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Acta Cryst. (2012). E68, m1572-m1573
[ doi:10.1107/S1600536812048210 ]

Bis([mu]-4,6-dimethylpyrimidine-2-thiolato)-[kappa]3N,S:S;[kappa]3S:N,S-bis[(triphenylphosphane-[kappa]P)silver(I)]

Y. Wattanakanjana, C. Pakawatchai, S. Kowittheeraphong and R. Nimthong


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT480_ALERT_4_C Long H...A H-Bond Reported H14 .. S1 .. 2.94 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H14 .. N2 .. 2.69 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H35 .. N2 .. 2.93 Ang. PLAT481_ALERT_4_C Long D...A H-Bond Reported C35 .. N2 .. 3.76 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.106
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c ....... P21/n PLAT164_ALERT_4_G Nr. of Refined C-H H-Atoms in Heavy-Atom Struct. 1 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- S1 .. 29.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- P1 .. 13.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- N1 .. 5.1 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- S1_a .. 11.0 su PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C5 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C6 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 4
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 9 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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