[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, o3133-o3134
[ doi:10.1107/S1600536812042328 ]

Dibenzo[b,f][1,4]thiazepin-11-yl-diethyl-amine

M. Altamura, A. Guidi, L. Jierry, P. Paoli and P. Rossi


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C THETM01_ALERT_3_C The value of sine(theta_max)/wavelength is less than 0.590 Calculated sin(theta_max)/wavelength = 0.5864 PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.969 PLAT480_ALERT_4_C Long H...A H-Bond Reported H5 .. N1 .. 2.70 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.586 73
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 64 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 2 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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