 2 7 2 8.86 10.88 0.79 o 3 7 2 41.42 49.30 1.24 o 4 7 2 1.85 2.21 0.70 o 5 7 2 4.76 4.78 0.86 o 6 7 2 2.85 3.25 1.03 o 0 8 2 99.64 86.97 2.44 o 1 8 2 10.12 11.24 0.96 o 2 8 2 196.33 186.80 2.46 o 3 8 2 27.60 28.66 1.26 o 4 8 2 189.13 188.18 2.44 o 5 8 2 5.61 6.00 0.99 o 1 9 2 117.67 116.46 2.07 o 2 9 2 25.90 27.37 1.24 o 3 9 2 22.50 21.43 1.20 o 4 9 2 8.06 6.57 0.99 o 0 10 2 299.55 320.29 5.15 o 1 10 2 0.08 -0.44 0.86 o 2 10 2 118.25 127.17 2.51 o 3 10 2 2.88 2.99 0.94 o 1 11 2 1.69 1.71 0.99 o 1 1 3 1604.83 1556.45 9.97 o 2 1 3 223.03 211.76 1.66 o 3 1 3 117.19 114.77 1.64 o 4 1 3 148.66 137.66 1.39 o 5 1 3 123.09 115.91 1.86 o 6 1 3 225.68 226.15 2.97 o 7 1 3 0.12 -0.15 0.85 o 8 1 3 47.98 52.15 2.89 o 0 2 3 321.40 309.17 3.10 o 1 2 3 1967.47 1976.36 11.41 o 2 2 3 715.43 705.39 4.41 o 3 2 3 1829.05 1784.25 10.00 o 4 2 3 421.90 420.19 3.04 o 5 2 3 109.42 107.54 1.95 o 6 2 3 95.09 87.31 2.54 o 7 2 3 1.44 0.82 0.78 o 1 3 3 5.93 4.81 0.37 o 2 3 3 637.34 655.11 3.90 o 3 3 3 245.97 221.36 1.84 o 4 3 3 161.03 157.32 1.68 o 5 3 3 142.38 132.63 2.40 o 6 3 3 19.53 17.52 1.13 o 7 3 3 38.84 36.64 1.66 o 0 4 3 16.93 14.19 0.70 o 1 4 3 13.77 15.20 0.54 o 2 4 3 100.59 98.69 1.14 o 3 4 3 12.66 13.22 0.58 o 4 4 3 50.65 54.86 1.14 o 5 4 3 30.56 31.92 1.92 o 6 4 3 0.22 0.42 0.65 o 7 4 3 0.01 0.94 1.06 o 1 5 3 706.45 740.90 4.62 o 2 5 3 259.94 258.46 2.45 o 3 5 3 89.82 95.86 1.53 o 4 5 3 84.22 84.14 1.51 o 5 5 3 30.92 33.15 1.48 o 6 5 3 2.69 2.32 0.74 o 7 5 3 42.16 42.75 1.97 o 0 6 3 69.97 75.43 1.60 o 1 6 3 113.99 106.82 1.48 o 2 6 3 0.32 0.25 0.55 o 3 6 3 227.60 221.25 2.39 o 4 6 3 44.17 44.67 1.16 o 5 6 3 32.85 30.07 1.22 o 6 6 3 17.39 17.67 1.26 o 1 7 3 68.48 73.61 1.49 o 2 7 3 0.14 -0.64 0.60 o 3 7 3 0.01 -0.31 0.62 o 4 7 3 24.65 24.72 1.04 o 5 7 3 10.90 11.87 1.16 o 6 7 3 31.09 30.56 1.71 o 0 8 3 808.41 768.08 8.29 o 1 8 3 2.00 2.63 0.79 o 2 8 3 357.86 334.05 3.51 o 3 8 3 43.99 45.99 1.39 o 4 8 3 42.24 40.37 1.36 o 5 8 3 44.83 40.77 1.60 o 1 9 3 43.16 43.57 1.42 o 2 9 3 2.44 2.41 0.85 o 3 9 3 1.31 1.31 0.84 o 4 9 3 13.47 12.75 1.16 o 0 10 3 0.95 0.40 1.19 o 1 10 3 11.13 10.91 1.31 o 2 10 3 9.23 10.23 1.12 o 3 10 3 15.03 15.43 1.21 o 1 11 3 0.00 0.07 0.96 o 1 0 4 840.29 788.95 7.27 o 2 0 4 360.35 308.51 3.58 o 3 0 4 488.25 482.79 4.55 o 4 0 4 1.80 1.10 0.87 o 5 0 4 2.15 2.66 1.01 o 6 0 4 16.21 17.99 1.66 o 7 0 4 28.89 25.51 2.53 o 1 1 4 1220.54 1248.37 8.16 o 2 1 4 39.63 42.52 0.69 o 3 1 4 83.56 78.86 0.99 o 4 1 4 341.84 323.34 2.71 o 5 1 4 6.35 7.75 0.77 o 6 1 4 178.30 179.38 2.45 o 7 1 4 15.33 16.14 1.06 o 0 2 4 21.43 19.19 0.70 o 1 2 4 239.92 223.38 1.92 o 2 2 4 3.98 5.17 0.40 o 3 2 4 98.41 91.57 1.08 o 4 2 4 24.02 25.06 0.90 o 5 2 4 29.23 27.43 1.06 o 6 2 4 8.94 8.83 0.89 o 7 2 4 26.33 24.36 1.57 o 1 3 4 179.70 171.94 2.13 o 2 3 4 461.35 456.56 3.01 o 3 3 4 19.34 18.68 0.59 o 4 3 4 114.60 113.92 1.50 o 5 3 4 69.85 69.33 1.50 o 6 3 4 2.45 2.98 0.78 o 7 3 4 20.26 18.74 1.34 o 0 4 4 512.11 589.07 5.76 o 1 4 4 95.19 104.55 1.16 o 2 4 4 4.56 5.95 0.48 o 3 4 4 62.36 58.96 1.00 o 4 4 4 90.56 88.42 1.43 o 5 4 4 2.36 3.40 0.76 o 6 4 4 4.61 2.84 0.92 o 7 4 4 1.12 1.41 0.99 o 1 5 4 856.29 900.25 5.33 o 2 5 4 3.16 3.10 0.53 o 3 5 4 549.76 551.93 4.28 o 4 5 4 14.59 15.64 0.87 o 5 5 4 103.38 102.92 1.97 o 6 5 4 12.12 15.12 1.26 o 7 5 4 0.20 0.78 1.04 o 0 6 4 616.44 644.37 5.94 o 1 6 4 23.53 26.47 1.04 o 2 6 4 208.66 215.31 2.51 o 3 6 4 19.50 21.37 0.90 o 4 6 4 5.41 6.54 0.79 o 5 6 4 1.86 2.28 0.94 o 6 6 4 2.15 2.04 0.97 o 1 7 4 317.24 334.16 3.20 o 2 7 4 289.13 279.10 2.74 o 3 7 4 42.19 44.88 1.28 o 4 7 4 80.25 78.16 2.13 o 5 7 4 5.37 6.62 1.10 o 6 7 4 0.70 1.53 1.03 o 0 8 4 1149.76 1071.81 10.70 o 1 8 4 7.00 7.30 0.89 o 2 8 4 520.34 501.77 4.40 o 3 8 4 9.04 8.70 0.90 o 4 8 4 47.36 47.41 1.61 o 5 8 4 0.16 -1.20 1.02 o 1 9 4 258.16 253.51 3.02 o 2 9 4 4.56 4.90 0.91 o 3 9 4 34.08 30.71 1.34 o 4 9 4 9.48 6.16 1.19 o 0 10 4 65.00 67.87 2.50 o 1 10 4 0.99 0.98 0.89 o 2 10 4 115.18 113.93 2.61 o 3 10 4 0.85 -0.44 0.91 o 1 1 5 66.26 61.25 0.90 o 2 1 5 433.43 442.35 3.24 o 3 1 5 119.41 136.75 1.48 o 4 1 5 26.85 29.85 0.89 o 5 1 5 26.64 26.13 1.00 o 6 1 5 13.29 13.71 1.00 o 7 1 5 0.13 0.14 0.87 o 0 2 5 76.36 101.91 1.47 o 1 2 5 34.03 33.09 0.64 o 2 2 5 81.45 87.66 1.06 o 3 2 5 109.15 119.95 1.38 o 4 2 5 28.23 28.16 1.04 o 5 2 5 410.40 396.08 3.79 o 6 2 5 0.00 -0.74 0.73 o 7 2 5 134.98 135.87 2.68 o 1 3 5 587.38 587.69 4.26 o 2 3 5 220.36 216.47 1.73 o 3 3 5 100.02 91.46 1.13 o 4 3 5 6.71 8.11 0.87 o 5 3 5 75.39 74.18 1.61 o 6 3 5 45.98 42.99 1.63 o 7 3 5 0.67 1.38 0.94 o 0 4 5 15.44 23.31 0.88 o 1 4 5 7.68 5.86 0.45 o 2 4 5 140.00 143.23 1.44 o 3 4 5 2.58 4.29 0.51 o 4 4 5 367.12 355.91 3.23 o 5 4 5 2.11 1.28 0.82 o 6 4 5 162.93 161.98 2.79 o 7 4 5 11.27 12.18 1.28 o 1 5 5 0.02 0.60 0.46 o 2 5 5 7.43 8.12 0.57 o 3 5 5 211.27 211.08 2.20 o 4 5 5 0.80 0.59 0.64 o 5 5 5 54.72 51.94 1.67 o 6 5 5 0.92 1.10 0.97 o 7 5 5 9.68 11.93 1.34 o 0 6 5 373.79 371.74 4.03 o 1 6 5 30.87 32.39 1.08 o 2 6 5 181.43 175.59 2.04 o 3 6 5 0.10 -0.31 0.56 o 4 6 5 35.38 37.86 1.32 o 5 6 5 116.57 115.64 2.81 o 6 6 5 21.59 24.61 1.53 o 1 7 5 71.00 60.21 1.49 o 2 7 5 19.17 16.85 0.90 o 3 7 5 32.84 30.11 1.06 o 4 7 5 3.54 1.09 0.73 o 5 7 5 3.45 3.35 1.03 o 6 7 5 0.04 0.98 1.05 o 0 8 5 0.04 -0.34 1.09 o 1 8 5 32.11 30.60 1.19 o 2 8 5 2.54 1.22 0.64 o 3 8 5 24.25 21.97 1.12 o 4 8 5 3.37 3.88 0.98 o 5 8 5 0.92 1.17 1.03 o 1 9 5 32.63 33.69 1.32 o 2 9 5 27.14 27.49 1.28 o 3 9 5 64.11 66.25 1.84 o 4 9 5 8.14 5.60 1.17 o 0 10 5 160.70 166.69 3.68 o 1 10 5 0.92 0.08 0.89 o 2 10 5 46.39 44.97 1.64 o 3 10 5 8.80 10.83 1.29 o 0 0 6 1438.48 1461.62 17.13 o 1 0 6 285.19 303.68 3.28 o 2 0 6 1289.51 1365.04 12.63 o 3 0 6 442.68 469.11 5.26 o 4 0 6 352.45 373.60 4.91 o 5 0 6 23.72 22.33 1.46 o 6 0 6 58.76 59.95 2.50 o 7 0 6 0.00 0.95 1.30 o 1 1 6 0.25 -0.06 0.30 o 2 1 6 273.65 283.02 2.34 o 3 1 6 28.20 27.78 0.75 o 4 1 6 25.86 28.87 1.00 o 5 1 6 8.36 7.95 0.84 o 6 1 6 1.06 0.21 0.78 o 7 1 6 0.25 -0.82 0.89 o 0 2 6 469.24 555.94 4.95 o 1 2 6 4.34 5.61 0.36 o 2 2 6 0.00 0.44 0.32 o 3 2 6 23.37 22.49 0.69 o 4 2 6 78.24 71.77 1.67 o 5 2 6 97.36 98.25 1.84 o 6 2 6 17.90 17.72 1.10 o 7 2 6 37.78 36.75 1.68 o 1 3 6 2125.38 2344.03 12.53 o 2 3 6 2.28 3.80 0.40 o 3 3 6 916.60 920.27 5.59 o 4 3 6 67.23 72.37 1.49 o 5 3 6 202.33 198.98 2.74 o 6 3 6 64.51 64.85 1.93 o 7 3 6 11.23 11.43 1.38 o 0 4 6 546.59 535.71 4.86 o 1 4 6 2.39 2.63 0.40 o 2 4 6 0.24 -0.01 0.40 o 3 4 6 4.26 6.10 0.70 o 4 4 6 232.37 214.50 3.05 o 5 4 6 0.79 0.86 0.81 o 6 4 6 12.04 11.01 1.12 o 7 4 6 0.38 0.56 1.08 o 1 5 6 403.14 403.84 2.92 o 2 5 6 160.30 158.45 2.04 o 3 5 6 122.01 123.82 1.77 o 4 5 6 10.89 13.29 1.09 o 5 5 6 12.51 16.56 1.20 o 6 5 6 17.96 17.22 1.33 o 0 6 6 176.19 187.21 2.68 o 1 6 6 78.16 73.19 1.48 o 2 6 6 307.71 307.86 2.77 o 3 6 6 236.27 231.86 2.71 o 4 6 6 247.94 246.17 3.38 o 5 6 6 99.20 99.61 2.41 o 6 6 6 20.34 18.31 1.50 o 1 7 6 470.48 429.33 3.94 o 2 7 6 79.58 81.41 1.50 o 3 7 6 106.33 96.88 2.01 o 4 7 6 2.75 3.36 0.97 o 5 7 6 1.75 1.50 1.03 o 0 8 6 102.00 87.73 2.42 o 1 8 6 5.91 5.89 0.80 o 2 8 6 109.59 103.34 1.84 o 3 8 6 47.28 46.15 1.69 o 4 8 6 80.46 85.66 2.24 o 5 8 6 53.63 55.48 2.03 o 1 9 6 93.70 85.68 1.83 o 2 9 6 7.69 6.24 1.28 o 3 9 6 66.46 69.87 2.09 o 4 9 6 0.06 0.50 1.15 o 0 10 6 12.46 12.18 1.59 o 1 10 6 0.44 0.09 0.90 o 2 10 6 0.72 0.35 0.98 o 1 1 7 389.13 434.16 3.19 o 2 1 7 0.88 0.83 0.34 o 3 1 7 106.92 118.94 1.54 o 4 1 7 0.81 1.33 0.59 o 5 1 7 1.60 0.23 0.74 o 6 1 7 3.97 2.84 0.87 o 7 1 7 0.94 1.44 0.99 o 0 2 7 102.12 114.13 1.68 o 1 2 7 306.03 344.22 2.38 o 2 2 7 40.35 38.34 0.72 o 3 2 7 282.20 282.84 2.51 o 4 2 7 5.60 4.94 0.74 o 5 2 7 34.12 32.21 1.29 o 6 2 7 0.14 0.75 0.86 o 7 2 7 22.36 27.72 1.58 o 1 3 7 71.69 76.78 1.05 o 2 3 7 1.44 1.86 0.40 o 3 3 7 124.03 114.97 1.66 o 4 3 7 0.51 -0.17 0.66 o 5 3 7 21.23 22.41 1.17 o 6 3 7 2.51 1.91 1.08 o 7 3 7 26.18 29.33 1.88 o 0 4 7 0.62 1.26 0.59 o 1 4 7 5.64 4.87 0.46 o 2 4 7 0.07 0.72 0.45 o 3 4 7 11.65 10.21 0.77 o 4 4 7 11.11 9.81 0.93 o 5 4 7 18.32 19.62 1.23 o 6 4 7 4.76 4.03 1.10 o 7 4 7 10.70 12.23 1.45 o 1 5 7 30.25 35.00 0.91 o 2 5 7 0.73 1.52 0.56 o 3 5 7 376.58 357.61 3.56 o 4 5 7 2.44 2.70 0.87 o 5 5 7 339.86 339.01 4.34 o 6 5 7 3.65 5.70 1.22 o 0 6 7 0.85 0.87 0.77 o 1 6 7 192.65 182.68 2.14 o 2 6 7 1.28 0.79 0.67 o 3 6 7 344.87 327.62 3.50 o 4 6 7 0.00 -1.24 0.88 o 5 6 7 4.03 4.87 1.23 o 6 6 7 0.09 0.62 1.07 o 1 7 7 21.84 21.08 1.00 o 2 7 7 0.09 -0.68 0.63 o 3 7 7 0.30 -0.16 0.64 o 4 7 7 0.82 -0.27 0.88 o 5 7 7 0.03 0.69 1.01 o 0 8 7 3.08 0.51 0.98 o 1 8 7 40.48 42.68 1.43 o 2 8 7 5.90 7.09 0.93 o 3 8 7 30.65 35.69 1.58 o 4 8 7 5.03 5.17 1.11 o 1 9 7 88.96 89.09 2.02 o 2 9 7 1.90 2.27 0.91 o 3 9 7 0.93 0.47 0.99 o 0 10 7 1.05 -1.87 1.25 o 1 10 7 8.59 11.65 1.21 o 2 10 7 3.13 3.87 1.06 o 0 0 8 627.28 679.85 8.86 o 1 0 8 9.40 9.46 0.65 o 2 0 8 59.15 51.21 1.13 o 3 0 8 30.73 26.01 1.45 o 4 0 8 6.97 7.76 1.18 o 5 0 8 18.40 18.69 1.65 o 6 0 8 1.03 0.27 1.18 o 7 0 8 3.18 0.39 1.32 o 1 1 8 145.01 173.05 1.58 o 2 1 8 338.47 368.43 2.97 o 3 1 8 16.32 18.53 0.89 o 4 1 8 48.34 49.01 1.60 o 5 1 8 0.07 -0.80 0.75 o 6 1 8 0.29 -0.53 0.82 o 7 1 8 0.68 -1.19 0.97 o 0 2 8 2421.77 2644.16 20.41 o 1 2 8 0.04 0.29 0.39 o 2 2 8 858.95 941.04 6.29 o 3 2 8 21.11 22.91 0.92 o 4 2 8 61.85 64.23 1.55 o 5 2 8 21.35 20.73 1.29 o 6 2 8 14.95 16.32 1.26 o 7 2 8 7.23 8.81 1.22 o 1 3 8 1016.52 1085.34 6.31 o 2 3 8 14.53 16.50 0.76 o 3 3 8 310.97 317.60 3.18 o 4 3 8 10.16 10.30 0.90 o 5 3 8 46.28 48.30 1.63 o 6 3 8 12.60 9.84 1.35 o 7 3 8 6.40 5.78 1.31 o 0 4 8 0.00 0.41 0.58 o 1 4 8 16.41 17.72 0.72 o 2 4 8 276.77 281.68 2.62 o 3 4 8 11.26 10.05 0.90 o 4 4 8 643.54 653.08 6.21 o 5 4 8 1.30 0.85 0.93 o 6 4 8 83.79 89.70 2.53 o 1 5 8 452.83 437.37 3.35 o 2 5 8 319.14 308.20 2.73 o 3 5 8 140.60 138.44 2.23 o 4 5 8 139.44 140.58 2.50 o 5 5 8 25.65 23.33 1.39 o 6 5 8 1.89 2.05 1.20 o 0 6 8 23.96 24.54 1.21 o 1 6 8 31.78 35.97 1.13 o 2 6 8 89.92 85.51 1.72 o 3 6 8 91.80 93.77 1.85 o 4 6 8 87.21 92.85 2.27 o 5 6 8 31.23 38.67 1.70 o 6 6 8 0.79 2.40 1.23 o 1 7 8 150.77 137.31 2.34 o 2 7 8 12.93 14.60 0.97 o 3 7 8 13.05 11.37 1.01 o 4 7 8 50.19 55.14 1.92 o 5 7 8 0.88 1.03 1.06 o 0 8 8 10.28 11.86 1.49 o 1 8 8 7.25 7.94 0.95 o 2 8 8 13.12 13.04 1.07 o 3 8 8 31.82 33.29 1.56 o 4 8 8 13.11 15.66 1.46 o 1 9 8 77.98 78.07 1.94 o 2 9 8 13.67 11.21 1.18 o 3 9 8 46.49 46.23 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9 2.97 0.91 0.95 o 5 6 9 99.79 102.61 3.37 o 1 7 9 12.18 16.69 1.04 o 2 7 9 2.02 3.02 0.78 o 3 7 9 15.73 17.51 1.28 o 4 7 9 0.35 -0.60 0.94 o 5 7 9 3.18 3.01 1.24 o 0 8 9 0.01 -1.65 1.10 o 1 8 9 25.77 25.79 1.31 o 2 8 9 1.08 0.99 0.94 o 3 8 9 30.31 27.32 1.69 o 4 8 9 0.05 -1.51 1.01 o 1 9 9 17.41 16.57 1.32 o 2 9 9 11.91 14.34 1.39 o 3 9 9 42.41 41.95 2.16 o 0 0 10 35.84 39.56 1.59 o 1 0 10 104.32 101.51 1.84 o 2 0 10 244.76 256.35 4.11 o 3 0 10 292.97 303.09 4.88 o 4 0 10 165.48 155.26 3.56 o 5 0 10 30.95 35.89 2.13 o 6 0 10 23.21 21.06 2.01 o 7 0 10 0.21 1.12 1.51 o 1 1 10 550.62 618.80 4.17 o 2 1 10 2.03 1.71 0.63 o 3 1 10 114.29 123.00 2.09 o 4 1 10 43.83 44.05 1.48 o 5 1 10 0.38 -0.41 0.81 o 6 1 10 34.41 35.03 1.64 o 0 2 10 102.59 113.15 1.85 o 1 2 10 14.64 13.07 0.60 o 2 2 10 111.25 117.25 2.02 o 3 2 10 4.68 5.57 0.81 o 4 2 10 60.74 65.36 1.73 o 5 2 10 26.74 28.48 1.58 o 6 2 10 10.38 11.26 1.23 o 1 3 10 15.49 11.09 0.63 o 2 3 10 34.41 39.80 1.13 o 3 3 10 0.15 0.96 0.73 o 4 3 10 3.03 2.26 0.93 o 5 3 10 13.77 13.15 1.18 o 6 3 10 17.66 22.22 1.88 o 0 4 10 821.59 869.10 8.56 o 1 4 10 15.89 16.20 0.75 o 2 4 10 173.46 183.04 2.60 o 3 4 10 9.62 11.97 1.06 o 4 4 10 3.66 3.47 0.91 o 5 4 10 9.27 8.38 1.24 o 6 4 10 1.14 0.48 1.07 o 1 5 10 425.93 410.20 3.71 o 2 5 10 0.01 0.78 0.67 o 3 5 10 273.50 268.04 3.42 o 4 5 10 25.60 27.04 1.63 o 5 5 10 69.63 74.72 2.37 o 6 5 10 44.30 48.46 2.34 o 0 6 10 0.36 2.07 0.98 o 1 6 10 28.89 29.07 1.19 o 2 6 10 31.86 34.97 1.26 o 3 6 10 49.43 48.80 2.21 o 4 6 10 74.01 74.97 2.44 o 5 6 10 1.03 0.98 1.09 o 1 7 10 311.94 311.38 4.46 o 2 7 10 171.21 164.59 3.63 o 3 7 10 53.61 58.30 1.86 o 4 7 10 53.35 51.98 2.59 o 0 8 10 128.83 157.24 3.84 o 1 8 10 0.25 1.68 0.92 o 2 8 10 39.62 47.94 1.93 o 3 8 10 0.15 0.43 1.19 o 1 9 10 47.29 46.96 1.91 o 2 9 10 0.16 0.48 1.12 o 1 1 11 49.21 48.44 0.99 o 2 1 11 2.57 2.41 0.68 o 3 1 11 33.73 28.81 1.22 o 4 1 11 17.94 17.64 1.14 o 5 1 11 45.74 43.61 1.65 o 6 1 11 61.14 60.15 2.08 o 0 2 11 22.95 24.27 1.11 o 1 2 11 170.08 169.38 1.96 o 2 2 11 9.75 9.84 0.86 o 3 2 11 258.07 250.02 3.19 o 4 2 11 13.14 11.27 1.02 o 5 2 11 18.33 20.41 1.33 o 6 2 11 9.92 9.58 1.24 o 1 3 11 11.29 13.49 0.77 o 2 3 11 210.52 211.64 2.80 o 3 3 11 69.06 69.84 1.85 o 4 3 11 73.06 72.08 2.17 o 5 3 11 93.34 96.04 2.66 o 6 3 11 0.90 0.50 1.17 o 0 4 11 118.61 121.23 2.47 o 1 4 11 4.94 4.51 0.71 o 2 4 11 124.14 124.44 2.29 o 3 4 11 17.02 14.02 1.23 o 4 4 11 96.99 106.95 2.82 o 5 4 11 11.12 11.89 1.94 o 6 4 11 23.34 25.43 1.75 o 1 5 11 116.03 106.83 2.22 o 2 5 11 97.84 98.58 2.15 o 3 5 11 8.49 9.22 1.08 o 4 5 11 27.98 30.47 1.66 o 5 5 11 6.68 6.81 1.58 o 0 6 11 139.57 132.06 3.14 o 1 6 11 38.67 39.70 1.31 o 2 6 11 39.81 37.92 1.67 o 3 6 11 84.62 81.84 2.51 o 4 6 11 1.18 2.12 1.11 o 5 6 11 9.90 9.52 1.48 o 1 7 11 82.52 92.95 2.14 o 2 7 11 0.03 -0.90 0.98 o 3 7 11 14.52 14.56 1.42 o 4 7 11 9.12 13.19 1.48 o 0 8 11 203.74 201.47 6.13 o 1 8 11 0.52 -0.07 0.94 o 2 8 11 73.41 82.64 2.75 o 3 8 11 18.49 23.30 2.18 o 1 9 11 2.73 2.44 1.12 o 0 0 12 60.31 58.61 2.74 o 1 0 12 4.54 3.45 1.20 o 2 0 12 210.99 198.91 3.73 o 3 0 12 40.60 37.87 1.95 o 4 0 12 145.07 140.40 4.66 o 5 0 12 110.43 111.21 3.91 o 6 0 12 0.22 0.66 1.42 o 1 1 12 450.14 463.34 4.33 o 2 1 12 0.87 1.14 0.68 o 3 1 12 134.52 132.73 2.30 o 4 1 12 29.99 30.76 1.40 o 5 1 12 16.14 16.00 1.25 o 6 1 12 32.21 33.42 1.71 o 0 2 12 69.12 66.94 2.33 o 1 2 12 44.79 42.32 1.26 o 2 2 12 17.29 18.17 1.03 o 3 2 12 79.55 79.04 1.86 o 4 2 12 5.66 4.36 0.93 o 5 2 12 2.00 0.65 0.93 o 6 2 12 1.45 3.01 1.09 o 1 3 12 169.60 156.58 2.35 o 2 3 12 67.10 62.19 2.49 o 3 3 12 121.22 121.94 2.26 o 4 3 12 6.70 5.09 1.02 o 5 3 12 56.15 55.92 2.01 o 6 3 12 1.49 2.61 1.23 o 0 4 12 232.14 238.01 3.91 o 1 4 12 47.88 41.38 1.40 o 2 4 12 241.53 244.61 3.60 o 3 4 12 87.34 83.91 2.19 o 4 4 12 92.13 88.52 2.26 o 5 4 12 2.11 2.57 1.11 o 1 5 12 312.56 277.18 3.40 o 2 5 12 1.54 0.02 0.91 o 3 5 12 45.21 52.43 1.92 o 4 5 12 0.15 0.26 0.98 o 5 5 12 0.05 -0.48 1.09 o 0 6 12 292.16 259.77 4.09 o 1 6 12 1.09 0.94 0.82 o 2 6 12 169.23 164.89 3.78 o 3 6 12 0.33 1.56 1.16 o 4 6 12 44.80 46.33 2.03 o 1 7 12 0.11 0.85 0.94 o 2 7 12 7.52 5.83 1.33 o 3 7 12 12.39 16.98 1.71 o 0 8 12 46.29 40.81 2.34 o 1 8 12 1.14 0.07 1.07 o 2 8 12 6.30 1.97 1.39 o 1 1 13 113.54 114.76 2.65 o 2 1 13 87.56 81.74 2.92 o 3 1 13 5.93 6.98 0.92 o 4 1 13 50.49 49.68 1.80 o 5 1 13 5.34 5.27 1.06 o 6 1 13 1.86 2.41 1.09 o 0 2 13 72.50 70.19 2.29 o 1 2 13 24.21 26.67 1.55 o 2 2 13 71.28 69.96 1.92 o 3 2 13 8.26 7.70 0.94 o 4 2 13 88.55 79.07 2.04 o 5 2 13 20.67 23.65 1.47 o 1 3 13 4.17 5.46 0.97 o 2 3 13 13.01 11.81 1.16 o 3 3 13 0.01 -0.01 0.90 o 4 3 13 68.55 72.46 2.78 o 5 3 13 7.56 5.38 1.20 o 0 4 13 24.89 18.40 1.68 o 1 4 13 7.93 5.38 0.95 o 2 4 13 17.53 18.95 1.33 o 3 4 13 19.79 18.18 1.40 o 4 4 13 12.09 14.11 1.34 o 5 4 13 0.17 0.03 1.04 o 1 5 13 12.53 9.81 1.13 o 2 5 13 15.26 11.72 1.30 o 3 5 13 0.67 0.03 1.09 o 4 5 13 0.21 0.02 1.08 o 0 6 13 1.56 2.15 1.05 o 1 6 13 0.76 0.62 0.83 o 2 6 13 14.26 15.81 1.54 o 3 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14 0.29 -0.85 1.07 o 2 6 14 58.92 57.30 2.35 o 3 6 14 0.01 0.58 1.22 o 1 7 14 2.13 0.84 1.83 o 2 7 14 0.09 -1.72 1.15 o 1 1 15 229.17 239.99 4.06 o 2 1 15 41.03 41.76 1.97 o 3 1 15 1.59 1.39 1.15 o 4 1 15 39.14 37.37 1.84 o 5 1 15 0.01 0.16 0.99 o 0 2 15 8.22 3.57 1.59 o 1 2 15 13.41 13.99 1.44 o 2 2 15 0.00 1.13 1.09 o 3 2 15 4.11 3.62 1.29 o 4 2 15 9.81 12.20 1.37 o 5 2 15 8.94 9.52 1.34 o 1 3 15 4.26 3.36 1.18 o 2 3 15 36.41 30.44 1.86 o 3 3 15 29.65 27.53 1.78 o 4 3 15 41.07 44.55 2.02 o 0 4 15 14.91 17.77 2.72 o 1 4 15 17.16 14.44 1.50 o 2 4 15 12.68 14.44 1.62 o 3 4 15 33.06 31.05 1.75 o 4 4 15 5.03 4.95 1.39 o 1 5 15 10.57 9.91 1.58 o 2 5 15 4.83 2.80 1.26 o 3 5 15 1.11 0.80 1.16 o 0 6 15 19.76 22.67 2.97 o 1 6 15 0.00 -0.64 1.64 o 2 6 15 6.64 4.83 1.41 o 1 7 15 0.13 -0.51 1.88 o 0 0 16 177.46 195.08 12.31 o 1 0 16 1.29 1.12 1.58 o 2 0 16 11.92 12.71 2.12 o 3 0 16 0.06 1.07 1.74 o 4 0 16 12.85 17.81 2.56 o 1 1 16 270.63 247.79 4.27 o 2 1 16 18.50 24.14 1.78 o 3 1 16 142.03 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