# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' k12kcm03' _shelx_refln_list_code 4 _shelx_F_calc_maximum 391.43 _exptl_crystal_F_000 1112.00 _reflns_d_resolution_high 0.7705 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.0258 _cell_length_b 13.8500 _cell_length_c 16.0177 _cell_angle_alpha 74.074 _cell_angle_beta 89.742 _cell_angle_gamma 77.291 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3099.74 2494.41 409.70 o 3 0 0 988.74 1004.87 22.68 o 4 0 0 6762.60 6921.63 144.95 o 5 0 0 220.00 312.88 12.42 o 6 0 0 12987.71 13858.06 283.31 o 7 0 0 259.27 240.38 15.02 o 8 0 0 1102.68 1172.71 31.75 o 9 0 0 727.72 827.10 28.38 o 10 0 0 12798.43 14089.53 327.62 o 11 0 0 2.57 -22.43 31.32 o 12 0 0 423.56 389.52 50.66 o 13 0 0 7.86 56.36 58.64 o -13 1 0 2.07 40.58 53.83 o -12 1 0 72.12 47.86 43.19 o -11 1 0 20.93 -13.78 36.33 o -10 1 0 8388.93 8669.08 489.20 o -9 1 0 1536.59 1553.54 40.33 o -8 1 0 309.66 455.66 22.52 o -7 1 0 1949.41 2094.84 46.87 o -6 1 0 13139.00 13110.43 318.82 o -5 1 0 2143.46 2734.97 50.83 o -4 1 0 6040.05 6741.83 128.66 o -3 1 0 639.85 820.90 18.03 o -2 1 0 20.13 57.28 11.19 o 2 1 0 1493.44 1205.15 234.24 o 3 1 0 12.63 51.02 6.44 o 4 1 0 8165.34 8812.92 210.63 o 5 1 0 87.48 75.51 8.68 o 6 1 0 18061.25 20080.68 461.30 o 7 1 0 16.10 -8.97 10.46 o 8 1 0 53.79 20.71 17.40 o 9 1 0 190.58 265.71 22.17 o 10 1 0 13075.36 14594.86 409.51 o 11 1 0 112.80 144.07 27.42 o 12 1 0 664.04 708.79 54.06 o 13 1 0 22.60 -34.54 78.29 o 14 1 0 1682.42 1479.81 231.95 o -13 2 0 0.67 57.48 109.98 o -12 2 0 12.94 131.26 70.51 o -11 2 0 203.19 248.65 55.33 o -10 2 0 4970.65 4840.21 121.13 o -9 2 0 1822.97 1993.12 52.55 o -8 2 0 1951.06 1992.15 42.86 o -7 2 0 3188.15 3348.61 60.39 o -6 2 0 10569.57 10561.27 195.60 o -5 2 0 485.46 531.83 29.11 o -4 2 0 9827.51 10090.73 167.54 o -3 2 0 730.76 646.30 13.97 o -2 2 0 435.85 518.69 14.28 o -1 2 0 2445.71 1971.03 166.93 o 1 2 0 3448.68 1113.48 1539.87 o 2 2 0 54.27 77.18 9.07 o 3 2 0 1396.55 1544.27 38.55 o 4 2 0 5553.15 5419.24 123.36 o 5 2 0 5.56 78.05 14.53 o 6 2 0 23554.47 26583.36 608.15 o 7 2 0 1.60 20.75 17.76 o 8 2 0 74.34 103.05 14.05 o 9 2 0 27.45 22.21 22.08 o 10 2 0 10235.87 11528.15 322.69 o 11 2 0 9.30 -26.23 27.79 o 12 2 0 767.53 801.13 54.53 o 13 2 0 61.91 95.60 148.71 o 14 2 0 2322.60 2444.12 183.85 o -13 3 0 115.22 201.17 71.98 o -12 3 0 194.33 189.28 43.86 o -11 3 0 183.01 219.33 47.76 o -10 3 0 3582.89 3585.82 105.45 o -9 3 0 403.33 531.83 34.34 o -8 3 0 5504.88 5573.73 99.59 o -7 3 0 2040.45 2134.09 42.69 o -6 3 0 5287.86 5091.22 88.63 o -5 3 0 596.80 598.27 15.51 o -4 3 0 5402.06 5966.44 107.05 o -3 3 0 88.24 131.54 10.84 o -2 3 0 193.01 205.79 8.27 o -1 3 0 4613.58 4039.26 95.52 o 0 3 0 129387.17 120551.45 7348.72 o 1 3 0 3967.56 3543.30 87.24 o 2 3 0 289.02 347.06 15.30 o 3 3 0 899.81 983.17 49.45 o 4 3 0 7019.88 7236.70 207.13 o 5 3 0 782.92 1107.69 28.98 o 6 3 0 13603.31 15839.00 380.84 o 7 3 0 75.10 123.11 14.38 o 8 3 0 55.47 38.10 12.67 o 9 3 0 25.91 39.24 15.07 o 10 3 0 9119.49 9640.56 278.04 o 11 3 0 40.26 13.68 32.58 o 12 3 0 618.22 702.15 70.84 o 13 3 0 1.16 -51.21 51.21 o 14 3 0 2619.55 2647.64 254.22 o -12 4 0 15.97 9.92 87.85 o -11 4 0 95.73 85.61 68.09 o -10 4 0 2715.59 2752.81 85.46 o -9 4 0 272.28 350.30 41.81 o -8 4 0 1520.14 1481.88 42.15 o -7 4 0 795.45 738.61 22.76 o -6 4 0 9419.03 8829.24 277.17 o -5 4 0 8.40 15.01 10.26 o -4 4 0 2075.85 2099.07 60.97 o -3 4 0 92.28 141.25 13.39 o -2 4 0 1479.38 1367.72 30.71 o -1 4 0 2292.56 2125.33 45.19 o 0 4 0 41603.37 39366.44 953.39 o 1 4 0 5318.54 4548.93 95.12 o 2 4 0 18.78 55.75 11.90 o 3 4 0 281.77 260.91 23.34 o 4 4 0 9026.51 9763.47 270.74 o 5 4 0 4993.11 5376.77 123.66 o 6 4 0 10847.18 11087.81 277.88 o 7 4 0 11.99 -7.73 34.19 o 8 4 0 742.49 764.00 38.32 o 9 4 0 389.00 442.61 34.44 o 10 4 0 12249.09 14064.62 486.10 o 11 4 0 67.54 60.53 37.96 o 12 4 0 591.16 669.48 105.23 o 13 4 0 2.60 -44.36 44.36 o 14 4 0 2443.59 2691.26 163.82 o -12 5 0 97.94 151.88 62.18 o -11 5 0 156.47 128.53 59.56 o -10 5 0 2255.27 2237.75 146.06 o -9 5 0 111.19 78.10 49.23 o -8 5 0 2342.92 2358.69 59.89 o -7 5 0 1210.74 1216.71 34.03 o -6 5 0 5416.25 4846.97 121.89 o -5 5 0 2.06 -11.29 12.32 o -4 5 0 2804.01 2556.34 47.76 o -3 5 0 368.18 435.66 17.29 o -2 5 0 373.58 392.98 12.06 o -1 5 0 4653.83 4364.24 70.50 o 0 5 0 78783.17 79307.54 1893.50 o 1 5 0 3453.16 3092.21 57.61 o 2 5 0 668.86 728.56 22.93 o 3 5 0 722.98 644.13 22.10 o 4 5 0 4669.08 4873.70 137.20 o 5 5 0 3.51 -19.73 26.13 o 6 5 0 15117.43 15267.97 334.50 o 7 5 0 1013.22 1233.60 35.20 o 8 5 0 2408.57 2493.37 62.60 o 9 5 0 1062.50 1208.85 50.50 o 10 5 0 13162.90 13900.18 831.94 o 11 5 0 238.30 285.61 71.54 o 12 5 0 512.56 551.20 140.60 o 13 5 0 1.06 96.95 60.74 o 14 5 0 2862.03 3238.10 184.33 o -11 6 0 20.83 166.62 57.09 o -10 6 0 1867.62 2028.22 99.41 o -9 6 0 64.32 224.68 67.34 o -8 6 0 2762.29 2798.68 86.83 o -7 6 0 2276.82 2304.98 54.73 o -6 6 0 1563.62 1473.46 33.98 o -5 6 0 2.44 14.03 13.67 o -4 6 0 4747.43 4949.98 120.99 o -3 6 0 907.00 800.07 18.16 o -2 6 0 399.99 329.47 12.57 o -1 6 0 395.85 407.81 14.76 o 0 6 0 26805.74 28611.47 614.16 o 1 6 0 3549.27 3109.12 66.31 o 2 6 0 243.01 208.04 11.49 o 3 6 0 100.01 134.07 12.17 o 4 6 0 3715.07 3956.33 132.73 o 5 6 0 264.08 214.24 19.66 o 6 6 0 4188.98 3936.11 84.43 o 7 6 0 1808.79 1929.08 48.53 o 8 6 0 938.53 984.46 36.03 o 9 6 0 687.89 782.26 59.47 o 10 6 0 7599.58 8361.55 880.57 o 11 6 0 17.88 -8.64 39.74 o 12 6 0 335.61 183.85 59.28 o 13 6 0 23.44 -7.27 68.04 o 14 6 0 2376.14 2046.85 243.74 o -11 7 0 67.10 53.66 56.14 o -10 7 0 1192.75 1069.92 125.46 o -9 7 0 162.00 293.98 69.58 o -8 7 0 1636.07 1725.16 81.96 o -7 7 0 1118.46 954.52 45.60 o -6 7 0 3200.69 2967.05 65.36 o -5 7 0 35.33 51.64 16.09 o -4 7 0 2578.29 2825.68 57.17 o -3 7 0 932.68 883.34 25.93 o -2 7 0 1041.10 968.83 23.30 o -1 7 0 115.30 71.06 10.86 o 0 7 0 5456.52 5436.52 113.90 o 1 7 0 1.44 32.34 10.46 o 2 7 0 152.54 155.04 17.98 o 3 7 0 227.69 247.59 16.38 o 4 7 0 3248.42 3073.77 83.83 o 5 7 0 278.00 240.03 23.84 o 6 7 0 8086.86 8032.03 268.24 o 7 7 0 2722.78 2609.33 58.02 o 8 7 0 2852.92 2906.19 87.56 o 9 7 0 1783.41 1999.81 107.68 o 10 7 0 5872.67 5539.61 234.36 o 11 7 0 0.77 55.72 46.97 o 12 7 0 182.73 152.97 58.19 o 13 7 0 82.89 47.97 104.81 o 14 7 0 1300.81 920.86 250.63 o -10 8 0 814.84 651.92 64.19 o -9 8 0 288.86 455.11 55.13 o -8 8 0 2377.87 2484.80 99.83 o -7 8 0 1130.13 1040.83 63.06 o -6 8 0 3167.33 3036.96 70.85 o -5 8 0 244.40 226.74 21.59 o -4 8 0 848.13 840.54 33.49 o -3 8 0 1125.90 1068.09 25.06 o -2 8 0 680.84 616.19 21.06 o -1 8 0 201.88 227.28 14.30 o 0 8 0 4430.03 4976.77 113.86 o 1 8 0 5.16 -6.21 14.64 o 2 8 0 802.46 731.96 22.05 o 3 8 0 1398.43 1274.00 41.53 o 4 8 0 3670.16 3731.46 104.87 o 5 8 0 8.30 7.56 13.74 o 6 8 0 8681.60 8155.76 221.81 o 7 8 0 252.34 275.33 20.84 o 8 8 0 4629.75 4592.06 201.79 o 9 8 0 1454.44 1508.13 56.57 o 10 8 0 4388.66 4078.85 130.32 o 11 8 0 85.69 119.02 52.62 o 12 8 0 16.83 4.52 54.48 o 13 8 0 9.66 93.63 72.10 o -10 9 0 755.60 753.95 87.24 o -9 9 0 723.00 648.35 61.47 o -8 9 0 964.38 995.00 67.34 o -7 9 0 846.82 924.54 57.67 o -6 9 0 2171.18 2107.68 70.95 o -5 9 0 253.63 163.14 22.55 o -4 9 0 1530.23 1534.40 41.85 o -3 9 0 3027.10 2853.34 61.18 o -2 9 0 2536.14 2379.89 53.89 o -1 9 0 2235.16 1969.97 46.85 o 0 9 0 910.55 1040.78 29.20 o 1 9 0 12.45 13.77 12.43 o 2 9 0 218.11 239.40 23.54 o 3 9 0 917.79 932.38 31.16 o 4 9 0 4301.03 4226.52 146.34 o 5 9 0 487.25 413.42 23.65 o 6 9 0 1408.88 1220.98 37.79 o 7 9 0 254.47 274.05 32.10 o 8 9 0 2752.86 2823.14 77.93 o 9 9 0 127.94 93.00 22.65 o 10 9 0 2024.46 1816.83 73.58 o 11 9 0 80.61 103.72 65.38 o 12 9 0 53.73 45.69 85.10 o 13 9 0 0.23 42.43 73.23 o -9 10 0 837.74 591.96 103.46 o -8 10 0 171.85 167.44 160.04 o -7 10 0 540.60 634.16 196.76 o -6 10 0 1797.28 1568.81 77.59 o -5 10 0 147.41 218.66 43.43 o -4 10 0 1911.78 2066.59 73.18 o -3 10 0 2613.01 2547.65 57.59 o -2 10 0 417.65 460.73 36.62 o -1 10 0 5005.62 4519.48 87.92 o 0 10 0 3290.22 3731.40 87.95 o 1 10 0 4137.77 3376.52 69.56 o 2 10 0 1367.23 1394.43 42.23 o 3 10 0 2172.53 2069.54 47.59 o 4 10 0 1435.79 1280.11 65.01 o 5 10 0 106.16 117.52 24.65 o 6 10 0 2844.44 2726.12 84.11 o 7 10 0 2196.34 2336.63 76.20 o 8 10 0 3083.72 2874.59 109.27 o 9 10 0 10.94 2.25 22.38 o 10 10 0 1678.42 1593.01 88.02 o 11 10 0 88.94 129.50 54.60 o 12 10 0 102.39 -31.66 70.32 o 13 10 0 86.25 147.66 79.48 o -8 11 0 5.10 -33.74 60.40 o -7 11 0 658.01 626.35 112.59 o -6 11 0 1503.07 1390.78 97.45 o -5 11 0 69.38 104.39 37.27 o -4 11 0 1098.95 1351.41 186.18 o -3 11 0 1534.19 1642.38 55.81 o -2 11 0 120.81 81.86 33.30 o -1 11 0 357.61 313.45 23.66 o 0 11 0 3713.02 4379.27 127.99 o 1 11 0 3152.40 2743.57 74.58 o 2 11 0 1458.57 1454.38 56.08 o 3 11 0 2047.60 1911.72 58.44 o 4 11 0 1385.78 1450.53 55.91 o 5 11 0 246.13 267.11 58.67 o 6 11 0 3373.99 3132.35 100.22 o 7 11 0 1024.31 1014.22 65.28 o 8 11 0 2291.92 2415.57 88.99 o 9 11 0 13.30 8.81 23.21 o 10 11 0 1234.88 1132.24 79.27 o 11 11 0 148.10 183.66 66.01 o 12 11 0 4.93 6.09 130.02 o -7 12 0 245.81 157.94 57.26 o -6 12 0 1167.46 1144.80 77.73 o -5 12 0 0.47 59.87 44.51 o -4 12 0 1223.55 1560.56 120.05 o -3 12 0 2130.94 2265.58 131.42 o -2 12 0 1117.59 1306.13 50.83 o -1 12 0 1079.27 1043.14 44.98 o 0 12 0 2446.99 3041.10 93.92 o 1 12 0 724.70 771.90 41.34 o 2 12 0 38.91 68.98 41.66 o 3 12 0 1145.03 1209.56 53.36 o 4 12 0 2932.51 3262.97 79.51 o 5 12 0 60.65 44.36 25.39 o 6 12 0 1905.19 1712.43 58.37 o 7 12 0 1150.95 1132.65 80.36 o 8 12 0 1970.65 1939.29 82.74 o 9 12 0 75.58 76.25 46.78 o 10 12 0 1218.09 1055.18 84.73 o 11 12 0 138.26 160.21 147.17 o 12 12 0 6.81 129.91 97.68 o -6 13 0 590.40 481.79 86.17 o -5 13 0 5.44 37.92 82.26 o -4 13 0 1024.36 1205.32 78.40 o -3 13 0 1379.62 1574.06 180.50 o -2 13 0 393.54 471.14 92.46 o -1 13 0 2481.02 2782.25 102.03 o 0 13 0 3081.75 4159.14 146.66 o 1 13 0 2556.74 2540.34 107.83 o 2 13 0 371.96 486.16 46.09 o 3 13 0 1428.65 1580.10 75.88 o 4 13 0 1309.40 1430.94 56.27 o 5 13 0 4.72 4.72 20.19 o 6 13 0 1885.95 1909.37 92.34 o 7 13 0 733.47 738.46 50.79 o 8 13 0 1786.23 1629.84 76.64 o 9 13 0 108.19 -62.80 62.80 o 10 13 0 1139.98 1111.40 113.58 o 11 13 0 126.33 264.52 84.29 o -5 14 0 0.29 54.69 65.44 o -4 14 0 612.36 814.50 152.63 o -3 14 0 428.89 453.36 67.85 o -2 14 0 513.95 587.76 80.72 o -1 14 0 1205.32 1398.81 82.17 o 0 14 0 3007.94 4151.77 156.88 o 1 14 0 2124.73 2243.08 89.37 o 2 14 0 337.21 414.16 68.88 o 3 14 0 1139.46 1250.53 100.94 o 4 14 0 1658.94 1977.88 89.01 o 5 14 0 12.16 32.09 37.27 o 6 14 0 1162.08 1242.68 109.24 o 7 14 0 363.77 335.67 45.23 o 8 14 0 677.91 506.35 122.47 o 9 14 0 460.49 459.08 75.32 o 10 14 0 612.16 561.38 78.48 o -4 15 0 518.17 679.29 106.16 o -3 15 0 175.67 143.63 74.01 o -2 15 0 172.70 123.03 72.33 o -1 15 0 1011.57 1263.61 142.89 o 0 15 0 3218.05 5073.83 278.28 o 1 15 0 1528.36 1807.16 83.94 o 2 15 0 92.73 89.30 44.22 o 3 15 0 524.81 611.70 95.44 o 4 15 0 1148.20 1463.29 79.34 o 5 15 0 7.86 1.55 42.37 o 6 15 0 1033.52 1202.89 72.69 o 7 15 0 718.40 1002.55 98.93 o 8 15 0 211.45 294.89 85.52 o 9 15 0 428.75 485.87 88.46 o -2 16 0 10.57 5.78 90.04 o -1 16 0 270.15 325.85 91.25 o 0 16 0 1944.65 2831.81 248.40 o 1 16 0 888.56 1079.96 96.56 o 2 16 0 83.51 124.79 74.43 o 3 16 0 205.82 308.66 55.53 o 4 16 0 615.07 902.58 74.88 o 5 16 0 55.16 79.52 49.86 o 6 16 0 596.21 795.76 71.54 o 7 16 0 222.01 280.23 72.37 o 8 16 0 53.78 -53.41 112.31 o 1 17 0 138.47 163.11 88.08 o 2 17 0 0.25 97.77 90.60 o 3 17 0 78.50 138.60 69.33 o 4 17 0 969.12 1371.78 109.68 o 5 17 0 2.46 76.56 75.95 o -4 -17 1 99.85 -41.38 89.94 o -3 -17 1 3.39 71.27 61.34 o -7 -16 1 206.16 300.49 84.46 o -6 -16 1 480.92 546.48 64.45 o -5 -16 1 59.00 50.05 52.10 o -4 -16 1 21.82 10.94 62.24 o -3 -16 1 9.10 14.68 63.62 o -2 -16 1 416.90 523.26 83.09 o -1 -16 1 48.17 90.79 63.23 o 0 -16 1 2.89 3.67 58.74 o 1 -16 1 5.03 100.48 88.83 o -9 -15 1 22.38 24.90 80.63 o -8 -15 1 467.05 538.79 81.34 o -7 -15 1 380.39 335.06 51.99 o -6 -15 1 340.10 351.80 54.54 o -5 -15 1 22.86 -58.68 58.68 o -4 -15 1 2.03 64.83 42.10 o -3 -15 1 108.90 99.02 52.30 o -2 -15 1 851.45 1043.26 61.68 o -1 -15 1 3.90 -28.57 51.77 o 0 -15 1 66.20 47.17 54.73 o 1 -15 1 6.11 86.18 58.58 o 2 -15 1 440.51 546.75 91.90 o 3 -15 1 25.97 61.42 68.79 o -10 -14 1 0.44 5.57 68.83 o -9 -14 1 90.76 -15.17 210.32 o -8 -14 1 1070.08 1018.28 97.23 o -7 -14 1 86.85 88.16 41.19 o -6 -14 1 236.29 215.50 42.87 o -5 -14 1 232.50 189.19 41.68 o -4 -14 1 24.55 87.65 40.04 o -3 -14 1 56.09 96.94 36.68 o -2 -14 1 2460.21 3147.79 180.41 o -1 -14 1 46.68 92.25 38.28 o 0 -14 1 2.27 58.45 60.54 o 1 -14 1 41.80 68.99 65.11 o 2 -14 1 1426.49 1737.47 99.75 o 3 -14 1 222.26 319.33 65.62 o 4 -14 1 33.68 152.21 70.18 o 5 -14 1 135.57 140.80 54.94 o -11 -13 1 1.91 -3.89 75.75 o -10 -13 1 6.82 30.13 68.66 o -9 -13 1 117.28 111.47 64.10 o -8 -13 1 2157.33 2294.56 91.02 o -7 -13 1 53.17 67.98 38.83 o -6 -13 1 559.49 612.60 47.02 o -5 -13 1 159.91 158.14 26.49 o -4 -13 1 556.86 511.36 40.21 o -3 -13 1 142.65 185.23 41.59 o -2 -13 1 4444.90 4945.91 192.88 o -1 -13 1 67.98 95.01 47.53 o 0 -13 1 98.75 136.42 32.14 o 1 -13 1 218.60 260.72 37.21 o 2 -13 1 2313.19 2985.13 131.28 o 3 -13 1 188.97 71.12 63.85 o 4 -13 1 29.77 127.00 79.37 o 5 -13 1 59.65 3.00 111.43 o 6 -13 1 439.20 317.44 60.90 o -12 -12 1 2020.64 1634.26 134.78 o -11 -12 1 9.00 -8.24 62.22 o -10 -12 1 104.26 6.05 56.08 o -9 -12 1 822.05 774.85 70.44 o -8 -12 1 3665.77 3527.96 120.24 o -7 -12 1 15.36 5.60 27.98 o -6 -12 1 564.29 537.09 32.87 o -5 -12 1 309.28 327.20 29.34 o -4 -12 1 1112.37 1204.95 49.37 o -3 -12 1 0.02 27.79 22.18 o -2 -12 1 6783.38 7733.58 201.00 o -1 -12 1 119.24 137.99 23.64 o 0 -12 1 40.58 62.04 24.86 o 1 -12 1 56.44 36.59 30.40 o 2 -12 1 4645.44 5461.19 169.91 o 3 -12 1 195.77 252.08 54.49 o 4 -12 1 25.20 184.64 85.70 o 5 -12 1 49.69 -11.00 75.31 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