[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, o3484
[ doi:10.1107/S1600536812048234 ]

Tris(naphthalen-1-yl)phosphane chloroform hemisolvate

W. L. Davis and A. Muller


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ ? PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0042 Ang PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -0.165
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 0.50 Ratio PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large. 0.10 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C31 PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 47
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster