[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1367
[ doi:10.1107/S1600536812041931 ]

[Bis[[mu]-bis(diphenylphosphino)methane-1:2[kappa]2P:P']-bis(nitrito-[kappa]2O,O')]disilver(I) acetonitrile disolvate

X. Yang, X. Huang, Q.-M. Qiu, Q.-H. Jin and C.-L. Zhang


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.20 PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ag1 -- P1 .. 6.0 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ag1 -- O1 .. 7.3 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ag1 -- O2 .. 8.4 su PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O1 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C12 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C22 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C26 PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -1.414 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 8 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 2
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 3 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c ....... P21/n PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 3 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 61 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 12 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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