[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1341
[ doi:10.1107/S1600536812040287 ]

Bis[4,4,5,5-tetramethyl-2-(pyridin-2-yl-[kappa]2N)imidazoline-1-oxyl 3-oxide-[kappa]O]tris(nitrato-[kappa]2O,O')terbium(III)

D. Li


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT213_ALERT_2_C Atom O6 has ADP max/min Ratio ..... 3.1 prola PLAT220_ALERT_2_C Large Non-Solvent O Ueq(max)/Ueq(min) ... 3.8 Ratio PLAT230_ALERT_2_C Hirshfeld Test Diff for O7 -- N8 .. 6.3 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Tb1 -- O4 .. 5.2 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Tb1 -- O10 .. 5.8 su PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.070 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c ....... P21/n PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 75 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 8 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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