[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1337
[ doi:10.1107/S1600536812040706 ]

[mu]2-Oxalato-bis[triphenyl(thiourea-[kappa]S)tin(IV)]

Y. Sow, L. Diop, K. C. Molloy and G. Kociok-Kohn


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 12
Alert level C PLAT213_ALERT_2_C Atom C10 has ADP max/min Ratio ..... 3.3 prola PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.7 Ratio PLAT230_ALERT_2_C Hirshfeld Test Diff for C9 -- C10 .. 6.8 su PLAT420_ALERT_2_C D-H Without Acceptor N1 - H1B ... ? PLAT420_ALERT_2_C D-H Without Acceptor N2 - H2B ... ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 7.48 PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Sn -- S .. 5.3 su PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 3
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 7 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster