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[Contents scheme]

Acta Cryst. (2012). E68, m1377-m1378
[ doi:10.1107/S1600536812042699 ]

Bis(acetato-[kappa]2O,O')(4,4'-dimethyl-2,2'-bipyridine-[kappa]2N,N')zinc

M. A. Harvey, S. A. Suarez, A. Ibañez, F. Doctorovich and R. Baggio


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT241_ALERT_2_B Check High Ueq as Compared to Neighbors for O2 PLAT915_ALERT_3_B Low Friedel Pair Coverage ...................... 47 Perc.
Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Zn1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C7 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G REFLT03_ALERT_4_G WARNING: Large fraction of Friedel related reflns may be needed to determine absolute structure From the CIF: _diffrn_reflns_theta_max 28.99 From the CIF: _reflns_number_total 1563 Count of symmetry unique reflns 1189 Completeness (_total/calc) 131.46% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 374 Fraction of Friedel pairs measured 0.315 Are heavy atom types Z>Si present yes PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Zn1 -- O1 .. 21.9 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Zn1 -- O2 .. 25.6 su PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.12 Ratio PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 106
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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