# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' iso-20Ph in Pn' _shelx_refln_list_code 4 _shelx_F_calc_maximum 76.03 _exptl_crystal_F_000 308.00 _reflns_d_resolution_high 0.8410 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y, z+1/2' _cell_length_a 8.4432 _cell_length_b 5.3030 _cell_length_c 16.3443 _cell_angle_alpha 90.000 _cell_angle_beta 90.453 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 -1 -19 14.42 9.75 2.66 o 0 -1 -19 67.42 83.63 3.09 o 1 -1 -19 7.45 7.50 1.95 o 1 0 -19 21.43 20.82 2.04 o -1 -2 -18 66.59 63.11 3.51 o 0 -2 -18 61.31 72.69 3.41 o 1 -2 -18 53.92 53.15 2.72 o 2 -2 -18 10.76 11.78 2.04 o -3 -1 -18 28.50 28.43 2.28 o -2 -1 -18 26.39 32.63 2.55 o -1 -1 -18 72.88 66.12 2.83 o 0 -1 -18 8.13 7.59 2.34 o 1 -1 -18 58.69 61.44 2.63 o 2 -1 -18 7.57 9.49 1.86 o 3 -1 -18 87.57 94.62 3.14 o -2 0 -18 73.06 83.88 3.08 o 0 0 -18 60.37 54.92 2.89 o 2 0 -18 25.88 25.82 2.03 o 1 1 -18 58.69 58.28 2.34 o 2 1 -18 7.57 8.99 1.71 o 3 1 -18 87.57 92.16 2.95 o 0 -3 -17 49.64 60.95 3.27 o 1 -3 -17 21.08 34.20 3.01 o -3 -2 -17 31.99 29.32 2.27 o -2 -2 -17 15.49 13.66 1.96 o -1 -2 -17 101.07 121.95 3.50 o 0 -2 -17 71.73 72.69 3.13 o 1 -2 -17 21.73 22.18 2.12 o 2 -2 -17 27.50 26.38 2.12 o 3 -2 -17 32.63 29.46 2.25 o -4 -1 -17 69.78 65.75 2.74 o -3 -1 -17 14.46 10.78 1.87 o -2 -1 -17 157.56 155.87 3.63 o -1 -1 -17 15.57 16.50 2.21 o 0 -1 -17 12.62 6.99 2.12 o 1 -1 -17 8.35 7.53 2.21 o 2 -1 -17 67.96 68.16 2.66 o 3 -1 -17 5.56 8.17 1.77 o 4 -1 -17 34.12 32.57 2.33 o -3 0 -17 54.30 46.83 2.34 o -1 0 -17 23.22 19.96 1.87 o 1 0 -17 62.64 57.61 2.70 o 3 0 -17 25.12 30.23 2.08 o 0 1 -17 12.62 11.89 1.94 o 1 1 -17 7.34 8.59 1.49 o 2 1 -17 67.96 68.33 2.42 o 3 1 -17 5.56 8.76 1.66 o 4 1 -17 34.12 31.57 2.17 o -3 -3 -16 36.97 38.47 2.51 o -2 -3 -16 16.97 19.05 2.16 o -1 -3 -16 18.17 17.38 2.07 o 0 -3 -16 27.02 32.42 2.60 o 1 -3 -16 77.39 79.29 3.29 o 2 -3 -16 20.30 19.59 2.06 o 3 -3 -16 6.64 6.91 1.85 o -4 -2 -16 40.41 42.29 2.52 o -3 -2 -16 51.39 44.50 2.38 o -2 -2 -16 82.00 90.33 2.96 o -1 -2 -16 1.30 0.00 1.56 o 0 -2 -16 24.07 22.38 2.13 o 1 -2 -16 49.18 47.97 2.78 o 2 -2 -16 30.10 30.98 2.53 o 3 -2 -16 29.77 23.52 2.05 o 4 -2 -16 28.49 25.16 2.22 o -5 -1 -16 15.08 13.31 1.94 o -4 -1 -16 43.82 40.75 2.33 o -3 -1 -16 96.90 95.08 2.96 o -2 -1 -16 51.33 49.45 2.33 o -1 -1 -16 7.96 7.48 1.56 o 0 -1 -16 39.49 37.95 2.24 o 1 -1 -16 55.99 51.30 2.62 o 2 -1 -16 24.81 23.08 1.89 o 3 -1 -16 101.36 95.65 2.91 o 4 -1 -16 5.86 8.06 1.76 o 5 -1 -16 40.32 39.22 2.30 o 10 0 0 37.24 69.00 3.39 o -4 0 -16 320.08 303.51 4.67 o -2 0 -16 60.91 67.06 2.39 o 0 0 -16 28.40 30.92 2.10 o 2 0 -16 132.08 119.83 2.96 o 4 0 -16 2.66 1.60 1.49 o -2 1 -16 51.33 51.29 2.10 o -1 1 -16 7.96 7.77 1.43 o 0 1 -16 39.49 38.86 2.13 o 1 1 -16 55.99 55.48 2.37 o 2 1 -16 24.81 21.99 1.72 o 3 1 -16 101.36 100.20 2.82 o 4 1 -16 5.86 8.89 1.65 o 5 1 -16 40.32 38.83 2.27 o 0 -4 -15 45.31 47.90 2.52 o -4 -3 -15 0.05 0.00 1.79 o -3 -3 -15 28.64 29.00 2.35 o -2 -3 -15 59.12 54.86 2.54 o -1 -3 -15 61.54 60.19 2.57 o 0 -3 -15 6.66 4.03 1.63 o 1 -3 -15 26.37 33.69 2.47 o 2 -3 -15 10.42 7.50 2.21 o 3 -3 -15 27.17 24.85 2.09 o 4 -3 -15 28.08 24.81 2.17 o -5 -2 -15 40.25 32.73 2.83 o -4 -2 -15 41.93 35.55 2.26 o -3 -2 -15 70.79 69.51 2.67 o -2 -2 -15 24.60 19.11 1.88 o -1 -2 -15 28.93 25.57 1.93 o 0 -2 -15 175.35 180.31 3.63 o 1 -2 -15 123.08 142.72 3.49 o 2 -2 -15 26.85 20.94 2.24 o 3 -2 -15 29.38 33.54 2.12 o 4 -2 -15 40.09 40.51 2.35 o 5 -2 -15 35.40 33.79 2.34 o -6 -1 -15 28.37 39.72 2.90 o -5 -1 -15 5.65 0.00 2.22 o -4 -1 -15 122.47 115.03 3.16 o -3 -1 -15 53.27 48.18 3.07 o -2 -1 -15 40.83 42.00 2.06 o -1 -1 -15 91.40 90.32 2.61 o 0 -1 -15 63.99 61.94 2.27 o 1 -1 -15 33.47 27.87 2.44 o 2 -1 -15 97.41 92.18 2.91 o 3 -1 -15 32.70 30.33 1.94 o 4 -1 -15 53.56 51.76 2.39 o 5 -1 -15 0.91 0.99 1.66 o 6 -1 -15 90.02 92.01 3.12 o -5 0 -15 12.32 11.83 2.23 o -3 0 -15 127.95 134.19 3.07 o -1 0 -15 185.62 183.53 3.32 o 1 0 -15 91.35 75.15 2.79 o 3 0 -15 92.34 85.06 2.61 o 5 0 -15 36.37 36.84 2.17 o -3 1 -15 53.27 47.88 2.88 o -2 1 -15 40.83 41.49 1.89 o -1 1 -15 91.40 88.30 2.40 o 0 1 -15 63.99 62.74 2.15 o 1 1 -15 33.47 36.50 1.95 o 2 1 -15 82.58 77.89 2.38 o 3 1 -15 32.70 30.46 1.89 o 4 1 -15 53.57 53.87 2.29 o 5 1 -15 0.91 0.45 1.60 o 6 1 -15 90.02 90.08 3.09 o -2 -4 -14 12.36 8.55 2.51 o -1 -4 -14 32.85 29.52 2.18 o 0 -4 -14 22.94 23.21 2.05 o 1 -4 -14 49.62 53.33 2.47 o 2 -4 -14 6.79 3.76 2.04 o -5 -3 -14 0.26 0.00 2.66 o -4 -3 -14 46.81 42.23 2.88 o -3 -3 -14 0.99 0.00 1.63 o -2 -3 -14 29.59 26.38 1.96 o -1 -3 -14 47.24 49.33 2.32 o 0 -3 -14 261.73 260.08 4.29 o 1 -3 -14 16.67 13.80 1.79 o 2 -3 -14 26.72 27.30 2.32 o 3 -3 -14 49.81 47.03 2.63 o 4 -3 -14 32.50 30.08 2.15 o 5 -3 -14 21.03 26.30 2.29 o -6 -2 -14 5.09 2.99 1.75 o -5 -2 -14 21.08 19.26 2.40 o -4 -2 -14 49.13 44.76 2.67 o -3 -2 -14 18.84 18.90 1.82 o -2 -2 -14 130.74 125.67 4.05 o -1 -2 -14 198.84 191.30 3.59 o 0 -2 -14 70.87 74.80 2.45 o 1 -2 -14 5.52 4.98 1.50 o 2 -2 -14 124.80 115.09 3.08 o 3 -2 -14 40.42 41.49 2.45 o 4 -2 -14 71.23 75.96 2.74 o 5 -2 -14 72.44 74.10 2.84 o 6 -2 -14 57.47 60.57 2.72 o -6 -1 -14 17.90 17.64 1.90 o -5 -1 -14 51.19 48.74 2.75 o -4 -1 -14 16.24 9.59 2.06 o -3 -1 -14 26.96 26.47 1.81 o -2 -1 -14 8.37 8.02 1.53 o -1 -1 -14 73.78 72.73 2.33 o 0 -1 -14 113.04 108.89 2.68 o 1 -1 -14 108.80 103.80 2.67 o 2 -1 -14 71.17 69.34 2.48 o 3 -1 -14 203.95 186.65 3.71 o 4 -1 -14 17.28 14.42 1.73 o 5 -1 -14 98.25 101.57 3.03 o 6 -1 -14 53.44 52.93 2.53 o -6 0 -14 57.60 61.92 2.52 o -4 0 -14 161.13 135.42 3.23 o -2 0 -14 387.89 384.26 4.55 o 0 0 -14 127.17 116.98 2.61 o 2 0 -14 127.41 108.01 2.72 o 4 0 -14 145.03 136.89 3.15 o 6 0 -14 26.20 34.02 2.26 o -4 1 -14 16.24 11.85 1.93 o -3 1 -14 26.96 24.23 1.65 o -2 1 -14 8.37 9.59 1.43 o -1 1 -14 73.78 73.41 2.11 o 0 1 -14 113.04 110.60 2.44 o 1 1 -14 108.80 106.39 2.41 o 2 1 -14 71.17 63.72 2.26 o 3 1 -14 94.92 90.13 2.49 o 4 1 -14 17.28 15.90 1.66 o 5 1 -14 98.25 93.49 2.77 o 6 1 -14 53.44 51.21 2.48 o -3 -4 -13 26.40 23.08 2.55 o -2 -4 -13 3.38 1.29 1.57 o -1 -4 -13 64.24 71.13 2.60 o 0 -4 -13 41.72 39.90 2.16 o 1 -4 -13 9.42 9.63 1.68 o 2 -4 -13 85.63 86.93 2.77 o 3 -4 -13 33.61 34.76 2.87 o -5 -3 -13 86.79 79.82 2.95 o -4 -3 -13 29.32 25.54 2.44 o -3 -3 -13 50.20 46.19 2.66 o -2 -3 -13 23.40 19.50 2.31 o -1 -3 -13 38.79 32.74 2.78 o 0 -3 -13 45.40 49.95 2.18 o 1 -3 -13 167.43 173.36 3.46 o 2 -3 -13 13.78 8.48 1.56 o 3 -3 -13 95.18 80.34 2.72 o 4 -3 -13 40.84 41.78 2.70 o 5 -3 -13 31.02 35.26 2.27 o -6 -2 -13 49.12 45.84 2.48 o -5 -2 -13 22.19 22.83 1.99 o -4 -2 -13 118.74 115.55 3.30 o -3 -2 -13 182.63 171.62 3.70 o -2 -2 -13 27.85 23.23 1.79 o -1 -2 -13 137.51 110.47 4.06 o 0 -2 -13 388.11 378.42 4.62 o 1 -2 -13 151.45 142.80 3.02 o 2 -2 -13 59.52 57.06 2.17 o 3 -2 -13 290.15 366.34 4.85 o 4 -2 -13 119.90 106.61 2.97 o 5 -2 -13 24.20 26.92 2.05 o 6 -2 -13 79.06 85.02 2.94 o -7 -1 -13 1.71 0.97 1.66 o -6 -1 -13 46.20 43.81 2.27 o -5 -1 -13 10.51 11.29 1.60 o -4 -1 -13 85.24 73.08 2.68 o -3 -1 -13 103.22 90.37 2.77 o -2 -1 -13 544.42 511.27 5.21 o -1 -1 -13 49.89 47.82 2.00 o 0 -1 -13 22.53 20.28 1.50 o 1 -1 -13 10.97 9.84 1.32 o 2 -1 -13 126.19 122.11 2.75 o 3 -1 -13 37.08 34.69 2.06 o 4 -1 -13 407.00 414.49 5.23 o 5 -1 -13 8.22 7.68 1.59 o 6 -1 -13 38.33 39.99 2.28 o 7 -1 -13 33.65 38.43 2.47 o -7 0 -13 35.61 32.94 2.17 o -5 0 -13 59.37 58.42 2.23 o -3 0 -13 459.16 425.89 4.79 o -1 0 -13 104.17 91.39 3.13 o 1 0 -13 226.18 211.42 3.24 o 3 0 -13 274.73 227.84 3.64 o 5 0 -13 114.20 120.27 2.96 o 7 0 -13 59.86 61.85 2.70 o -6 1 -13 46.20 43.45 2.16 o -5 1 -13 10.51 10.71 1.53 o -4 1 -13 85.24 74.23 2.50 o -3 1 -13 103.22 93.58 2.57 o -2 1 -13 544.43 518.22 4.75 o -1 1 -13 49.89 40.09 2.35 o 0 1 -13 22.53 21.45 1.34 o 1 1 -13 10.97 10.43 1.18 o 2 1 -13 126.19 117.50 2.55 o 3 1 -13 37.08 41.95 2.05 o 4 1 -13 379.75 384.97 4.62 o 5 1 -13 8.22 6.05 1.48 o 6 1 -13 38.33 49.49 2.47 o 7 1 -13 33.65 35.25 2.31 o -4 -4 -12 35.98 32.82 2.21 o -3 -4 -12 46.92 56.78 2.76 o -2 -4 -12 5.87 4.88 2.06 o -1 -4 -12 18.95 17.16 1.78 o 0 -4 -12 76.25 71.70 3.48 o 1 -4 -12 136.75 141.89 3.22 o 2 -4 -12 20.22 20.89 1.77 o 3 -4 -12 54.19 57.29 2.35 o 4 -4 -12 10.08 4.53 2.25 o -6 -3 -12 20.39 23.61 2.24 o -5 -3 -12 8.26 7.73 1.77 o -4 -3 -12 134.78 126.65 3.21 o -3 -3 -12 36.03 34.14 2.35 o -2 -3 -12 24.55 24.76 2.20 o -1 -3 -12 32.76 29.98 1.81 o 0 -3 -12 306.14 254.70 5.53 o 1 -3 -12 120.23 115.49 2.83 o 2 -3 -12 240.74 236.51 3.81 o 3 -3 -12 42.75 38.86 2.02 o 4 -3 -12 79.76 90.98 2.93 o 5 -3 -12 26.63 27.14 2.04 o 6 -3 -12 121.10 130.92 3.46 o -7 -2 -12 28.16 32.25 2.50 o -6 -2 -12 48.06 48.68 2.44 o -5 -2 -12 47.68 45.25 2.27 o -4 -2 -12 47.08 44.61 2.20 o -3 -2 -12 80.26 75.32 2.64 o -2 -2 -12 448.62 430.77 4.83 o -1 -2 -12 23.22 20.92 1.63 o 0 -2 -12 41.36 29.50 2.69 o 1 -2 -12 200.80 191.51 3.28 o 2 -2 -12 301.08 282.94 3.95 o 3 -2 -12 27.76 26.47 1.74 o 4 -2 -12 295.90 427.89 5.23 o 5 -2 -12 17.80 19.19 1.83 o 6 -2 -12 42.05 45.82 2.32 o 7 -2 -12 88.26 103.45 3.33 o -7 -1 -12 96.86 104.90 3.24 o -6 -1 -12 25.14 25.26 1.91 o -5 -1 -12 54.70 49.36 2.17 o -4 -1 -12 11.57 10.03 1.50 o -3 -1 -12 348.33 328.30 4.34 o -2 -1 -12 51.56 50.25 2.17 o -1 -1 -12 292.14 282.96 3.71 o 0 -1 -12 27.92 25.73 1.54 o 1 -1 -12 134.44 122.98 2.57 o 2 -1 -12 24.93 26.78 1.58 o 3 -1 -12 458.03 437.31 4.78 o 4 -1 -12 63.58 54.86 2.32 o 5 -1 -12 75.38 76.75 2.85 o 6 -1 -12 23.02 23.18 1.87 o 7 -1 -12 68.24 72.32 2.80 o -6 0 -12 118.92 110.94 2.89 o -4 0 -12 371.09 343.92 4.28 o -2 0 -12 153.02 135.66 2.73 o 0 0 -12 117.40 110.84 2.37 o 2 0 -12 455.87 450.89 4.49 o 4 0 -12 393.36 526.92 5.41 o 6 0 -12 113.68 110.94 3.03 o -7 1 -12 96.86 99.84 2.91 o -6 1 -12 25.14 24.42 1.78 o -5 1 -12 54.70 48.36 1.95 o -4 1 -12 11.57 10.54 1.33 o -3 1 -12 348.33 335.51 3.96 o -2 1 -12 36.99 38.00 1.60 o -1 1 -12 292.14 280.23 3.31 o 0 1 -12 27.92 25.23 1.40 o 1 1 -12 134.44 122.34 2.29 o 2 1 -12 24.93 24.39 1.41 o 3 1 -12 458.03 457.96 4.62 o 4 1 -12 63.58 57.40 2.21 o 5 1 -12 51.68 54.15 2.18 o 6 1 -12 23.02 23.96 1.86 o 7 1 -12 68.24 80.11 2.90 o 5 2 -12 24.04 23.86 2.08 o 6 2 -12 42.05 42.53 2.18 o 7 2 -12 88.26 102.88 3.14 o -5 -4 -11 8.28 7.49 1.78 o -4 -4 -11 111.85 109.01 3.09 o -3 -4 -11 9.52 8.34 1.58 o -2 -4 -11 38.23 35.11 1.94 o -1 -4 -11 20.57 19.85 2.16 o 0 -4 -11 79.20 79.61 2.46 o 1 -4 -11 28.28 30.03 1.88 o 2 -4 -11 192.09 197.37 3.53 o 3 -4 -11 83.95 82.81 2.53 o 4 -4 -11 43.20 45.80 2.24 o -6 -3 -11 26.87 28.93 2.36 o -5 -3 -11 73.66 66.13 2.58 o -4 -3 -11 46.71 47.78 2.19 o -3 -3 -11 184.50 164.07 3.27 o -2 -3 -11 125.51 112.01 2.88 o -1 -3 -11 52.14 52.27 2.02 o 0 -3 -11 109.13 108.25 2.64 o 1 -3 -11 461.40 435.24 5.79 o 2 -3 -11 108.26 111.32 2.68 o 3 -3 -11 111.17 115.22 2.75 o 4 -3 -11 56.04 58.15 2.29 o 5 -3 -11 73.33 62.35 3.00 o 6 -3 -11 178.43 185.99 3.87 o -7 -2 -11 84.32 82.28 2.99 o -6 -2 -11 20.83 15.28 2.01 o -5 -2 -11 61.32 54.75 2.29 o -4 -2 -11 269.34 256.09 3.97 o -3 -2 -11 97.83 90.87 2.47 o -2 -2 -11 36.81 30.79 1.81 o -1 -2 -11 664.88 658.18 5.64 o 0 -2 -11 97.91 92.68 2.28 o 1 -2 -11 179.94 117.92 3.73 o 2 -2 -11 430.01 433.12 4.59 o 3 -2 -11 83.74 84.21 2.32 o 4 -2 -11 10.21 12.30 1.53 o 5 -2 -11 192.21 168.47 4.02 o 6 -2 -11 29.23 30.32 2.02 o 7 -2 -11 43.05 46.88 2.47 o -8 -1 -11 52.65 51.52 2.60 o -7 -1 -11 12.79 11.53 1.77 o -6 -1 -11 103.80 104.51 2.93 o -5 -1 -11 28.10 24.57 1.74 o -4 -1 -11 230.09 219.77 3.54 o -3 -1 -11 85.37 77.93 2.20 o -2 -1 -11 465.53 431.11 4.41 o -1 -1 -11 51.50 54.22 1.77 o 0 -1 -11 212.23 201.93 2.99 o 1 -1 -11 122.04 87.61 2.76 o 2 -1 -11 318.46 308.72 3.72 o 3 -1 -11 72.36 67.80 2.06 o 4 -1 -11 406.49 403.61 4.69 o 5 -1 -11 165.59 202.23 3.73 o 6 -1 -11 35.80 38.90 2.11 o 7 -1 -11 3.52 4.28 1.65 o 8 -1 -11 53.98 54.74 2.69 o -7 0 -11 19.74 19.24 1.82 o -5 0 -11 155.57 151.60 3.01 o -3 0 -11 169.03 165.21 2.79 o -1 0 -11 234.25 234.90 3.04 o 1 0 -11 611.94 594.56 4.75 o 3 0 -11 179.23 163.99 2.81 o 5 0 -11 181.85 173.11 3.32 o 7 0 -11 105.54 106.86 3.09 o -8 1 -11 52.65 54.06 2.52 o -7 1 -11 12.79 13.01 1.70 o -6 1 -11 103.80 108.46 2.78 o -5 1 -11 28.10 23.26 1.53 o -4 1 -11 230.09 222.49 3.24 o -3 1 -11 85.37 76.86 2.01 o -2 1 -11 465.53 439.45 4.02 o -1 1 -11 51.49 55.17 1.61 o 0 1 -11 212.23 205.32 2.68 o 1 1 -11 122.04 106.08 2.05 o 2 1 -11 318.46 302.95 3.40 o 3 1 -11 72.36 69.49 1.97 o 4 1 -11 406.49 407.19 4.39 o 5 1 -11 165.59 172.21 3.29 o 6 1 -11 35.80 40.21 2.05 o 7 1 -11 3.52 3.58 1.59 o 8 1 -11 53.98 64.66 2.82 o 4 2 -11 10.21 10.60 1.40 o 5 2 -11 192.21 227.27 3.72 o 6 2 -11 29.23 28.04 1.86 o 7 2 -11 43.05 45.46 2.30 o -5 -4 -10 60.54 68.03 2.72 o -4 -4 -10 17.96 17.66 1.76 o -3 -4 -10 84.17 79.54 2.52 o -2 -4 -10 13.46 14.43 1.51 o -1 -4 -10 43.14 52.60 2.33 o 0 -4 -10 14.80 14.89 1.57 o 1 -4 -10 181.55 186.53 3.29 o 2 -4 -10 45.83 54.51 2.16 o -7 -3 -10 18.55 17.00 2.61 o -6 -3 -10 18.65 15.10 1.85 o -5 -3 -10 12.99 12.79 1.84 o -4 -3 -10 302.70 291.75 4.27 o -3 -3 -10 92.95 91.14 2.49 o -2 -3 -10 27.94 26.14 1.59 o -1 -3 -10 212.16 230.01 3.58 o 0 -3 -10 139.16 128.82 2.69 o 1 -3 -10 148.80 147.53 2.82 o 2 -3 -10 504.73 355.35 6.45 o 3 -3 -10 88.96 89.05 2.41 o 4 -3 -10 77.43 76.78 2.41 o 5 -3 -10 58.47 58.15 2.26 o 6 -3 -10 38.42 56.09 2.66 o 7 -3 -10 34.51 41.34 2.37 o -7 -2 -10 79.63 84.71 3.34 o -6 -2 -10 78.30 71.64 2.56 o -5 -2 -10 50.53 49.09 2.22 o -4 -2 -10 231.78 217.16 3.57 o -3 -2 -10 310.78 291.81 3.87 o -2 -2 -10 253.03 238.75 3.38 o -1 -2 -10 211.35 204.43 3.15 o 0 -2 -10 352.85 354.64 3.90 o 1 -2 -10 247.87 237.49 3.25 o 2 -2 -10 43.02 45.51 1.85 o 3 -2 -10 379.95 365.42 4.19 o 4 -2 -10 348.03 346.17 4.35 o 5 -2 -10 13.22 12.99 1.52 o 6 -2 -10 133.63 173.38 3.76 o 7 -2 -10 73.89 77.35 2.80 o 8 -2 -10 0.60 0.00 1.76 o -8 -1 -10 6.17 5.36 2.27 o -7 -1 -10 45.02 41.96 2.23 o -6 -1 -10 51.10 49.28 2.19 o -5 -1 -10 377.47 392.86 4.69 o -4 -1 -10 125.74 114.39 2.54 o -3 -1 -10 212.16 204.49 3.10 o -2 -1 -10 24.42 23.09 1.35 o -1 -1 -10 641.75 684.58 5.13 o 0 -1 -10 60.76 64.93 1.79 o 1 -1 -10 348.23 317.17 3.50 o 2 -1 -10 307.52 300.96 3.56 o 3 -1 -10 43.10 41.32 1.67 o 4 -1 -10 15.22 15.84 1.43 o 5 -1 -10 316.78 310.75 4.18 o 6 -1 -10 110.93 109.84 3.18 o 7 -1 -10 25.54 25.72 2.38 o 8 -1 -10 28.16 27.04 2.17 o -8 0 -10 72.80 76.79 3.08 o -6 0 -10 91.84 87.28 2.49 o -4 0 -10 323.78 306.43 3.73 o -2 0 -10 149.88 145.85 2.38 o 0 0 -10 313.59 300.14 3.18 o 2 0 -10 483.70 485.74 4.26 o 4 0 -10 612.71 623.55 5.32 o 6 0 -10 294.53 361.45 4.78 o 8 0 -10 174.99 167.96 3.86 o -8 1 -10 6.17 6.44 2.14 o -7 1 -10 45.02 40.76 2.09 o -6 1 -10 51.10 47.96 1.97 o -5 1 -10 377.47 417.10 4.45 o -4 1 -10 125.74 117.18 2.33 o -3 1 -10 212.16 200.34 2.78 o -2 1 -10 24.42 25.13 1.18 o -1 1 -10 641.74 594.25 4.23 o 0 1 -10 60.76 65.34 1.55 o 1 1 -10 348.24 317.31 3.14 o 2 1 -10 307.52 259.10 3.63 o 3 1 -10 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2 46.24 44.74 0.91 o 3 -1 2 9.95 11.55 0.65 o 5 -1 2 63.65 65.42 1.59 o 6 -1 2 13.65 15.17 1.21 o 8 -1 2 0.80 0.00 1.12 o 6 0 2 47.62 44.66 1.62 o 8 0 2 27.45 29.88 1.76 o 1 1 2 664.41 659.58 2.68 o 3 1 2 9.95 10.18 0.78 o 5 1 2 63.65 62.11 1.70 o 6 1 2 13.65 13.94 1.29 o 8 1 2 0.80 0.00 1.30 o 1 2 2 43.82 45.75 0.89 o 3 2 2 46.24 44.90 1.29 o 5 2 2 24.28 25.97 1.39 o 6 2 2 17.41 16.87 1.45 o 8 2 2 24.43 24.04 1.90 o 1 3 2 27.71 29.14 0.82 o 3 3 2 130.64 131.61 2.12 o 5 3 2 15.18 14.54 1.34 o 6 3 2 3.33 2.31 1.23 o 8 3 2 27.15 29.36 2.08 o 6 4 2 4.41 4.25 1.34 o 2 -2 3 57.32 59.28 0.95 o 4 -2 3 245.90 256.13 2.41 o 2 -1 3 406.16 405.97 2.38 o 4 -1 3 64.35 67.81 1.42 o 6 -1 3 111.59 117.92 2.34 o 7 -1 3 9.52 11.33 1.31 o 9 -1 3 5.66 4.91 1.45 o 1 0 3 1039.56 1048.29 3.43 o 7 0 3 93.33 100.26 2.49 o 9 0 3 7.61 8.89 1.50 o 2 1 3 406.16 415.29 2.76 o 4 1 3 64.35 69.33 1.64 o 6 1 3 111.59 114.44 2.46 o 7 1 3 9.52 11.38 1.40 o 9 1 3 5.66 5.83 1.57 o 0 2 3 154.43 167.18 1.30 o 2 2 3 57.32 63.31 1.27 o 4 2 3 245.90 260.44 3.08 o 6 2 3 56.35 57.09 2.03 o 7 2 3 22.75 23.24 1.73 o 9 2 3 0.84 0.00 1.62 o 2 3 3 62.70 65.79 1.41 o 4 3 3 16.82 18.24 1.25 o 7 3 3 18.16 18.65 1.72 o 7 4 3 0.41 1.05 1.45 o 3 -2 4 1.99 2.11 0.57 o 3 -1 4 215.76 220.40 2.17 o 5 -1 4 12.84 12.96 1.01 o 7 -1 4 12.08 28.84 1.64 o 8 -1 4 0.36 2.20 1.27 o 8 0 4 5.97 6.58 1.42 o 1 1 4 120.78 115.31 1.43 o 3 1 4 215.76 225.35 2.45 o 5 1 4 12.84 12.70 1.10 o 7 1 4 12.08 25.84 1.68 o 8 1 4 0.36 1.81 1.39 o 0 2 4 16.10 16.42 0.60 o 1 2 4 60.49 64.87 1.12 o 3 2 4 1.99 1.95 0.75 o 5 2 4 92.40 96.35 2.24 o 8 2 4 23.58 26.28 2.00 o 1 3 4 20.88 22.15 0.84 o 3 3 4 9.35 10.33 0.96 o 5 3 4 50.46 49.88 1.91 o 8 3 4 27.79 26.93 2.16 o 5 4 4 39.36 39.84 1.80 o 4 -2 5 33.75 33.39 1.13 o 2 -1 5 30.09 28.48 0.88 o 4 -1 5 24.86 29.02 1.13 o 6 -1 5 80.53 87.02 2.16 o 8 -1 5 51.22 55.92 2.11 o 9 -1 5 1.14 0.00 1.35 o 9 0 5 19.45 19.62 1.78 o 1 1 5 131.92 141.89 1.69 o 2 1 5 30.09 29.50 1.00 o 4 1 5 24.86 28.96 1.23 o 6 1 5 80.53 80.39 2.22 o 8 1 5 51.22 54.98 2.28 o 9 1 5 1.14 0.58 1.57 o 1 2 5 52.14 50.44 1.10 o 2 2 5 36.70 36.77 1.10 o 4 2 5 33.75 34.43 1.41 o 6 2 5 62.60 67.63 2.20 o 9 2 5 11.16 11.97 2.03 o 1 3 5 23.60 26.21 0.94 o 2 3 5 6.73 6.57 0.84 o 4 3 5 79.81 85.41 2.10 o 6 3 5 1.02 0.00 1.23 o 6 4 5 4.55 5.26 1.38 o 3 -2 6 18.17 15.91 0.95 o 5 -2 6 43.75 44.47 1.49 o 3 -1 6 63.43 62.46 1.42 o 5 -1 6 14.19 14.64 1.12 o 7 -1 6 91.01 105.06 2.60 o 9 -1 6 23.88 26.79 1.94 o 2 0 6 79.70 73.98 1.43 o 1 1 6 89.91 90.97 1.47 o 2 1 6 14.62 15.13 0.85 o 3 1 6 63.43 61.65 1.47 o 5 1 6 14.19 14.52 1.24 o 7 1 6 91.01 100.26 2.71 o 9 1 6 23.88 25.93 2.09 o 0 2 6 44.52 47.73 1.06 o 2 2 6 8.71 8.38 0.76 o 3 2 6 18.17 16.49 1.05 o 5 2 6 43.75 45.20 1.77 o 7 2 6 2.45 5.19 1.47 o 2 3 6 4.26 3.61 0.84 o 3 3 6 13.39 13.84 1.18 o 5 3 6 23.74 24.25 1.59 o 7 3 6 5.41 4.53 1.54 o 5 4 6 16.14 17.62 1.55 o 7 4 6 0.20 0.00 1.58 o 3 -2 7 135.46 145.66 2.19 o 4 -2 7 93.63 85.77 1.87 o 3 -1 7 81.97 84.01 1.69 o 4 -1 7 30.08 29.18 1.27 o 6 -1 7 114.94 117.99 2.58 o 8 -1 7 48.14 53.95 2.25 o 3 0 7 25.65 28.40 1.13 o 3 1 7 81.97 88.47 1.81 o 4 1 7 30.08 30.72 1.34 o 6 1 7 114.94 115.56 2.68 o 8 1 7 48.14 53.26 2.38 o 1 2 7 7.53 6.56 0.76 o 3 2 7 135.46 138.36 2.29 o 4 2 7 93.63 87.54 2.06 o 6 2 7 12.66 13.34 1.44 o 8 2 7 6.99 7.03 1.71 o 1 3 7 45.81 45.20 1.26 o 3 3 7 12.78 15.56 1.25 o 4 3 7 45.21 46.84 1.80 o 6 3 7 2.66 4.55 1.45 o 8 3 7 2.89 3.75 1.80 o 6 4 7 7.02 8.35 1.51 o 4 -2 8 49.09 49.72 1.65 o 5 -2 8 16.24 17.25 1.30 o 4 -1 8 30.99 34.91 1.43 o 5 -1 8 11.47 12.92 1.17 o 7 -1 8 94.11 100.65 2.73 o 2 0 8 65.25 62.75 1.51 o 4 0 8 2.89 8.94 1.04 o 2 1 8 10.93 10.36 0.93 o 4 1 8 30.99 33.97 1.43 o 5 1 8 11.47 16.92 1.35 o 7 1 8 94.11 103.10 2.84 o 2 2 8 152.29 162.81 2.41 o 4 2 8 49.09 49.30 1.74 o 5 2 8 16.24 17.53 1.47 o 7 2 8 50.90 53.60 2.38 o 2 3 8 32.78 33.31 1.31 o 4 3 8 43.10 44.84 1.81 o 5 3 8 10.21 10.06 1.45 o 7 3 8 13.14 15.48 1.84 o 3 -2 9 52.45 52.74 1.65 o 5 -2 9 44.85 45.96 1.70 o 3 -1 9 10.69 13.23 1.08 o 5 -1 9 30.49 27.44 1.51 o 6 -1 9 105.63 105.36 2.57 o 8 -1 9 19.92 26.84 2.02 o 3 0 9 1.48 2.05 0.88 o 5 0 9 114.84 132.28 2.62 o 3 1 9 10.69 12.15 1.11 o 5 1 9 30.49 32.21 1.67 o 6 1 9 105.63 103.07 2.68 o 8 1 9 19.92 23.56 1.98 o 1 2 9 158.41 168.21 2.46 o 3 2 9 52.45 49.96 1.66 o 5 2 9 44.85 45.20 1.88 o 6 2 9 27.94 28.51 1.83 o 8 2 9 3.17 1.10 1.77 o 1 3 9 26.37 28.03 1.26 o 3 3 9 39.93 39.20 1.62 o 5 3 9 57.09 59.02 2.17 o 6 3 9 3.00 3.78 1.55 o 6 4 9 13.00 13.57 1.68 o 4 -2 10 66.70 65.69 1.99 o 4 -1 10 36.25 35.16 1.57 o 6 -1 10 14.57 14.13 1.45 o 7 -1 10 13.23 18.21 1.72 o 4 0 10 93.54 94.99 2.27 o 6 0 10 25.51 25.41 1.64 o 2 1 10 7.11 8.12 1.01 o 4 1 10 36.25 35.15 1.61 o 6 1 10 14.57 13.84 1.50 o 7 1 10 13.23 17.34 1.80 o 2 2 10 71.92 70.94 1.89 o 4 2 10 66.70 62.97 2.01 o 6 2 10 22.35 23.52 1.84 o 7 2 10 3.07 6.81 1.74 o 2 3 10 8.19 8.83 1.12 o 4 3 10 86.80 85.13 2.38 o 6 3 10 5.13 5.93 1.60 o 7 3 10 4.25 5.68 1.75 o 3 -2 11 27.68 27.21 1.48 o 5 -2 11 17.64 17.73 1.48 o 3 -1 11 24.84 24.51 1.47 o 5 -1 11 7.93 7.68 1.27 o 7 -1 11 3.60 3.42 1.52 o 8 -1 11 15.10 20.00 2.02 o 3 0 11 48.91 50.71 1.80 o 5 0 11 43.14 43.30 1.85 o 7 0 11 5.73 8.97 1.63 o 3 1 11 24.84 24.25 1.46 o 5 1 11 7.93 7.07 1.32 o 7 1 11 3.60 5.04 1.55 o 8 1 11 15.10 16.75 2.04 o 1 2 11 163.04 172.27 2.77 o 3 2 11 27.68 27.56 1.56 o 5 2 11 17.64 16.10 1.55 o 7 2 11 24.24 26.16 2.18 o 3 3 11 53.45 50.20 1.82 o 5 3 11 20.56 21.74 1.79 o 4 -2 12 13.20 14.13 1.45 o 6 -2 12 13.91 12.07 1.65 o 4 -1 12 3.21 3.85 1.26 o 6 -1 12 7.07 9.27 1.48 o 4 0 12 104.23 99.51 2.50 o 6 0 12 34.50 35.66 1.95 o 2 1 12 10.70 11.70 1.27 o 4 1 12 3.21 3.25 1.25 o 6 1 12 7.07 5.34 1.49 o 1 2 12 6.80 6.87 1.15 o 2 2 12 128.30 128.81 2.63 o 4 2 12 13.20 12.61 1.41 o 6 2 12 13.91 15.87 1.77 o 2 3 12 6.93 7.99 1.21 o 4 3 12 38.66 39.53 1.91 o 6 3 12 5.61 8.91 1.78 o 3 -2 13 37.51 35.15 1.77 o 5 -2 13 6.78 6.80 1.49 o 3 -1 13 26.47 27.58 1.63 o 5 -1 13 3.07 4.18 1.39 o 7 -1 13 0.48 1.27 1.46 o 3 0 13 99.51 104.24 2.60 o 5 0 13 17.32 16.45 1.55 o 7 0 13 10.39 14.02 1.84 o 2 1 13 155.61 159.04 3.04 o 3 1 13 26.47 27.97 1.67 o 5 1 13 3.07 2.23 1.36 o 7 1 13 0.48 1.03 1.51 o 2 2 13 7.77 7.36 1.29 o 3 2 13 37.51 39.33 1.90 o 5 2 13 6.78 6.59 1.53 o 2 3 13 0.94 1.07 1.15 o 3 3 13 13.70 12.57 1.40 o 5 3 13 25.19 25.07 2.00 o 3 -2 14 5.60 10.22 1.42 o 4 -2 14 8.64 8.30 1.54 o 6 -2 14 1.41 0.65 1.33 o 3 -1 14 7.40 14.85 1.46 o 4 -1 14 2.46 2.85 1.39 o 6 -1 14 5.02 3.62 1.60 o 4 0 14 19.63 18.04 1.61 o 6 0 14 16.93 18.24 1.83 o 3 1 14 7.40 8.82 1.45 o 4 1 14 2.46 4.55 1.45 o 6 1 14 5.02 3.44 1.58 o 1 2 14 56.65 57.36 2.04 o 3 2 14 5.60 7.60 1.47 o 4 2 14 8.64 8.68 1.56 o 6 2 14 1.41 2.11 1.58 o 3 3 14 0.28 0.00 1.27 o 4 3 14 12.55 11.24 1.60 o 4 -2 15 12.36 14.51 1.75 o 5 -2 15 7.86 7.87 1.71 o 4 -1 15 34.33 37.19 2.08 o 5 -1 15 0.60 0.00 1.50 o 5 0 15 0.90 1.08 1.45 o 2 1 15 12.39 15.34 1.60 o 4 1 15 34.33 36.16 2.10 o 5 1 15 0.60 1.49 1.48 o 2 2 15 6.89 4.95 1.41 o 4 2 15 12.36 11.90 1.67 o 5 2 15 7.86 7.22 1.73 o 2 3 15 16.90 18.50 1.68 o 4 3 15 0.02 0.17 1.41 o 3 -2 16 14.93 15.57 1.66 o 3 -1 16 28.33 30.26 1.97 o 5 -1 16 4.38 9.14 1.73 o 3 1 16 28.33 31.40 2.03 o 5 1 16 4.38 6.07 1.71 o 1 2 16 0.35 0.00 1.33 o 3 2 16 14.93 15.67 1.80 o 3 3 16 10.61 11.28 1.66 o 4 -1 17 19.82 23.56 2.05 o 2 1 17 45.66 53.16 2.39 o 4 1 17 19.82 23.15 2.06 o 2 2 17 4.52 4.18 1.52 o 3 -1 18 8.20 8.96 1.85 o 3 1 18 8.20 12.73 1.84 o 1 2 18 18.75 22.02 1.98 o 0 -1 -10 60.76 64.57 2.17 o 0 0 -10 313.59 315.72 5.09 o -1 -1 -9 106.19 112.10 2.29 o 0 -1 -9 776.99 803.53 6.40 o 1 0 -9 1735.64 1848.05 11.96 o -1 -1 -8 458.83 445.59 3.96 o -1 -1 -7 246.53 261.99 2.72 o 1 0 -7 2157.93 2285.88 11.81 o 1 1 -7 139.91 155.10 3.70 o 2 1 -7 66.62 65.76 2.69 o -1 -1 -6 305.17 282.06 2.41 o 2 1 -6 172.55 185.01 3.98 o 3 1 -6 657.61 732.58 8.28 o 1 0 -5 508.29 507.93 4.94 o 2 1 -5 135.05 144.00 3.37 o 2 2 -5 201.10 217.00 4.57 o -3 -2 -4 6.14 5.75 0.78 o 2 1 -4 535.03 557.56 6.06 o 2 2 -4 9.47 9.79 1.45 o 3 2 -4 429.25 440.53 6.47 o -3 -2 -3 504.23 513.58 4.50 o 1 0 -3 5781.30 5659.05 13.50 o 2 1 -3 1295.60 1316.17 8.67 o 2 2 -3 396.48 404.63 5.52 o 3 2 -3 233.60 232.49 4.57 o 2 3 -3 241.18 250.27 5.15 o -4 -2 -2 195.14 199.09 3.72 o -3 -2 -2 160.51 156.09 2.76 o 2 1 -2 1793.70 1828.09 9.56 o 2 2 -2 139.27 144.25 3.20 o 3 2 -2 749.76 775.07 7.71 o 2 3 -2 544.73 548.95 6.92 o 3 3 -2 516.60 510.98 7.06 o -5 -2 -1 206.00 192.97 4.26 o -4 -2 -1 290.77 283.85 4.49 o -2 -1 -1 1118.94 1146.75 5.94 o 1 1 -1 2556.59 2560.69 9.00 o 2 2 -1 486.48 488.46 5.29 o 2 3 -1 179.58 177.80 3.83 o 3 3 -1 164.81 165.95 3.97 o -4 -2 0 122.01 120.13 3.18 o -2 -1 0 1396.30 1417.88 7.21 o 1 1 0 1362.32 1323.48 5.65 o 2 2 0 167.73 155.76 2.82 o 2 3 0 167.63 143.41 3.28 o 3 3 0 147.90 141.38 3.46 o -4 -2 1 201.11 179.25 4.51 o -3 -1 1 342.01 366.44 4.72 o -2 -1 1 2010.12 1975.37 9.16 o 1 1 1 750.81 712.63 3.45 o 2 2 1 229.43 218.64 3.06 o 2 3 1 608.26 600.15 6.00 o -4 -2 2 183.35 185.22 4.24 o -4 -1 2 152.83 156.01 3.75 o -3 -1 2 158.68 157.24 3.50 o -2 -1 2 1798.21 1843.81 9.52 o -4 -1 3 361.78 361.65 5.77 o -3 -1 3 255.08 259.60 4.38 o -2 -1 3 1276.26 1309.51 8.59 o -1 0 3 5739.30 5546.65 13.37 o -4 -1 4 151.57 158.09 4.04 o -3 -1 4 1091.10 1132.58 9.34 o -2 0 4 1428.99 1447.06 8.87 o 0 1 4 87.95 85.16 1.24 o -3 -1 5 182.42 179.36 4.06 o -3 0 5 35.71 34.02 1.97 o -1 0 5 511.75 491.82 4.84 o -3 -1 6 653.38 723.40 8.23 o -2 0 6 406.46 438.30 5.47 o -1 1 6 425.60 424.38 4.38 o 0 2 6 155.08 147.79 1.85 o -3 0 7 0.78 3.68 1.43 o -2 1 7 66.82 66.85 2.30 o -1 1 7 140.56 145.85 2.81 o -2 0 8 57.23 66.62 2.64 o -3 1 8 99.14 95.20 3.28 o -2 1 8 187.41 191.97 3.86 o -1 1 8 534.85 540.56 5.56 o -2 1 9 200.65 192.34 4.07 o -2 1 10 310.11 301.42 5.34 o 1 -1 -8 151.04 146.38 3.77 o 1 -1 -7 40.17 41.12 2.11 o 2 -1 -7 19.13 17.77 1.62 o 3 0 -7 0.38 0.00 1.17 o -1 -2 -6 135.23 141.80 3.40 o 0 -2 -6 45.78 48.08 2.21 o 0 -1 -6 6.60 7.84 1.17 o 2 -1 -6 49.54 47.39 2.18 o 2 0 -6 115.56 119.89 2.89 o 4 0 -6 53.83 53.74 2.30 o -1 -3 -5 24.54 29.22 1.90 o -1 -2 -5 53.30 51.21 2.05 o 0 -2 -5 65.00 71.11 2.46 o 0 -1 -5 110.90 107.25 2.68 o 1 -1 -5 89.67 86.51 2.45 o 3 0 -5 9.97 8.61 1.14 o -1 -3 -4 21.64 20.97 1.67 o -1 -2 -4 61.43 65.33 2.08 o 0 -2 -4 16.67 15.90 1.33 o 0 -1 -4 25.55 25.79 1.41 o 1 -1 -4 113.43 108.23 2.53 o 2 0 -4 415.35 399.45 4.27 o 4 1 -4 43.47 43.93 1.48 o -1 -2 -3 100.87 101.27 2.32 o 0 -1 -3 339.36 315.41 3.59 o 1 0 -3 1659.81 1582.52 6.96 o 3 1 -3 72.50 73.78 1.49 o -1 -2 -2 44.86 44.73 1.51 o -1 -1 -2 663.80 654.26 4.17 o 3 1 -2 19.25 17.33 0.67 o -2 -2 -1 66.01 66.70 1.34 o -2 -2 0 49.48 47.38 0.94 o 1 1 2 664.41 672.38 4.21 o -2 -1 3 366.41 376.10 2.98 o -1 0 3 1647.75 1616.78 7.07 o 1 1 3 246.06 255.03 3.09 o -2 -1 4 153.63 158.75 2.36 o 0 1 4 25.25 24.56 1.40 o 1 1 4 120.78 118.68 2.45 o 3 2 4 1.99 2.66 0.79 o -1 0 5 146.92 149.35 2.84 o 0 1 5 109.91 112.47 2.66 o 1 1 5 131.92 139.69 2.90 o 2 2 5 36.70 39.24 1.76 o -2 -1 6 50.20 52.38 1.85 o 0 1 6 6.78 7.49 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