[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, o3404-o3405
[ doi:10.1107/S1600536812046909 ]

Ethyl 4-(5-bromo-1H-indol-3-yl)-2,6,6-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate

M. G. Gündüz, R. J. Butcher, S. Öztürk Yildirim, A. El-Khouly, C. Safak and R. Simsek


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 4.272 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 42
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 4 PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.83 mm PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 14 PLAT793_ALERT_4_G The Model has Chirality at C7A (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at C7B (Verify) .... R PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 265
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check
checkCIF publication errors
Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
Author Response: Author Response: As the reported work is a part of collaboration between three Universities. Hence the number of authors are greater than 5. Synthesis has been carried out by M. G. G\"und\"uz, A. El-Khouly, C. \,Safak and R. \,Simsek while S. \"Ozt\"urk Yildirim and R. J. Butcher are responsible for the single crystal growth, X-ray data collection, refinement of the structure, structure completion in the form of paper.

1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing

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