[Open access]

Acta Cryst. (2012). E68, i88
[ doi:10.1107/S1600536812044224 ]

Li0.17Na5.83Mo11O36

I. Ennajeh, H. Hamza, M. F. Zid and A. Driss


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)... ? PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms .. ? PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.749 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT975_ALERT_2_C Positive Residual Density at 0.88A from O7 . 0.94 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 0.57A from O5 . 0.92 eA-3
Alert level G PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ... ? PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 53.47 PLAT112_ALERT_2_G ADDSYM Detects Additional (Pseudo) Symm. Elem... m PLAT112_ALERT_2_G ADDSYM Detects Additional (Pseudo) Symm. Elem... c PLAT113_ALERT_2_G ADDSYM Suggests Possible Pseudo/New Space-group. Cccm PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 50 Perc. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 1 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 46
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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