[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, o3079-o3080
[ doi:10.1107/S1600536812041396 ]

2-Cyano-5-({4-[N-methyl-N-(2-hydroxyethyl)amino] phenyl}diazenyl)pyridine

R. Centore and V. Piccialli


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT230_ALERT_2_B Hirshfeld Test Diff for N2 -- C7 .. 7.5 su
Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.974 PLAT230_ALERT_2_C Hirshfeld Test Diff for N3 -- C10 .. 6.5 su PLAT230_ALERT_2_C Hirshfeld Test Diff for C6 -- C7 .. 5.5 su PLAT355_ALERT_3_C Long O-H Bond (0.82A) O1 - H1O ... 1.03 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H6 .. N4 .. 2.74 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H2B .. O1 .. 2.68 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 9.809 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 62
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 1 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C13 - C15 ... 1.45 Ang.
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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