Acta Crystallographica Section E

Structure Reports Online

Volume 68, Part 12 (December 2012)

organic compounds

Acta Cryst. (2012). E68, o3494    [ doi:10.1107/S1600536812047769 ]


S. Wilbrand, C. Neis and K. Hegetschweiler

Abstract: The crystal structure of the title compound, C8H9NO3, features centrosymmetric dimers with two amide groups inter­connected by a pair of almost linear N-H...O hydrogen bonds. Through inter­molecular O-H...O inter­actions between phenolic hy­droxy groups and carbonyl O atoms, these dimers are assembled into undulating hydrogen-bonded layers parallel to the [101] plane. Additionally, the anti-H(-N) atom of the primary amide group forms an intra­molecular hydrogen bond to the O atom of the meth­oxy group. The amide group froms a dihedral angle of 12.6 (1)° with the phenyl ring.

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