[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1439
[ doi:10.1107/S1600536812044078 ]

1-[(Z)-1-Ferrocenylethylidene]thiocarbonohydrazide

A. M. Asiri, M. N. Arshad, M. Ishaq, K. A. Alamry and M. Shafiq


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Fe1 PLAT353_ALERT_3_C Long N-H Bond (0.87A) N3 - H3N ... 1.05 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ... ? PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large. 0.11 PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c ....... P21/a PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 75 PLAT982_ALERT_1_G The C-f'= 0.003 Deviates from the IT-value 0.018 PLAT982_ALERT_1_G The N-f'= 0.006 Deviates from the IT-value 0.031 PLAT983_ALERT_1_G The N-f"= 0.003 Deviates from the IT-Value 0.018
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster