[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1398-m1399
[ doi:10.1107/S160053681204336X ]

trans-Bis[4-amino-N-(pyrimidin-2-yl-[kappa]N)benzenesulfonamidato-[kappa]N]bis(N,N-dimethylformamide-[kappa]O)cobalt(II)

J. J. Guo, W. Wang, Y. D. Zhang, L. Yang and S. H. Zhang


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.4 Ratio PLAT230_ALERT_2_C Hirshfeld Test Diff for N5 -- C12 .. 6.0 su PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.396 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Co1 -- N1 .. 6.1 su PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for N5 PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for N5' PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 22 Perc. PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C13 PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 36 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 22
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 11 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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