[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1361-m1362
[ doi:10.1107/S160053681204247X ]

(Ammine)(carbonyl)[hydridotris(pyrazol-1-yl-[kappa]N2)borato](triphenylphosphine-[kappa]P)ruthenium(II) chloride dichloromethane disolvate

T.-C. Hu, J.-X. Ye, S.-T. He, G.-R. Chiang and Y.-H. Lo


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.970 PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ru1 -- C1 .. 7.0 su PLAT420_ALERT_2_C D-H Without Acceptor N7 - H7B ... ? PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 192 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 5
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 3 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00100 Deg. PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 77 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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